Bicontinuous Block Copolymer Microparticles through Hydrogen-Bonding-Mediated Dual Phase Separation between Polymer Segments and Fluorinated Additives DOI
Min Ren, Mengmeng Zhang,

Zaiyan Hou

и другие.

ACS Nano, Год журнала: 2024, Номер unknown

Опубликована: Дек. 22, 2024

Bicontinuous microparticles have advanced transport, mechanical, and electrochemical properties show promising applications in energy storage, catalysis, other fields. However, it remains a great challenge to fabricate bicontinuous of block copolymers (BCPs) by controlling the microphase separation due extremely narrow region structure phase diagram. Here, we demonstrate strategy balance BCPs fluorinated additives at different length scales emulsion droplets, providing large window access microparticles. The key point is simultaneously introduce contradictory attractive–repulsive interactions between poly(4-vinylpyridine)-containing carboxylated perfluorinated additives. Hydrogen bonding poly(4-vinylpyridine) carboxyl groups, as an attractive interaction, directs Meanwhile, repulsive interaction high immiscibility perfluoroalkyl residues induces macrophase separation. compromise triggers formation space. In addition, vulnerable nature hydrogen provides flexible route for reversibly shaping BCP assemblies. This work establishes platform fabricating structured which structures are hardly accessible through traditional solution self-assembly.

Язык: Английский

Advancing Adsorption and Separation with Modified SBA-15: A Comprehensive Review and Future Perspectives DOI Creative Commons
Binjun Liang,

Pingxin Zhu,

Jihan Gu

и другие.

Molecules, Год журнала: 2024, Номер 29(15), С. 3543 - 3543

Опубликована: Июль 27, 2024

Mesoporous silica SBA-15 has emerged as a promising adsorbent and separation material due to its unique structural physicochemical properties. To further enhance performance, various surface modification strategies, including metal oxide noble incorporation for improved catalytic activity stability, organic functionalization with amino thiol groups enhanced adsorption capacity selectivity, inorganic-organic composite synergistic effects, have been extensively explored. This review provides comprehensive overview of the recent advances in applications. The synthesis methods, properties, advantages are discussed, followed by detailed analysis different strategies their structure-performance relationships. performance functionalized materials removal pollutants, heavy ions, gases, biomolecules, well chromatographic solid-liquid separation, is critically evaluated. Despite significant progress, challenges opportunities future research identified, development low-cost sustainable routes, rational design SBA-15-based tailored integration into practical aims guide efforts developing advanced environmental industrial applications, an emphasis on green scalable strategies.

Язык: Английский

Процитировано

8

A“Duet‐Insurance” Sensing Strategy by Combining Janus TpMa COF/Eu‐doped α‐Fe2O3 and Variable‐Temperature Excitation for Robust, Visual Indoor Pollution Gas Detection DOI
Bing Yu,

Zhao Song,

Hongtao Jiang

и другие.

Advanced Functional Materials, Год журнала: 2024, Номер unknown

Опубликована: Дек. 11, 2024

Abstract Water competitive adsorption and limited reaction sites on the micro‐scale sensing area of micro‐electro‐mechanical system (MEMS) sensors are two bottleneck problems that restrict detection trace indoor polluted gases, leading to drifting weak signals. To address this, a “duet‐insurance” strategy is proposed protect amplify signal. For first‐level protection, well‐designed double‐layer structure consisting Janus TpMa covalent organic framework (COF)/Eu‐doped α‐Fe 2 O 3 can resist diffusion water molecules facilitate electron transfer from formaldehyde (CH O) layers, benefiting outer hydrophobic character strong CH capacity Eu‐doped Fe . second‐level amplification, unique variable temperature excitation facilitates deep penetration into active across COF enabling signal amplification through thermally actuated carrier modulation. The sensor demonstrates high ability O, with an ultra‐low limit 794 ppt. Leveraging novel strategy, multi‐functional, visual designed identify multi‐indoor pollution gases by feature encoding color mapping, showcasing promising potential for MEMS based COF/Eu‐doped materials.

Язык: Английский

Процитировано

3

Short Aromatic Blocks Enhance Styrene Conversion in Polymer Cubosome Formation via Polymerization‐Induced Self‐Assembly DOI Open Access

Yalan Sun,

Yongbin Zhao,

Aihua Chen

и другие.

Macromolecular Rapid Communications, Год журнала: 2025, Номер unknown

Опубликована: Янв. 7, 2025

Polymer cubosomes (PCs) have garnered significant interest in the field of nanomaterials and nanotechnology due to their unique properties potential applications. However, fabrication PCs remains challenging. Polymerization-induced self-assembly (PISA) is recognized as an efficient method for producing a variety polymer particles, including PCs. Despite advantages PISA, conversion styrene (St), core-forming monomer commonly used PC preparation, relatively low. Herein, novel strategy introduced enhance St preparation via PISA by incorporating short azobenzene-containing block (PMAAz) into hydrophilic macro-chain transfer agent (macro-CTA). Utilizing PMAAz-tailed poly(poly(ethylene glycol) methyl ether methacrylate), successfully improved from initial 12.9-13.8% enhanced range 19.1-26.9%. This enhancement allows reduced feeding ratio macro-CTA Further studies various blocks consisting different hydrophobic monomers reveal that aromatic interactions, derived these blocks, are crucial increasing facilitating formation. study offers direct convenient approach obtaining with diversified functional groups efficiently, thereby significantly broadening application materials.

Язык: Английский

Процитировано

0

Visualization of different morphologies of block copolymer assemblies using various fluorescent colors via the introduction of solvent-responsive AIEgen DOI

Shaoyu Xu,

Mian Wang, Hui Liu

и другие.

Science China Chemistry, Год журнала: 2025, Номер unknown

Опубликована: Апрель 23, 2025

Язык: Английский

Процитировано

0

A Regiospecific Co-Assembly Method to Functionalize Ordered Mesoporous Metal Oxides with Customizable Noble Metal Nanocrystals DOI Creative Commons
Jichun Li, Lingxiao Xue, Yu Deng

и другие.

ACS Central Science, Год журнала: 2024, Номер 10(12), С. 2274 - 2284

Опубликована: Ноя. 21, 2024

An efficient regiospecific co-assembly (RSCA) strategy is developed for general synthesis of mesoporous metal oxides with pore walls precisely decorated by highly dispersed noble nanocrystals customized parameters (diameter and composition). It features the rational utilization specific interactions between hydrophilic molecular precursors, hydrophobic nanocrystals, amphiphilic block copolymers, to achieve as confirmed dynamics simulations. Through this RSCA strategy, we achieved a controllable variety functional oxide composites (e.g., WO3, ZrO2, TiO2) in-pore various tailored components (Au, Ag, Pt, Pd their nanoalloys) sizes (3.0-8.5 nm). As an example, obtained 0.5-Ag/WO3 material has interconnected structure uniform 6.5 nm Ag confined in mesopores, showing superior NO sensing performances high sensitivity, good selectivity, stability at low working temperature (127 °C). In situ spectroscopy study indicates that process involves unique gas-solid reaction, where molecules are converted into chemisorbed x species over sensitive materials, inducing remarkable change resistance outputting dramatic response signal.

Язык: Английский

Процитировано

1

Synthesis and Self‐Assembly of Poly(4‐acetoxystyrene) Cubosomes DOI Creative Commons

Marcel Schumacher,

Marvin Foith,

Manuel Trömer

и другие.

Macromolecular Rapid Communications, Год журнала: 2024, Номер unknown

Опубликована: Окт. 16, 2024

Abstract Polymer cubosomes (PCs) are a recent class of self‐assembled nanostructures with great application potential due to their high porosity and surface area. Currently, most reported PCs consist polystyrene block copolymers (BCPs), for which self‐assembly parameters rather well understood. Changing the chemistry would be desirable introduce more functionality; however, knowledge adapting process new chemistries remains limited. This work, reports on synthesizing poly(ethylene oxide)‐ ‐poly(4‐acetoxystyrene) its styrene, provide conditions into yield inner order. It is shown that polarity starting solvent toward corona allows tuning final morphology by controlling volume packing parameter.

Язык: Английский

Процитировано

0

Bicontinuous Block Copolymer Microparticles through Hydrogen-Bonding-Mediated Dual Phase Separation between Polymer Segments and Fluorinated Additives DOI
Min Ren, Mengmeng Zhang,

Zaiyan Hou

и другие.

ACS Nano, Год журнала: 2024, Номер unknown

Опубликована: Дек. 22, 2024

Bicontinuous microparticles have advanced transport, mechanical, and electrochemical properties show promising applications in energy storage, catalysis, other fields. However, it remains a great challenge to fabricate bicontinuous of block copolymers (BCPs) by controlling the microphase separation due extremely narrow region structure phase diagram. Here, we demonstrate strategy balance BCPs fluorinated additives at different length scales emulsion droplets, providing large window access microparticles. The key point is simultaneously introduce contradictory attractive–repulsive interactions between poly(4-vinylpyridine)-containing carboxylated perfluorinated additives. Hydrogen bonding poly(4-vinylpyridine) carboxyl groups, as an attractive interaction, directs Meanwhile, repulsive interaction high immiscibility perfluoroalkyl residues induces macrophase separation. compromise triggers formation space. In addition, vulnerable nature hydrogen provides flexible route for reversibly shaping BCP assemblies. This work establishes platform fabricating structured which structures are hardly accessible through traditional solution self-assembly.

Язык: Английский

Процитировано

0