Directional Electron Flow in a Selenoviologen‐Based Tetracationic Cyclophane for Enhanced Visible‐Light‐Driven Hydrogen Evolution DOI

Naiyao Li,

Yawen Li,

Zengrong Wang

и другие.

Angewandte Chemie, Год журнала: 2024, Номер 136(47)

Опубликована: Июль 23, 2024

Abstract Directional electron flow in the photocatalyst enables efficient charge separation, which is essential for photocatalysis of H 2 production. Here, we report a novel class tetracationic cyclophanes ( 7 ) incorporating bipyridine Pt(II) and selenoviologen. X‐ray single‐crystal structures reveal that not only fixes distances spatial positions between its individual units but also exhibits box‐like rigid electron‐deficient cavity. Moreover, host–guest recognition phenomena are observed ferrocene, forming complexes with 1 : stoichiometry. good redox properties, narrow energy gaps, strong absorption visible range (370–500 nm) due to containing two selenoviologen (SeV 2+ units. Meanwhile, femtosecond transient (fs‐TA) reveals has stabilized dicationic biradical, facilitates directional achieve transfer formation cyclophane electronic architecture. Then, applied visible‐light‐driven hydrogen evolution high production (132 μmol), generation rate (11 μmol/h), turnover number (221), apparent quantum yield (1.7 %), provides simplified photocatalytic strategy solar conversion.

Язык: Английский

An electrochromic device based on dynamic coordination and the dissociation of Fe2+/Fe3+ and a leuco dye with an improved cycle life DOI

Ruipeng Shen,

Min Li, Shuo Wang

и другие.

Journal of Materials Chemistry C, Год журнала: 2025, Номер unknown

Опубликована: Янв. 1, 2025

Electrochromic device based Fe n + and a leuco dye has been fabricated, which shows satisfying cycle life optical modulate ability. This strategy to improve may accelerate the application of electrochromic devices.

Язык: Английский

Процитировано

0

Hydrogen-bonded green box-based host-guest complexes on g-C3N4 composites for enhanced visible-light photocatalysis DOI
Yawen Li,

Naiyao Li,

Tianle Cao

и другие.

Science China Chemistry, Год журнала: 2025, Номер unknown

Опубликована: Март 31, 2025

Язык: Английский

Процитировано

0

Directional Electron Flow in a Selenoviologen‐Based Tetracationic Cyclophane for Enhanced Visible‐Light‐Driven Hydrogen Evolution DOI

Naiyao Li,

Yawen Li,

Zengrong Wang

и другие.

Angewandte Chemie International Edition, Год журнала: 2024, Номер 63(47)

Опубликована: Июль 23, 2024

Abstract Directional electron flow in the photocatalyst enables efficient charge separation, which is essential for photocatalysis of H 2 production. Here, we report a novel class tetracationic cyclophanes ( 7 ) incorporating bipyridine Pt(II) and selenoviologen. X‐ray single‐crystal structures reveal that not only fixes distances spatial positions between its individual units but also exhibits box‐like rigid electron‐deficient cavity. Moreover, host–guest recognition phenomena are observed ferrocene, forming complexes with 1 : stoichiometry. good redox properties, narrow energy gaps, strong absorption visible range (370–500 nm) due to containing two selenoviologen (SeV 2+ units. Meanwhile, femtosecond transient (fs‐TA) reveals has stabilized dicationic biradical, facilitates directional achieve transfer formation cyclophane electronic architecture. Then, applied visible‐light‐driven hydrogen evolution high production (132 μmol), generation rate (11 μmol/h), turnover number (221), apparent quantum yield (1.7 %), provides simplified photocatalytic strategy solar conversion.

Язык: Английский

Процитировано

2

A Triphasic Membrane-Free Redox Flow Battery in a Total Aqueous System DOI
Junjie Liu,

Jintao Deng,

Yutong Hua

и другие.

ACS Applied Energy Materials, Год журнала: 2024, Номер unknown

Опубликована: Ноя. 28, 2024

The membrane-free redox flow battery (RFB) represents an innovative design philosophy that encompasses reduced costs, flexible schemes, and enhanced overall performance. However, despite these advantages, RFBs encounter several challenges including low Coulombic efficiency (CE), limited cycling stability, elevated toxicity from organic solvents. Aiming at issues, we constructed a triphasic RFB using total aqueous system. electrolytes for both the anolyte catholyte are extracted tetrabutylammonium chloride-Na2SO4–H2O salting-out system, while other phase serves as separator. A novel material, N,N′-di(ethyl butyrate)-4,4′-bipyridinium dichloride, significantly boosts performance when paired with 2,2,6,6-tetramethylpiperidine-N-oxyl-4-sulfate potassium catholyte. Our static delivers open-circuit voltage of 1.24 V, demonstrating stable energy capacity loss 0.064% per hour average CE 98.6% over 493 h (345 cycles). Furthermore, have conducted preliminary construction exhibited efficiency, decay 0.035% cycle 98.7%. These results provide promising evidence supporting feasibility this all-aqueous RFB. We also identify primary intermediate species following extended elucidate two potential degradation pathways material. anticipate combined our scheme comprehensive mechanistic analysis, will expand research scope RFBs.

Язык: Английский

Процитировано

1

Donor–Acceptor Viologens with Through‐Space Conjugation for Enhanced Visible‐Light‐Driven Photocatalysis DOI Creative Commons
Yi Qiao, Liang Xu, Xiaoyang Liu

и другие.

Advanced Science, Год журнала: 2024, Номер 12(2)

Опубликована: Ноя. 21, 2024

Abstract A series of novel donor–acceptor (D–A) type viologens with through‐space conjugation (TSC) are synthesized. The synergistic effect D–A and TSC endow these compounds a narrower energy gap, excellent redox properties, strong absorption in the visible range (up to 450 nm), high efficiency intramolecular charge transfer (ICT). These also exhibit long‐lived separation state stable radical formation. Considering their impressive photophysical explored for visible‐light‐driven photocatalysis. As catalyst oxidative coupling reactions under light, compound 9 can achieve yield 94%, attributed its ICT effect. Additionally, hybridized into graphitic carbon nitride (g‐C₃N₄), enhances hydrogen production performance achieving an H 2 generation rate 4102 µmol h −1 g . This study highlights potential applications photocatalytic systems.

Язык: Английский

Процитировано

1

Directional Electron Flow in a Selenoviologen‐Based Tetracationic Cyclophane for Enhanced Visible‐Light‐Driven Hydrogen Evolution DOI

Naiyao Li,

Yawen Li,

Zengrong Wang

и другие.

Angewandte Chemie, Год журнала: 2024, Номер 136(47)

Опубликована: Июль 23, 2024

Abstract Directional electron flow in the photocatalyst enables efficient charge separation, which is essential for photocatalysis of H 2 production. Here, we report a novel class tetracationic cyclophanes ( 7 ) incorporating bipyridine Pt(II) and selenoviologen. X‐ray single‐crystal structures reveal that not only fixes distances spatial positions between its individual units but also exhibits box‐like rigid electron‐deficient cavity. Moreover, host–guest recognition phenomena are observed ferrocene, forming complexes with 1 : stoichiometry. good redox properties, narrow energy gaps, strong absorption visible range (370–500 nm) due to containing two selenoviologen (SeV 2+ units. Meanwhile, femtosecond transient (fs‐TA) reveals has stabilized dicationic biradical, facilitates directional achieve transfer formation cyclophane electronic architecture. Then, applied visible‐light‐driven hydrogen evolution high production (132 μmol), generation rate (11 μmol/h), turnover number (221), apparent quantum yield (1.7 %), provides simplified photocatalytic strategy solar conversion.

Язык: Английский

Процитировано

0