Chiral Self‐Assembly of Twisted Prisms, Cuboids, and Polyhedral Capped Cages with Tartrate Ligands DOI

Qiu‐Shui Mu,

Xinyu Wang, Xiang Gao

и другие.

Small, Год журнала: 2024, Номер unknown

Опубликована: Окт. 6, 2024

Abstract Homochiral triangular prisms, cuboid cages, and capped polyhedral cages are successfully synthesized via coordination‐driven self‐assembly. Typical tartrate ligands demonstrated notable torsional flexibility variable coordination numbers, allowing for diverse patterns, including saturated chelation terminal mono‐coordination with half‐sandwich rhodium iridium fragments. The ligand lengths, molar ratios, metal vertices meticulously designed fine‐tuned to yield chiral entirely distinct architectures. Tartrate exhibits abundant hydrogen bonding interactions induction capabilities, these supramolecular assemblies characterized by single‐crystal X‐ray diffraction, nuclear magnetic resonance, circular dichroism spectroscopy. An efficient method is developed constructing structurally versatile cage‐like entities, facilitating self‐assembly in complicated multi‐component systems.

Язык: Английский

Supramolecular Eu(III)4L4 Tetrahedra-Based Films for Luminescence Sensing of Volatile Amines with Sub-ppt-Level Detection Limit DOI
Yang Zhou, Fan Yin,

Shao‐Jun Hu

и другие.

Inorganic Chemistry, Год журнала: 2025, Номер unknown

Опубликована: Март 27, 2025

Metal–organic cages are a class of discrete supramolecular architectures endowed with well-defined cavity and diverse functionalities, offering broad range applications that, however, predominantly confined to liquid phases. In this study, we present the self-assembly Eu(III)4L4 tetrahedra, constructed from triarylborane-cored tritopic tridentate ligands, which were fabricated into spin-coated films bright emission, smooth surfaces, uniform thickness. These demonstrated ultralow detection limits for series volatile amines, reaching sub-ppt level. This work serves as compelling example preparation application metal–organic-cage-based films, paving way broader scenarios.

Язык: Английский

Процитировано

0

Chiral Self‐Assembly of Twisted Prisms, Cuboids, and Polyhedral Capped Cages with Tartrate Ligands DOI

Qiu‐Shui Mu,

Xinyu Wang, Xiang Gao

и другие.

Small, Год журнала: 2024, Номер unknown

Опубликована: Окт. 6, 2024

Abstract Homochiral triangular prisms, cuboid cages, and capped polyhedral cages are successfully synthesized via coordination‐driven self‐assembly. Typical tartrate ligands demonstrated notable torsional flexibility variable coordination numbers, allowing for diverse patterns, including saturated chelation terminal mono‐coordination with half‐sandwich rhodium iridium fragments. The ligand lengths, molar ratios, metal vertices meticulously designed fine‐tuned to yield chiral entirely distinct architectures. Tartrate exhibits abundant hydrogen bonding interactions induction capabilities, these supramolecular assemblies characterized by single‐crystal X‐ray diffraction, nuclear magnetic resonance, circular dichroism spectroscopy. An efficient method is developed constructing structurally versatile cage‐like entities, facilitating self‐assembly in complicated multi‐component systems.

Язык: Английский

Процитировано

0