Preparation and characterisation of BiOCl nano photocatalyst for the remediation of wastewater under LED light DOI
Brijesh Pare,

Roshni Joshi,

S.P.S. Mehta

и другие.

International Journal of Environmental & Analytical Chemistry, Год журнала: 2024, Номер unknown, С. 1 - 25

Опубликована: Дек. 22, 2024

Dye, a major global pollutant causing environmental and health issues, can be effectively degraded through photocatalysis. This study synthesised bismuth oxychloride (BiOCl) nano-photocatalyst via hydrolysis characterized it using various analytical instruments. The UV-Vis absorbance of the displayed peaks at 211 nm, 361 688 with band gap 3.0 eV, conduction minimum 1.97 valence maximum 4.97 eV. dynamic light scattering showed 3349 nm 660 while BiOCl had zeta potential -17.3 mV conductivity 0.245 mS/cm. X-ray diffraction exhibited four sharp intensity 11.95º, 25.81º, 32.50º, 33.40º, average crystallite size was 43.39 scanning electron microscope plate-like morphology. achieved 88.21% degradation methyl green within 60 minutes under LED irradiation pH 7.5 dye concentration 6×10−6 mol/L. photocatalytic performance, driven by hydroxyl (•OH) superoxide (O2•−) radicals, 96.55% mineralization as confirmed COD analysis. These findings emphasize for effective sustainable wastewater remediation visible conditions.

Язык: Английский

Innovative use of recycled aluminum adsorbent for methylene blue adsorption and post-application for soil stabilization DOI
Emad Hussein,

Farouk Abdullah Rasheed

Journal of Contaminant Hydrology, Год журнала: 2025, Номер 272, С. 104553 - 104553

Опубликована: Март 28, 2025

Язык: Английский

Процитировано

0

Amoxicillin adsorption onto oil palm trunk‐derived activated carbon: synthesis optimization, modelling of mass transfer and ultrasonic regeneration DOI
Mohamad Firdaus Mohamad Yusop,

M S Baharudin,

Md Mamoon Rashid

и другие.

Journal of Chemical Technology & Biotechnology, Год журнала: 2025, Номер unknown

Опубликована: Апрель 10, 2025

Abstract BACKGROUND Antibiotics such as amoxicillin (AMC) can persist in the environment due to their stable molecular structures. This study aimed (i) optimize synthesis of oil palm trunk‐based activated carbon (OPTAC) for AMC removal, (ii) model adsorption process using mass transfer (MTM) and (iii) evaluate OPTAC regeneration through ultrasonic washing. was synthesized potassium hydroxide activation followed by dioxide treatment. RESULTS Response surface methodology (RSM) identified optimal conditions at 343 W, 12.87 min an impregnation ratio 2.00 g −1 . Under these conditions, predicted uptake 146.44 mg (actual: 154.15 ; 5.00% error), yield 42.78% 41.19%; 3.86% error). The AMC–OPTAC Freundlich isotherm, with a Langmuir capacity ( Q m ) 238.67 Kinetic analysis revealed that pseudo‐first‐order best described system. MTM yielded average constant k 0.23 L h , rate 0.00051 estimated area 611.34 2 closely matching measured mesopore (647.82 5.63% Thermodynamic confirmed physisorption dominant mechanism, spontaneous endothermic behavior. In studies, washing outperformed microwave reactivation, maintaining removal efficiency above 50% five cycles, compared three CONCLUSIONS RSM successfully optimized yield, while effectively active involved process. © 2025 Society Chemical Industry (SCI).

Язык: Английский

Процитировано

0

Optimized size and stability of composite CuOZnO metal oxide nanoparticles for efficient removal of Reactive Black 5 dye DOI

Shanza Shafaat,

Nasira Hussain,

Zeeshan Abbasi

и другие.

Journal of Chemical Technology & Biotechnology, Год журнала: 2025, Номер unknown

Опубликована: Апрель 16, 2025

Abstract BACKGROUND The increasing contamination of water bodies with industrial dyes necessitates efficient remediation strategies. CuO–ZnO composite nanoparticles (NPs) have shown promise as adsorbents due to their high surface area, stability, and tunable properties. This study focuses on optimizing the synthesis conditions CuO‐ZnO NPs via a co‐precipitation method evaluating performance for removal Reactive Black 5 (RB5) dye. RESULTS were synthesized varied precursor ratios, pH values, temperatures, reagent addition times achieve optimal size stability. Characterization using ultraviolet–visible spectroscopy, fluorescence, X‐ray diffraction, Fourier transform infrared dynamic light scattering, vibrating‐sample magnetometry, Brunauer–Emmett–Teller analysis confirmed structural, optical, physical properties optimized composite. smallest highest stability concentration ratio 50:50 was obtained at 11, 80 °C, time min. Composite show ferromagnetic behavior. adsorption efficiency RB5 dye studied under different operational parameters, revealing that maximum (92%) occurred 2 contact 60 Adsorption kinetics followed pseudo‐first‐order model, while equilibrium data aligned Freundlich isotherm, indicating multilayer adsorption. Thermodynamic endothermic spontaneous nature process. CONCLUSION demonstrated maintained significant reusability across multiple adsorption–desorption cycles. These findings highlight potential an effective sustainable adsorbent wastewater treatment. © 2025 Society Chemical Industry (SCI).

Язык: Английский

Процитировано

0

Preparation and characterisation of BiOCl nano photocatalyst for the remediation of wastewater under LED light DOI
Brijesh Pare,

Roshni Joshi,

S.P.S. Mehta

и другие.

International Journal of Environmental & Analytical Chemistry, Год журнала: 2024, Номер unknown, С. 1 - 25

Опубликована: Дек. 22, 2024

Dye, a major global pollutant causing environmental and health issues, can be effectively degraded through photocatalysis. This study synthesised bismuth oxychloride (BiOCl) nano-photocatalyst via hydrolysis characterized it using various analytical instruments. The UV-Vis absorbance of the displayed peaks at 211 nm, 361 688 with band gap 3.0 eV, conduction minimum 1.97 valence maximum 4.97 eV. dynamic light scattering showed 3349 nm 660 while BiOCl had zeta potential -17.3 mV conductivity 0.245 mS/cm. X-ray diffraction exhibited four sharp intensity 11.95º, 25.81º, 32.50º, 33.40º, average crystallite size was 43.39 scanning electron microscope plate-like morphology. achieved 88.21% degradation methyl green within 60 minutes under LED irradiation pH 7.5 dye concentration 6×10−6 mol/L. photocatalytic performance, driven by hydroxyl (•OH) superoxide (O2•−) radicals, 96.55% mineralization as confirmed COD analysis. These findings emphasize for effective sustainable wastewater remediation visible conditions.

Язык: Английский

Процитировано

0