Maneuvering the Electronic State and Active Site of Assembled-Gold Nanoclusters through Polyoxometalate Implantation for Heterogeneous Green-Light Photocatalysis DOI

Satya Ranjan Sahoo,

Tarun Kumar Dinda, Sumit Saha

и другие.

ACS Applied Materials & Interfaces, Год журнала: 2025, Номер unknown

Опубликована: Март 25, 2025

Gold nanoclusters (AuNCs) exhibit unique molecule-like optical and electronic properties, making them promising candidates for photocatalysis. However, their application as primary photocatalysts in heterogeneous systems is limited by rapid electron recombination, small size, high solubility. To overcome these limitations, we developed an approach combining AuNCs assemblies with trap centers to enhance charge separation transfer. Using a depletion-driven assembly method, Keggin-type polyoxometalates (POMs), Na10SiW9O34 (SiW9), were uniformly embedded within spherical of glutathione-protected AuNCs, forming gold superclusters (AuSCs). The resulting AuSCs@SiW9 exhibited complete photoluminescence quenching, enhanced metallicity, stabilized photogenerated electrons via SiW9, enabling use photocatalysts. efficiently catalyzed the functionalization terminal aryl alkyne N-bromosuccinimide (NBS), achieving tribromoketones yield 94%, significantly outperforming AuSCs lower or higher metallicity (38 65%, respectively). Mechanistic studies revealed that improved promotes transfer complex formation NBS, while SiW9 stabilizes electrons, enhancing density under light irradiation. strong visible-light absorption, photostability, solvent dispersibility, recyclability up five cycles scalability broader applications. This strategy positions viable photocatalyst, expanding its potential photocatalysis toward synthesizing molecules.

Язык: Английский

Photo(electro)catalytic Water Splitting for Hydrogen Production: Mechanism, Design, Optimization, and Economy DOI Creative Commons
Xingpeng Li, Chenxi Zhang, Jiafeng Geng

и другие.

Molecules, Год журнала: 2025, Номер 30(3), С. 630 - 630

Опубликована: Янв. 31, 2025

As an energy carrier characterized by its high density and eco-friendliness, hydrogen holds a pivotal position in transition. This paper elaborates on the scientific foundations recent progress of photo- electro-catalytic water splitting, including corresponding mechanism, material design optimization, economy production. It systematically reviews research photo(electro)catalytic materials, oxides, sulfides, nitrides, noble metals, non-noble metal, some novel photocatalysts provides in-depth analysis strategies for optimizing these materials through design, component adjustment, surface modification. In particular, it is pointed out that nanostructure regulation, dimensional engineering, defect introduction, doping, alloying, functionalization can remarkably improve catalyst performance. The importance adjusting reaction conditions, such as pH addition sacrificial agents, to boost catalytic efficiency also discussed, along with comparison cost-effectiveness different production technologies. Despite significant advancements made splitting technology, this highlights challenges faced field, development more efficient stable photo(electro)catalysts, improvement system conversion efficiency, cost reduction, promotion technology industrialization, addressing environmental issues.

Язык: Английский

Процитировано

0

Maneuvering the Electronic State and Active Site of Assembled-Gold Nanoclusters through Polyoxometalate Implantation for Heterogeneous Green-Light Photocatalysis DOI

Satya Ranjan Sahoo,

Tarun Kumar Dinda, Sumit Saha

и другие.

ACS Applied Materials & Interfaces, Год журнала: 2025, Номер unknown

Опубликована: Март 25, 2025

Gold nanoclusters (AuNCs) exhibit unique molecule-like optical and electronic properties, making them promising candidates for photocatalysis. However, their application as primary photocatalysts in heterogeneous systems is limited by rapid electron recombination, small size, high solubility. To overcome these limitations, we developed an approach combining AuNCs assemblies with trap centers to enhance charge separation transfer. Using a depletion-driven assembly method, Keggin-type polyoxometalates (POMs), Na10SiW9O34 (SiW9), were uniformly embedded within spherical of glutathione-protected AuNCs, forming gold superclusters (AuSCs). The resulting AuSCs@SiW9 exhibited complete photoluminescence quenching, enhanced metallicity, stabilized photogenerated electrons via SiW9, enabling use photocatalysts. efficiently catalyzed the functionalization terminal aryl alkyne N-bromosuccinimide (NBS), achieving tribromoketones yield 94%, significantly outperforming AuSCs lower or higher metallicity (38 65%, respectively). Mechanistic studies revealed that improved promotes transfer complex formation NBS, while SiW9 stabilizes electrons, enhancing density under light irradiation. strong visible-light absorption, photostability, solvent dispersibility, recyclability up five cycles scalability broader applications. This strategy positions viable photocatalyst, expanding its potential photocatalysis toward synthesizing molecules.

Язык: Английский

Процитировано

0