Phosphotungstic Acid Intercalated MgAlLa Ternary Layered Double Hydroxides as High-Efficiency Additives for Epoxy Resin: Synergistic Enhancement of Flame Retardancy and Smoke Suppression DOI Open Access
Wensheng Zhao, Jiao Jin,

Zhaoxu Guang

и другие.

Coatings, Год журнала: 2025, Номер 15(5), С. 523 - 523

Опубликована: Апрель 27, 2025

The inherent flammability and toxic smoke emission of epoxy resins (EPs) pose significant challenges to their advanced engineering applications. To address this limitation, we developed a novel flame-retardant additive through the organic modification layered double hydroxides (LDHs) using ternary MgAlLa hydrotalcite structure intercalated with phosphotungstic acid (PWA). This innovative design established synergistic mechanism by combining catalytic carbonization effect lanthanum radical scavenging capability PWA. optimized MgAlLa-PWA/EP composite demonstrated remarkable flame retardancy suppression improvements, exhibiting 77.9% 62.4% reductions in peak heat release rate (pHRR) total (THR), respectively, compared pure EP. Particularly noteworthy was 72.6% decrease (TSR), accompanied elevation limiting oxygen index (LOI) value 26.8% achievement UL-94 V-0 rating. Microstructural analysis revealed that modified formed continuous uniform layer increased density during combustion, effectively inhibiting exchange, diffusion, transfer. study provides strategy for designing multi-element LDHs high-efficiency

Язык: Английский

Constructing a gradient modulus interfacial layer on the surface of hydrotalcite enhances the interfacial properties of hydrotalcite/benzoxazine composites DOI Creative Commons
Lu Zhang, Liwu Zu, Shaobo Dong

и другие.

Polymer Composites, Год журнала: 2025, Номер unknown

Опубликована: Фев. 24, 2025

Abstract The gradient modulus interface layer between hydrotalcite (LDH) and benzoxazine (Bz) polymer matrix was designed by grafting silane coupling agent KH560. effect of varying proportions LDH on the mechanical properties poly(LDH/Bz) analyzed. When content at 6 wt%, poly(KH560‐LDH/Bz) exhibited enhancements 78.31%, 68.58%, 117.91% in tensile strength, flexural impact respectively, compared to poly(LDH/Bz). This improvement is attributed interfacial phase KH560, which enhances surface roughness polarity LDH, effectively buffering equilibrating disparity matrix. tension functionalized calculated using Harmonic Mean formula. Upon incorporation energy difference reduced, thereby enhancing compatibility two materials. thickness investigated atomic force microscopy (AFM), confirmed presence a graded within poly(KH560‐LDH/Bz). Highlights poly(KH560‐LDH/BZ) were improved most when addition KH560‐LDH wt%. has low free energy, conducive dispersion composite with wt% showed excellent thermal thermomechanical properties. increased 41.27%. promotes stress transfer

Язык: Английский

Процитировано

0

Transformation of magnesium hydroxide whiskers into high-performance multifunctional flame retardant synergists by interfacial engineering modulation DOI

Kangsi Zhou,

Yandong Hu,

K. X. Zhao

и другие.

Construction and Building Materials, Год журнала: 2025, Номер 473, С. 141009 - 141009

Опубликована: Апрель 1, 2025

Язык: Английский

Процитировано

0

Tannic acid-mediated assembly of ultrafine Fe(OH)3 on the surface of phytic acid intercalated LDH to reduce fire hazard and improve mechanical properties of epoxy resin DOI
Jiachen Zhu, Lijuan Li,

Lianmin Ji

и другие.

Construction and Building Materials, Год журнала: 2025, Номер 476, С. 141210 - 141210

Опубликована: Апрель 14, 2025

Язык: Английский

Процитировано

0

Poly(Butanediol Sebacate‐Butanediol Terephthalate) (PBSeT)/Zinc Gluconate (ZG) Nanocomposite Films: A Comprehensive Investigation of Mechanical, Thermal, Rheological, and Degradation Properties DOI
Jia Mi, Yingchun Li, Wensheng Wang

и другие.

Journal of Applied Polymer Science, Год журнала: 2025, Номер unknown

Опубликована: Апрель 21, 2025

ABSTRACT Poly(butanediol sebacate‐butanediol terephthalate) (PBSeT) has emerged as a promising biodegradable material, attributed to its excellent tensile strength and water vapor barrier properties. However, certain challenges persist, including susceptibility puncture tearing. To solve these problems, the researchers developed composite material consisting of PBSeT zinc gluconate (ZG) improve performance through synergistic effect ionic hydrogen bonds. Notably, tearing PBSeT/ZG‐3 exhibits remarkable increase 48.7% relative alone, while load is enhanced by 25.3%. Furthermore, XRD TG analyses indicate that incorporation ZG negligible impact on crystallinity thermal stability composites. Interestingly, enzymatic degradation properties are significantly improved with increasing content, hydrophilicity imparted results in reduction contact angle materials. In conclusion, integration enhances resistance, tear strength, biodegradability PBSeT. These advancements critical for development implementation novel applications, particularly fields food packaging, films, medical

Язык: Английский

Процитировано

0

Phosphotungstic Acid Intercalated MgAlLa Ternary Layered Double Hydroxides as High-Efficiency Additives for Epoxy Resin: Synergistic Enhancement of Flame Retardancy and Smoke Suppression DOI Open Access
Wensheng Zhao, Jiao Jin,

Zhaoxu Guang

и другие.

Coatings, Год журнала: 2025, Номер 15(5), С. 523 - 523

Опубликована: Апрель 27, 2025

The inherent flammability and toxic smoke emission of epoxy resins (EPs) pose significant challenges to their advanced engineering applications. To address this limitation, we developed a novel flame-retardant additive through the organic modification layered double hydroxides (LDHs) using ternary MgAlLa hydrotalcite structure intercalated with phosphotungstic acid (PWA). This innovative design established synergistic mechanism by combining catalytic carbonization effect lanthanum radical scavenging capability PWA. optimized MgAlLa-PWA/EP composite demonstrated remarkable flame retardancy suppression improvements, exhibiting 77.9% 62.4% reductions in peak heat release rate (pHRR) total (THR), respectively, compared pure EP. Particularly noteworthy was 72.6% decrease (TSR), accompanied elevation limiting oxygen index (LOI) value 26.8% achievement UL-94 V-0 rating. Microstructural analysis revealed that modified formed continuous uniform layer increased density during combustion, effectively inhibiting exchange, diffusion, transfer. study provides strategy for designing multi-element LDHs high-efficiency

Язык: Английский

Процитировано

0