A
straightforward
and
effective
chromatographic
method
has
been
created
for
the
analysis
of
progesterone
from
human
plasma
using
a
composite
based
on
polypyrrole/magnetic
nanoparticles
in
sample
preparation
procedure.
The
quantification
is
necessary
due
to
its
importance
development
fertility.
employed
conditions
used
acetonitrile:ultrapure
water
(70:30,
v/v)
as
mobile
phase
at
1.0
mL
min
Journal of Materials Chemistry B,
Год журнала:
2025,
Номер
unknown
Опубликована: Янв. 1, 2025
This
review
provides
a
comprehensive
analysis
on
the
applications
of
various
MOFs
in
both
microbial
eradication
and
protection,
emphasizing
their
potential
as
promising
smart
materials
field
ecosystem
regulation.
Analytical Letters,
Год журнала:
2024,
Номер
unknown, С. 1 - 41
Опубликована: Май 5, 2024
In
this
review,
the
principles
and
characteristics
of
solid-phase
extraction
(SPE)
are
discussed.
The
categories
nanomaterial-based
adsorbents
namely
metal/metal
oxides,
magnetic
nanoparticles,
silica-based
two-dimensional
(2D)
nanomaterials
(NMs),
polymeric
nanotubes,
semiconductor
NMs,
nanoporous
materials
along
with
their
features
discussed
followed
by
evaluating
synthetic
strategies.
Finally,
application
sorbents
for
preconcentration
drugs,
pesticides,
heavy
metals
in
biological,
food,
environmental
samples
is
assessed.
Overall,
future
SPE
techniques
expected
to
include
advances
downsizing,
automation,
selectivity,
sustainability,
integration
other
analytical
techniques,
resulting
more
efficient
effective
sample
preparation
procedures
a
variety
applications.
Separations,
Год журнала:
2025,
Номер
12(1), С. 11 - 11
Опубликована: Янв. 8, 2025
Miniaturized
solid-based
approaches
have
added
an
eco-friendly
dimension
to
analytical
procedures,
establishing
themselves
as
promising
strategies
for
a
wide
range
of
applications.
Among
these,
microextraction
by
packed
sorbent
(MEPS)
stands
out
due
its
ability
facilitate
efficient
sample
interaction
with
densely
sorb
ent
phase
within
the
system.
MEPS
offers
several
advantages,
including
preconcentration
capabilities
and
use
minimal
solvent
volumes,
making
it
appealing
choice
modern
workflows.
Since
extraction
efficiency
is
largely
dictated
phase,
recent
advancements
in
design
garnered
considerable
attention
field
preparation.
Innovations
phases
not
only
enhanced
but
also
enabled
development
semi-
fully
automated
systems,
paving
way
high-throughput
methodologies.
These
elevated
beyond
traditional
offline
miniaturized
preparation
methods,
offering
new
opportunities
streamlined
scalable
analyses.
Therefore,
this
study
provides
comprehensive
overview
novel
used
MEPS,
particular
focus
on
both
bio-based
synthetic
materials.
Furthermore,
explores
aspects
highlighting
current
trends,
technological
advancements,
future
directions
rapidly
evolving
field.
Journal of Applied Polymer Science,
Год журнала:
2025,
Номер
unknown
Опубликована: Март 18, 2025
ABSTRACT
A
novel
analytical
methodology
was
developed
in
this
study
for
the
determination
of
four
nonsteroidal
anti‐inflammatory
drugs,
including
aspirin,
naproxen,
ibuprofen,
and
mefenamic
acid
water
samples
using
high‐performance
liquid
chromatography‐diode
array
detection.
The
thin
film
solid‐phase
microextraction
technique
employed,
coupled
with
a
96‐well
plate
sampling
system,
polyaniline‐silica
doped
hydrochloric
used
as
extractor
phase.
optimized
conditions
were
obtained
through
univariate
multivariate
approaches,
optimum
extraction
1.5
mL
sample,
pH
3,
without
salt
addition,
300
μL
acetonitrile.
Calibration
curves
spiked
ultrapure
water;
linear
ranges
from
15
to
500
μg
L
−1
,
coefficients
higher
than
0.9957.
Detection
quantification
limits
4.55
respectively.
relative
recoveries
varied
81%
117%
river
sample
at
three
different
concentration
levels
each
analyte.
intraday
(
n
=
3)
interday
9)
precision
values
≤
8%
15%,