Process Intensification and Reaction Kinetics for Synthesis of 5‐Hydroxymethyl Furfural Using DICAT‐1 Solid Acid Catalyst in a Batch Reactor DOI
Ayush Vasishta, Hitesh S. Pawar

ChemistrySelect, Год журнала: 2024, Номер 9(41)

Опубликована: Окт. 28, 2024

Abstract 5‐HMF is a potential platform multifaceted molecule for various industrial applications and can be produced from biomass‐based hexose sugars. In the present study, indigenously prepared catalyst DIC A T‐1 (an acronym derived DBT‐ICT Center Energy Biosciences Catalyst #1) has been explored fructose dehydration, using isopropyl alcohol (IPA) as green low boiling point (LBP) organic solvent. The exploration of heterogeneous adds specific advantages synthesis in terms high yield, conversion, selectivity, separation, recycle, reuse, so forth. Different variants T‐1, such T‐1A, T‐1B, T‐1C, T‐1D, having variable surface acidity were tested dehydration presence IPA. Of variants, T‐1C provides good yield selectivity 5‐HMF. Thus, further process optimization study was conducted to obtain maximum T‐1C. intensified 78% with 83% conversion 94% selectivity. recyclability showed consistency five consecutive recycle runs. reaction kinetics first‐order an activation energy 13.16 kJ/mole by catalyst. use easily recyclable robust efficient route production

Язык: Английский

Biomass-derived magnetic amorphous carbon as an efficient catalyst in the conversion of fructose into 5-hydroxymethylfurfural DOI
Tuan Minh Dang, Trinh Hao Nguyen, Ha-Thanh Nguyen

и другие.

Dalton Transactions, Год журнала: 2025, Номер unknown

Опубликована: Янв. 1, 2025

We developed a magnetic solid acid derived from rice husk as an efficient catalyst for 5-HMF production. The was easily recovered using external magnet without significant loss in the catalytic activity.

Язык: Английский

Процитировано

0

Recent advances in selective 2,5-diformylfuran production from renewable biomass: Novel catalytic strategies and sustainable approaches DOI
Trinh Hao Nguyen,

Mai Ngoc Thi Le,

Dao Anh Le Nguyen

и другие.

Renewable and Sustainable Energy Reviews, Год журнала: 2025, Номер 215, С. 115599 - 115599

Опубликована: Март 13, 2025

Язык: Английский

Процитировано

0

Bifunctional Chromium-Doped Phenolic Porous Hydrothermal Carbon Catalysts for the Catalytic Conversion of Glucose to 5-Hydroxymethylfurfural DOI Open Access
Pengfeng Xiao,

Wei Mao,

Zhiming Wu

и другие.

International Journal of Molecular Sciences, Год журнала: 2025, Номер 26(8), С. 3648 - 3648

Опубликована: Апрель 12, 2025

A sustainable and efficient approach for converting carbohydrates into 5-hydroxymethylfurfural (HMF) via heterogeneous catalysis is crucial effectively utilizing biomass. In this study, we synthesized a series of CrX-polyphenol-formaldehyde resin (PTF) catalysts, which are composites Cr-doped phenolic-resin-based hydrothermal carbon, using chelation-assisted multicomponent co-assembly strategy. The performance the catalysts was assessed through various analytical techniques, including scanning electron microscopy, transmission thermogravimetric analysis, X-ray photoelectron spectroscopy, pyrolysis–Fourier transform infrared Brunauer–Emmett–Teller analysis. Cr incorporation enhanced total Lewis acidities. Notably, optimized catalyst, designated as Cr0.6-PTF, achieved an effective glucose conversion HMF, yielding maximum 69.5% at 180 °C min in saturated NaCl solution (NaClaq)/dimethyl sulfoxide (2: 18) solvent system. Furthermore, Cr0.6-PTF maintained excellent catalytic activity stable chemical structure after nine cyclic reactions, resulting 63.8% HMF yield from glucose. This study revealed innovative metal-doped phenolic carbon to platform chemicals.

Язык: Английский

Процитировано

0

Boron-doped sulfonated graphitic carbon nitride as a highly efficient catalyst for the production of 5-hydroxymethylfurfural from carbohydrates DOI Creative Commons

Diep Dinh Le,

Trinh Hao Nguyen,

Luc Tan Nguyen

и другие.

Heliyon, Год журнала: 2024, Номер 10(18), С. e37812 - e37812

Опубликована: Сен. 1, 2024

Язык: Английский

Процитировано

0

A sustainable one-pot synthesis of 2,5-diformylfuran from carbohydrates using tetracationic ionic liquid DOI
Trinh Hao Nguyen, Thien Phuoc Nguyen, Ha Bich Phan

и другие.

Journal of Molecular Liquids, Год журнала: 2024, Номер unknown, С. 126032 - 126032

Опубликована: Сен. 1, 2024

Язык: Английский

Процитировано

0

Process Intensification and Reaction Kinetics for Synthesis of 5‐Hydroxymethyl Furfural Using DICAT‐1 Solid Acid Catalyst in a Batch Reactor DOI
Ayush Vasishta, Hitesh S. Pawar

ChemistrySelect, Год журнала: 2024, Номер 9(41)

Опубликована: Окт. 28, 2024

Abstract 5‐HMF is a potential platform multifaceted molecule for various industrial applications and can be produced from biomass‐based hexose sugars. In the present study, indigenously prepared catalyst DIC A T‐1 (an acronym derived DBT‐ICT Center Energy Biosciences Catalyst #1) has been explored fructose dehydration, using isopropyl alcohol (IPA) as green low boiling point (LBP) organic solvent. The exploration of heterogeneous adds specific advantages synthesis in terms high yield, conversion, selectivity, separation, recycle, reuse, so forth. Different variants T‐1, such T‐1A, T‐1B, T‐1C, T‐1D, having variable surface acidity were tested dehydration presence IPA. Of variants, T‐1C provides good yield selectivity 5‐HMF. Thus, further process optimization study was conducted to obtain maximum T‐1C. intensified 78% with 83% conversion 94% selectivity. recyclability showed consistency five consecutive recycle runs. reaction kinetics first‐order an activation energy 13.16 kJ/mole by catalyst. use easily recyclable robust efficient route production

Язык: Английский

Процитировано

0