Fluorescent “On‐off‐on” Probe for Cascade Detection of Ag(I) and Ascorbic Acid Using Folic Acid Protected Copper Nanoclusters DOI Open Access

Yagnik Vegad,

Lata Rana, Bigyan Ranjan Jali

и другие.

ChemNanoMat, Год журнала: 2024, Номер unknown

Опубликована: Окт. 18, 2024

Abstract Folic acid (FA) protected copper nanoclusters (FA‐CuNCs, λ ex =350 nm, em =445 nm) were synthesized and used as a fluorescent “on‐off‐on” probe for the cascade detection of Ag + ascorbic (AA). The fluorescence emission FA‐CuNCs at 445 nm was quenched significantly by due to analyte‐induced aggregation followed formation larger nanoparticles. However, when AA added in‐situ generated Ag@FA‐CuNCs, recovered because AA‐directed reduction 0 . experimental conditions, such pH, incubation time, quencher concentrations, optimized achieve improved sensitivity. limit estimated 37.1 nM 0.27 μM with linearity range 2.49–22 4.71–81.53 μM, respectively. In real sample analysis, recoveries ions in river water orange juice samples found between 99–93 % 97–94 using probes Overall, this work offers viable method sequential via switch mechanism.

Язык: Английский

Development of a Carbon Paste Electrode Modified with Saffron-Conjugated Silver Nanoparticles for the Simultaneous Determination of Cd, Pb, Zn, Cu and Cl in Soils and Plants DOI Creative Commons
Stella Girousi,

Vasiliki Keramari,

Ioanna Paraschi

и другие.

Chemosensors, Год журнала: 2025, Номер 13(3), С. 91 - 91

Опубликована: Март 5, 2025

A simple and easily applicable analytical method for the simultaneous determination of Cd2+, Pb2+, Zn2+, Cu2+, Cl− by applying a modified carbon paste electrode with saffron-conjugated silver nanoparticles (AgNPs@Sa) is being presented. The CPE was then used Cu2+ as well chloride ions in soil plants. comparative analysis demonstrated significant enhancement applicability through incorporation (AgNPs) at (CPE) surface, leading to development poly-Sa-CPE. This newly proposed offers notably superior qualitative performance compared other metal nanoparticle-based modifications reported literature. accordingly successfully applied ion. novel sensor that makes possible heavy metals chlorides same solution, plant samples. enhanced sensitivity selectivity poly-Sa-CPE system highlights its potential more effective alternative analysis, further demonstrating advantages electrochemical applications. LODs their are 0.38 μg·L−1, 0.44 0.72 0.42 0.11 respectively, comparably high relative standard deviations about 8.1%, 9.4%, 8.3%, 7.6%, 7.9%, respectively.

Язык: Английский

Процитировано

0

Theoretical Insights into the Impact of the Central Atom on the Photoluminescence Mechanisms of Ligand-Protected Cu Nanoclusters DOI

Yuting Luo,

Pu Wang, Yong Pei

и другие.

The Journal of Physical Chemistry Letters, Год журнала: 2025, Номер unknown, С. 3705 - 3714

Опубликована: Апрель 4, 2025

Ligand-protected copper nanoclusters (CuNCs) have attracted considerable attention in both fundamental research and practical applications due to their easy availability, environmental friendliness, exceptional optical properties. In this study, density functional theory (DFT) time-dependent (TD-DFT) calculations were employed investigate the photoluminescence (PL) mechanism of two-electron (2e) cluster [Au@Cu14(SCH2CH3)12(P(CH2CH3)3)6]+ (Au@Cu14) zero-electron (0e) [Cl@Cu14(SCH2CH3)12(P(CH2CH3)3)6]+ (Cl@Cu14) explore impact central atom on PL mechanisms CuNCs. The accuracy various exchange-correlation (XC) functionals used for fluorescence phosphorescence energy was evaluated. BP86 PBE0 calculate radiative nonradiative transition processes two clusters. Theoretical showed that enhanced spin-orbit coupling, larger dipole moments, more significant orbital overlap, smaller Huang-Rhys factors reorganization energies main reasons higher quantum yield (PLQY) Au@Cu14 than Cl@Cu14. These findings provide important insights into effect CuNCs valuable guidance design optimization applications.

Язык: Английский

Процитировано

0

A review of metal nanomaterials-based electrochemical biosensors for environmental wastewater monitoring and their remediation DOI

PratimaDevi Sivasubramanian,

Mohanraj Kumar,

Ching‐Lung Chen

и другие.

Environmental Nanotechnology Monitoring & Management, Год журнала: 2024, Номер unknown, С. 101023 - 101023

Опубликована: Ноя. 1, 2024

Язык: Английский

Процитировано

3

Red-emitting copper nanoclusters for ultrasensitive and selective detection of creatinine and its application in portable smartphone-based paper strips and polymer thin film DOI

Thangarasu Sasikumar,

Krishnamoorthy Shanmugaraj, Karuppasamy Nandhini

и другие.

Surfaces and Interfaces, Год журнала: 2024, Номер 53, С. 105014 - 105014

Опубликована: Авг. 26, 2024

Язык: Английский

Процитировано

1

Glycerate-assisted CoMn-sulfide with microsphere architecture confined by nanoparticles as an efficient enzyme-free sensor for amperometric measurement of glucose in serum, saliva and beverage samples DOI

Zahra Hajesfandyari,

Leila Naderi,

Saeed Shahrokhian

и другие.

Food Chemistry, Год журнала: 2024, Номер 467, С. 142175 - 142175

Опубликована: Ноя. 20, 2024

Язык: Английский

Процитировано

1

Fluorescent “On‐off‐on” Probe for Cascade Detection of Ag(I) and Ascorbic Acid Using Folic Acid Protected Copper Nanoclusters DOI Open Access

Yagnik Vegad,

Lata Rana, Bigyan Ranjan Jali

и другие.

ChemNanoMat, Год журнала: 2024, Номер unknown

Опубликована: Окт. 18, 2024

Abstract Folic acid (FA) protected copper nanoclusters (FA‐CuNCs, λ ex =350 nm, em =445 nm) were synthesized and used as a fluorescent “on‐off‐on” probe for the cascade detection of Ag + ascorbic (AA). The fluorescence emission FA‐CuNCs at 445 nm was quenched significantly by due to analyte‐induced aggregation followed formation larger nanoparticles. However, when AA added in‐situ generated Ag@FA‐CuNCs, recovered because AA‐directed reduction 0 . experimental conditions, such pH, incubation time, quencher concentrations, optimized achieve improved sensitivity. limit estimated 37.1 nM 0.27 μM with linearity range 2.49–22 4.71–81.53 μM, respectively. In real sample analysis, recoveries ions in river water orange juice samples found between 99–93 % 97–94 using probes Overall, this work offers viable method sequential via switch mechanism.

Язык: Английский

Процитировано

0