Antioxidants,
Год журнала:
2023,
Номер
12(6), С. 1298 - 1298
Опубликована: Июнь 18, 2023
While
various
methods
exist
for
synthesizing
silver
nanoparticles
(AgNPs),
green
synthesis
has
emerged
as
a
promising
approach
due
to
its
affordability,
sustainability,
and
suitability
biomedical
purposes.
However,
is
time-consuming,
necessitating
the
development
of
efficient
cost-effective
techniques
minimize
reaction
time.
Consequently,
researchers
have
turned
their
attention
photo-driven
processes.
In
this
study,
we
present
photoinduced
bioreduction
nitrate
(AgNO3)
AgNPs
using
an
aqueous
extract
Ulva
lactuca,
edible
seaweed.
The
phytochemicals
found
in
seaweed
functioned
both
reducing
capping
agents,
while
light
served
catalyst
biosynthesis.
We
explored
effects
different
intensities
wavelengths,
initial
pH
mixture,
exposure
time
on
biosynthesis
AgNPs.
Confirmation
AgNP
formation
was
achieved
through
observation
surface
plasmon
resonance
band
at
428
nm
ultraviolet-visible
(UV-vis)
spectrophotometer.
Fourier
transform
infrared
spectroscopy
(FTIR)
revealed
presence
algae-derived
bound
outer
synthesized
Additionally,
high-resolution
transmission
electron
microscopy
(HRTEM)
atomic
force
(AFM)
images
demonstrated
that
NPs
possessed
nearly
spherical
shape,
ranging
size
from
5
40
nm.
crystalline
nature
confirmed
by
selected
area
diffraction
(SAED)
X-ray
(XRD),
with
Bragg's
pattern
revealing
peaks
2θ
=
38°,
44°,
64°,
77°,
corresponding
planes
111,
200,
220,
311
face-centered
cubic
crystal
lattice
metallic
silver.
Energy-dispersive
(EDX)
results
exhibited
prominent
peak
3
keV,
indicating
Ag
elemental
configuration.
highly
negative
zeta
potential
values
provided
further
confirmation
stability
Moreover,
reduction
kinetics
observed
via
UV-vis
spectrophotometry
superior
photocatalytic
activity
degradation
hazardous
pollutant
dyes,
such
rhodamine
B,
methylene
orange,
Congo
red,
acridine
Coomassie
brilliant
blue
G-250.
our
biosynthesized
hold
great
redox
applications.
Nanomaterials,
Год журнала:
2022,
Номер
12(22), С. 3992 - 3992
Опубликована: Ноя. 12, 2022
Photocatalytic
degradation
has
been
suggested
to
be
a
cheap
and
efficient
way
dispose
of
organic
pollutants,
such
as
dyes.
Therefore,
our
research
team
strives
produce
nanophotocatalysts
in
simple
inexpensive
way.
In
this
work,
the
Pechini
sol-gel
technique
was
employed
for
facile
synthesis
Mn0.5Zn0.5Fe2O4/Fe2O3
Fe0.5Mn0.5Co2O4/Fe2O3
mixed
metal
oxide
nanoparticles
photocatalytic
Rhodamine
B
Congo
Red
XRD,
FT-IR,
N2
adsorption/desorption
analyzer,
EDS,
FE-SEM,
an
UV-Vis
diffuse
reflectance
spectrophotometer
were
used
characterize
produced
samples.
The
XRD
patterns
revealed
that
average
crystallite
size
samples
is
90.25
80.62
nm,
respectively.
FE-SEM
images
sample
consists
cubic
irregular
shapes
with
diameter
1.71
µm.
Additionally,
spherical
0.26
energy
gaps
are
3.50
4.3
eV
3.52
4.20
eV,
presence
hydrogen
peroxide,
complete
100
mL
20
mg/L
dyes
occurred
at
pH
=
8
3,
respectively,
within
50
min,
using
0.1
g
synthesized
Water Science and Engineering,
Год журнала:
2023,
Номер
16(3), С. 261 - 270
Опубликована: Март 16, 2023
Malachite
green
(MG)
dye
is
a
common
industrial
and
organic
contaminant
that
can
be
found
in
(waste)water.
Textile
food
industries
make
use
of
MG
as
dyeing
coloring
agents,
respectively.
However,
both
genotoxic
mutagenic.
Hence,
the
elimination
from
MG-laden-wastewater
germane.
This
review
summarizes
up-to-date
researches
have
been
reported
literature
regards
decontamination
toxic
wastewater.
Various
removal
methods
(adsorption,
membrane,
Fenton
system,
heterogenous
homogeneous
photodegradation)
were
discussed.
Of
two
basic
technologies
are
comprehensively
explored
reviewed,
chemical
treatment
not
viable
physical
methods,
such
adsorption
technology,
due
to
lack
secondary
pollutant
production,
simple
design,
low
operation
costs,
resource
availability.
also
presents
various
practical
knowledge
gaps
needed
for
large-scale
applications
adsorptive
MG.
It
concludes
by
recommending
further
research
on
techniques
cheap
get
clean
water.
Antioxidants,
Год журнала:
2023,
Номер
12(6), С. 1298 - 1298
Опубликована: Июнь 18, 2023
While
various
methods
exist
for
synthesizing
silver
nanoparticles
(AgNPs),
green
synthesis
has
emerged
as
a
promising
approach
due
to
its
affordability,
sustainability,
and
suitability
biomedical
purposes.
However,
is
time-consuming,
necessitating
the
development
of
efficient
cost-effective
techniques
minimize
reaction
time.
Consequently,
researchers
have
turned
their
attention
photo-driven
processes.
In
this
study,
we
present
photoinduced
bioreduction
nitrate
(AgNO3)
AgNPs
using
an
aqueous
extract
Ulva
lactuca,
edible
seaweed.
The
phytochemicals
found
in
seaweed
functioned
both
reducing
capping
agents,
while
light
served
catalyst
biosynthesis.
We
explored
effects
different
intensities
wavelengths,
initial
pH
mixture,
exposure
time
on
biosynthesis
AgNPs.
Confirmation
AgNP
formation
was
achieved
through
observation
surface
plasmon
resonance
band
at
428
nm
ultraviolet-visible
(UV-vis)
spectrophotometer.
Fourier
transform
infrared
spectroscopy
(FTIR)
revealed
presence
algae-derived
bound
outer
synthesized
Additionally,
high-resolution
transmission
electron
microscopy
(HRTEM)
atomic
force
(AFM)
images
demonstrated
that
NPs
possessed
nearly
spherical
shape,
ranging
size
from
5
40
nm.
crystalline
nature
confirmed
by
selected
area
diffraction
(SAED)
X-ray
(XRD),
with
Bragg's
pattern
revealing
peaks
2θ
=
38°,
44°,
64°,
77°,
corresponding
planes
111,
200,
220,
311
face-centered
cubic
crystal
lattice
metallic
silver.
Energy-dispersive
(EDX)
results
exhibited
prominent
peak
3
keV,
indicating
Ag
elemental
configuration.
highly
negative
zeta
potential
values
provided
further
confirmation
stability
Moreover,
reduction
kinetics
observed
via
UV-vis
spectrophotometry
superior
photocatalytic
activity
degradation
hazardous
pollutant
dyes,
such
rhodamine
B,
methylene
orange,
Congo
red,
acridine
Coomassie
brilliant
blue
G-250.
our
biosynthesized
hold
great
redox
applications.