Efficient Synthesis and Characterization of Antibacterial Xanthan Gum–Based Self‐Healing Hydrogels: Conventional Versus Microwave Treated DOI

Homa Etemadi Moghaddam,

Mahsa Baghban Salehi

Polymers for Advanced Technologies, Год журнала: 2024, Номер 35(12)

Опубликована: Дек. 1, 2024

ABSTRACT The development of self‐healing hydrogels with mechanical integrity is vital for biomedical applications. This study synthesizes multi‐network (MN) using xanthan gum (XG) through conventional and microwave‐assisted methods via free‐radical polymerization. synthesis materials included XG, acrylamide, acrylonitrile, sodium dodecyl sulfate, ferric chloride hexahydrate, ammonium persulfate. Conventional took 60 min at 70°C, while microwave was completed in 4.5 540 W, enhancing energy material efficiency. Structural tests like FTIR SEM confirmed the results. Microwave produced a layered structure smaller pores, leading to slower swelling kinetics, EDX mapping showed higher Fe 3+ ion concentrations, indicating better crosslinking. Thermal gravimetric analysis demonstrated that degradation onset temperatures were 184°C XG hydrogel (MHXG) 163°C water bath method (HXG), 20°C enhancement due coherent induced by treatment. Evaluation capabilities visual rheological significant enhancements MHXG, which exhibited time 2 h compared 1 day required HXG, attributed increased crosslink density hydrogen bonding facilitated Rheological assessments both types maintained their structural viscoelastic properties after healing. MHXG strength 21.12 kPa elasticity 10 kPa, whereas HXG 11.59 respectively. Microwave‐treated enhanced antibacterial effectiveness against Staphylococcus aureus distribution agents matrix. synthesizing XG‐based promising advanced

Язык: Английский

Cellulose-based 3D printing bio-inks for biomedical applications: A review DOI Creative Commons
Chhavi Sharma, Muhammad Asim Raza,

Shiv Dutt Purohit

и другие.

International Journal of Biological Macromolecules, Год журнала: 2025, Номер 305, С. 141174 - 141174

Опубликована: Фев. 20, 2025

Cellulose is the most ubiquitous polymer found in nature. In recent years, cellulose derivatives of various kinds, such as esters and ethers, nanocelluloses, have become popular bioprintable materials used for making bio-inks because their affordability, biocompatibility, biodegradability, printability. Nevertheless, potential uses nanocellulose derivative-based not been thoroughly explored. This review emphasizes advancements design cellulose-based 3D bioprinting diverse tissues well physicochemical attributes that make them a viable choice bioprinting. Additionally, bio-inks' current benefits drawbacks printing are examined. Various cross-linking approaches offered multicomponent nanocellulose-based to control fidelity ink alter mechanical stiffness printed hydrogel construct bioactive cue. By emphasizing interactions involving cells matrix, it additionally examines effect functional groups surface charge on vital cellular functions (including cell survival, adhesion, proliferation). Thus, this aims offer an integrated platform with biomedical industry.

Язык: Английский

Процитировано

1

Development of Mn3O4 nanoparticles and Justicia adhatoda extract incorporated Carboxymethyl cellulose/Carbopol hydrogels: Rheological and in vitro bioactivity for sustained drug delivery system DOI
Karolinekersin Enoch, Anbumozhi Angayarkanni Somasundaram

International Journal of Biological Macromolecules, Год журнала: 2025, Номер unknown, С. 141713 - 141713

Опубликована: Март 1, 2025

Язык: Английский

Процитировано

0

Cellulose nanocrystals reinforcement for glycerol-based gels: Effects on gelation behavior and thermal insulation performance DOI
Paulo César França da Câmara, Stéphanie Cavalcante de Morais, Nívia do Nascimento Marques

и другие.

Journal of Molecular Liquids, Год журнала: 2025, Номер unknown, С. 127562 - 127562

Опубликована: Апрель 1, 2025

Язык: Английский

Процитировано

0

Capsaicin nanocrystals burdened topical polymeric gel: An encouraging tactic for alleviation of paclitaxel-induced peripheral neuropathy DOI

Sagar Hade,

Pawan Devangan, Gopal Bajad

и другие.

International Journal of Pharmaceutics, Год журнала: 2024, Номер 669, С. 125082 - 125082

Опубликована: Дек. 12, 2024

Язык: Английский

Процитировано

1

Efficient Synthesis and Characterization of Antibacterial Xanthan Gum–Based Self‐Healing Hydrogels: Conventional Versus Microwave Treated DOI

Homa Etemadi Moghaddam,

Mahsa Baghban Salehi

Polymers for Advanced Technologies, Год журнала: 2024, Номер 35(12)

Опубликована: Дек. 1, 2024

ABSTRACT The development of self‐healing hydrogels with mechanical integrity is vital for biomedical applications. This study synthesizes multi‐network (MN) using xanthan gum (XG) through conventional and microwave‐assisted methods via free‐radical polymerization. synthesis materials included XG, acrylamide, acrylonitrile, sodium dodecyl sulfate, ferric chloride hexahydrate, ammonium persulfate. Conventional took 60 min at 70°C, while microwave was completed in 4.5 540 W, enhancing energy material efficiency. Structural tests like FTIR SEM confirmed the results. Microwave produced a layered structure smaller pores, leading to slower swelling kinetics, EDX mapping showed higher Fe 3+ ion concentrations, indicating better crosslinking. Thermal gravimetric analysis demonstrated that degradation onset temperatures were 184°C XG hydrogel (MHXG) 163°C water bath method (HXG), 20°C enhancement due coherent induced by treatment. Evaluation capabilities visual rheological significant enhancements MHXG, which exhibited time 2 h compared 1 day required HXG, attributed increased crosslink density hydrogen bonding facilitated Rheological assessments both types maintained their structural viscoelastic properties after healing. MHXG strength 21.12 kPa elasticity 10 kPa, whereas HXG 11.59 respectively. Microwave‐treated enhanced antibacterial effectiveness against Staphylococcus aureus distribution agents matrix. synthesizing XG‐based promising advanced

Язык: Английский

Процитировано

1