Preparation and application of novel sorbents for in-tube solid-phase microextraction

TrAC Trends in Analytical Chemistry, Год журнала: 2024, Номер 181, С. 118047 - 118047

Опубликована: Ноя. 8, 2024

Язык: Английский

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Polystyrene grafted hollow layered double hydroxides (NiCo-LDH@PS) as solid phase microextraction coating for enhanced capture of polycyclic aromatic hydrocarbons

Journal of environmental chemical engineering, Год журнала: 2023, Номер 11(6), С. 111317 - 111317

Опубликована: Окт. 26, 2023

Язык: Английский

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Sustainable hybrid sorbent based on a thin film gelatin coating over cellulose paper for the determination of steroid hormones in urine and environmental water samples

Microchemical Journal, Год журнала: 2025, Номер unknown, С. 112769 - 112769

Опубликована: Янв. 1, 2025

Язык: Английский

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Detection of trace estrogens in environmental water by multi-template molecularly imprinted polymers based magnetic solid phase extraction coupled solidified floating organic drop microextraction and HPLC

Microchemical Journal, Год журнала: 2025, Номер 213, С. 113875 - 113875

Опубликована: Май 6, 2025

Язык: Английский

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A robust multi-residue method for the monitoring of 25 endocrine disruptors at ultra-trace levels in surface waters by SPE-LC-MS/MS

Analytical Methods, Год журнала: 2023, Номер 15(21), С. 2606 - 2621

Опубликована: Янв. 1, 2023

Analysis of surface water samples with solid phase extraction and tandem mass spectrometry dansyl chloride derivatization enables the environmental monitoring 25 endocrine disruptors at ultra-trace levels.

Язык: Английский

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Exploring advanced strategies in SPME-HPLC-DAD: Enhancing analytical precision and diverse applications in modern era

Journal of Liquid Chromatography &amp Related Technologies, Год журнала: 2024, Номер 47(6-10), С. 181 - 200

Опубликована: Май 7, 2024

In analytical chemistry, the synergy between innovative sample preparation techniques and advanced chromatographic methods has paved way for unprecedented advancements in analysis of complex samples. Solid Phase Microextraction (SPME) stands out as a powerful tool extraction, preconcentration. When coupled with High-Performance Liquid Chromatography (HPLC) equipped Diode Array Detector (DAD), integrated SPME-HPLC-DAD system emerges sophisticated platform, offering enhanced sensitivity, selectivity, versatility various applications. Desorption is accomplished by either depositing organic solvent desorption chamber or else flowing mobile phase through specificity. An ordinary description, along visual illustration, been thoroughly provided concepts developed well-known thin film SPME cartridges (Figure 2). The tabular representation also available proper description like technique name, targeted analyte, column used, %RSD, extraction recovery, LOD, data acquired R2 considered Based on information present study. Discussed HPLC-DAD brings great turning point successfully utilization biomedical sciences, environmental monitors, food safety, clinical This cost-effective, readily both environmentally friendly stable, allowing rapid, reliable, accurate measurements across wide range analyte concentrations, thanks to hyphenated techniques. different strategies HPLC -DAD possible future apllications have incorporated review. understanding these still limited challenging.

Язык: Английский

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Packed in-tube solid-phase microextraction with mesoporous zirconium titanium oxides for highly efficient phosphopeptide enrichment and analysis

Microchemical Journal, Год журнала: 2023, Номер 195, С. 109423 - 109423

Опубликована: Сен. 23, 2023

Язык: Английский

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Novel ferrofluid based on hydrophobic deep eutectic solvents for separation and analysis of trace estrogens in environmental water and urine samples

Analytical and Bioanalytical Chemistry, Год журнала: 2024, Номер 416(18), С. 4057 - 4070

Опубликована: Июнь 6, 2024

Язык: Английский

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Ionic liquid-functionalized covalent organic frameworks on the surface of silica for online solid-phase extraction

Journal of Chromatography A, Год журнала: 2024, Номер 1732, С. 465200 - 465200

Опубликована: Июль 20, 2024

Язык: Английский

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Dispersive solid‐phase extraction of risperidone from plasma samples using graphene oxide aerogels and determination with liquid chromatography

Journal of Separation Science, Год журнала: 2023, Номер 46(14)

Опубликована: Май 14, 2023

A graphene oxide-based aerogel was synthesized and applied to the extraction determinations with high-performance liquid chromatography-ultraviolet detector. After characterization of produced graphene-aerogel, it utilized as a dispersive solid-phase sorbent for risperidone from plasma samples. Aerogels are materials large surface area-to-mass ratio plenty core functional groups which can easily attach analytes extract them second phase. The suggested method determined in samples wide dynamic range 20 ng/ml 3 μg/ml. limits detection quantification developed were calculated 2.4 8.2 ng/ml, respectively. As novel feature, has no need precipitate proteins, improving analytical performance analysis. Also, first time, obtained results revealed that approach could be employed an accurate real

Язык: Английский

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