Preparation of hollow mesoporous silica/polyimide composite films and study of their properties DOI
Xin Li,

Qi‐wen Ma,

Guang‐ning Yu

и другие.

Polymer Composites, Год журнала: 2025, Номер unknown

Опубликована: Апрель 18, 2025

Abstract Constructing high‐performance polyimide (PI) films with low dielectric constant, excellent mechanical properties, hydrophobicity, and thermal stability is of great significance, but remains a challenge. Herein, five PI (labeled as P1, P2, P3, P4, P5, respectively) were successfully synthesized by conventional two‐step method using 1,4‐bis(4‐amino‐2‐trifluoromethylphenoxy)benzene the sole diamine monomer pyromellitic dianhydride, 2,3,6,7‐Naphthalenetetracarboxylic 2,3:6,7‐Dianhydride, 3,3′,4,4′‐biphenyltetracarboxylic o‐4,4′‐oxydiphthalic anhydride, 3,3′,4,4′‐benzophenonetetracarboxylic dianhydride monomers, respectively. Particularly, hollow mesoporous silica (HMSMs)/PI film comprehensive properties was introducing HMSMs into P4 based on polymerization strategy. The results showed that doping contributed to reducing improving maintaining in comparison film. When content 1.5 wt.%, decomposition temperature, tensile strength, water contact angle, constant HMSMs/PI composite measured at 489°C, 162 MPa, 86.45°, 2.40, This study presents new approach for preparing advanced films. Highlights High‐performance synthesized. Doping enhances overall performance A lower (2.40) achieved.

Язык: Английский

Molecular structure influence of porous intrinsic polyimide nanofiber for high temperature flue gas filtration: Bisphenol AF, sulfone, ether bonds and hydroxyl groups DOI Creative Commons
Xinming Wang, Yongqi Wang,

Anning Sun

и другие.

Materials Today Advances, Год журнала: 2025, Номер 25, С. 100564 - 100564

Опубликована: Фев. 4, 2025

Язык: Английский

Процитировано

0

Low-CTE, Strong-Adhesion, and High-Resolution Photosensitive Polyimide Materials for Advanced Packaging Applications: Structure and Properties DOI

Huifa Meng,

Kaijin Chen,

Chuying Li

и другие.

ACS Applied Polymer Materials, Год журнала: 2025, Номер unknown

Опубликована: Март 17, 2025

The use of traditional photosensitive polyimide (PSPI) insulating materials, which possess high coefficients thermal expansion (CTE) and poor adhesion to copper, easily causes failure issues in the redistribution layers (RDLs). However, there are some trade-offs design low-CTE PSPI materials such as ultraviolet (UV) transmittance precursors dielectric properties films. To overcome above challenges, an AB2-type fluorinated monoamine (ETFPh-NH2) with a nonplanar steric structure was designed synthesized, then used end-capper attached poly(amic ester) (PAE) linear/stiff structure. solutions were developed by using as-prepared PAE resins, solvents, other additives. Despite presence ETFPh-NH2 relatively low molar ratio total precursor chains, transparency PAE-4 notably enhanced, resulting achievement high-resolution lithographic pattern. Meanwhile, PI-4 film exhibited characteristics (23.65 ppm K–1), its mechanical enhanced microbranched cross-link structure, constructed reaction arylethynyl groups during imidization process. Furthermore, between PI films Cu significantly improved introducing aromatic silane (TMS). In short, PI-4, high-dimensional stability, strong Cu, photopatternable capabilities, could be feasible reliable material for advanced packaging. addition, end-groups modification strategy seems effective way greatly improve overall performance materials.

Язык: Английский

Процитировано

0

Functional Groups‐Regulated Organic Semiconductors for Efficient Artificial Photosynthesis of Hydrogen Peroxide DOI Open Access
Xiaohui Yu, Zhen Wei, Yuan Qin

и другие.

Advanced Materials, Год журнала: 2025, Номер unknown

Опубликована: Март 18, 2025

Abstract Hydrogen peroxide (H 2 O ) is an environmentally friendly reagent, and organic semiconductors (OSCs) are ideal photocatalysts for the synthesis of H due to their well‐defined molecular structure, strong donor‐acceptor interactions, efficient charge separation. This review discusses regulatory mechanisms functional group modifications in tuning photocatalytic performance OSCs, highlighting relationship between structure catalytic performance. For example, electron‐regulating groups, such as cyano halogen, induce dipoles, facilitating migration photogenerated electrons. Fluorine groups optimize band prolong carrier lifetime high electronegativity. π‐Conjugated extension like anthraquinone thiophene, expand conjugation, improve visible light capture, stabilize intermediates through redox cycles. Hydroxyl enhance surface hydrophilicity promote activation, while imine bond protonation adjusts distribution improves selectivity cycle stability. Multi‐active site sulfonic acid amide, accelerate reaction kinetics inhibit decomposition. Functional absorption, separation, reactions electronic regulation, intermediate adsorption optimization, proton‐electron transfer. Future work should integrate machine learning identify optimal combinations develop green functionalization strategies photocatalyst synthesis.

Язык: Английский

Процитировано

0

Reveling the Structural, Electric, and High-Frequency Dielectric Properties of Residue Doped-CaWO4 Flexible Multilayer Ceramic Sheets DOI Creative Commons
Nívia Luciana Costa de Siqueira, Hugo P.A. Alves, Paulo Henrique Chibério

и другие.

Materials Research, Год журнала: 2025, Номер 28

Опубликована: Янв. 1, 2025

The mineralization process to reach Tungsten (W) involves several steps reduce the impurities (residues), which makes more expensive. However, it is possible explore pure scheelite (CaWO4) and residue doped-CaWO4 on flexible sheets using Tape Casting technique. In particular, high frequency dielectric properties of multilayers have an increased appeal in electronics industry. this study, we present a systematic investigation structural, morphological, electrical high-frequency ceramics sheet composed CaWO4 residue-doped CaWO4. Our findings demonstrate that constant has small dependence amount, but remarkable modification as number layers increases. Here achieved 34% increase for ceramic when from 1 3.

Язык: Английский

Процитировано

0

Fluorine-Free Thermoplastic High-Frequency Low Dielectric Poly(ether imide)s for Flexible Copper Clad Laminates DOI
Bo Deng, Kaijin Chen,

Runxin Bei

и другие.

ACS Applied Polymer Materials, Год журнала: 2025, Номер unknown

Опубликована: Март 25, 2025

To meet the requirements of high-frequency signal transmission in 5G or 6G applications, development high-performance functional polyimide possessing a low dielectric constant (Dk) and loss (Df) at high frequencies, along with melting processing capabilities good adhesion to copper foil, is both urgent highly challenging. In this work, three diamines containing tert-butyl moieties ether bonds but different substitution positions amine groups were designed synthesized, poly(ether imide)s (PEIs; TBPI, TTBPI, ATBPI, PTBPI) obtained from their polycondensation 4,4′-(4,4′-isopropylidenediphenoxy) diphthalic anhydride (BPADA). The introduction flexible such as bond bisphenol A structure has potential improve flexibility molecular chains reduce density imide ring, polarity, glass transition temperature PEIs. incorporation unique spatial nonpolar side group may help increase free volume exceptional hydrophobicity Both give as-prepared fluorine-free PEIs range beneficial characteristics, property, excellent solubility, water absorption (0.42, 0.35, 0.50% P/P0 = 0.50 (50% relatively humidity (RH)), respectively), Dk (2.83, 2.84, 2.82 10 GHz 50% RH), Df (0.00339, 0.00257, 0.00366 peel strength foil via hot-pressing molding. successful enables preparation truly adhesive-free clad laminates (FCCLs) This significantly simplifies process FCCLs enhances reliability electronic circuits, thereby presenting attractive application prospects for mobile communication.

Язык: Английский

Процитировано

0

High Performance Polyimide Films with Low Dk and Low Df at 10 GHz via Cross-Linking of Bulky Pendant Groups DOI
Shiying Qi, Shuo Han, Jianhao He

и другие.

ACS Applied Polymer Materials, Год журнала: 2025, Номер unknown

Опубликована: Март 28, 2025

Язык: Английский

Процитировано

0

Preparation of hollow mesoporous silica/polyimide composite films and study of their properties DOI
Xin Li,

Qi‐wen Ma,

Guang‐ning Yu

и другие.

Polymer Composites, Год журнала: 2025, Номер unknown

Опубликована: Апрель 18, 2025

Abstract Constructing high‐performance polyimide (PI) films with low dielectric constant, excellent mechanical properties, hydrophobicity, and thermal stability is of great significance, but remains a challenge. Herein, five PI (labeled as P1, P2, P3, P4, P5, respectively) were successfully synthesized by conventional two‐step method using 1,4‐bis(4‐amino‐2‐trifluoromethylphenoxy)benzene the sole diamine monomer pyromellitic dianhydride, 2,3,6,7‐Naphthalenetetracarboxylic 2,3:6,7‐Dianhydride, 3,3′,4,4′‐biphenyltetracarboxylic o‐4,4′‐oxydiphthalic anhydride, 3,3′,4,4′‐benzophenonetetracarboxylic dianhydride monomers, respectively. Particularly, hollow mesoporous silica (HMSMs)/PI film comprehensive properties was introducing HMSMs into P4 based on polymerization strategy. The results showed that doping contributed to reducing improving maintaining in comparison film. When content 1.5 wt.%, decomposition temperature, tensile strength, water contact angle, constant HMSMs/PI composite measured at 489°C, 162 MPa, 86.45°, 2.40, This study presents new approach for preparing advanced films. Highlights High‐performance synthesized. Doping enhances overall performance A lower (2.40) achieved.

Язык: Английский

Процитировано

0