Selective molecular characterization of organic aerosols using in situ laser desorption ionization mass spectrometry DOI

Daohe Yuan,

Yulin Qi, Chao Ma

и другие.

Rapid Communications in Mass Spectrometry, Год журнала: 2024, Номер 38(16)

Опубликована: Июнь 18, 2024

Rationale The sources and chemical compositions of organic aerosol (OA) exert a significant influence on both regional global atmospheric conditions, thereby having far‐reaching implications environmental chemistry. However, existing mass spectrometry (MS) methods have limitations in characterizing the detailed composition OA due to selective ionization as well fractionation during cold‐water extraction solid‐phase (SPE). Methods A comprehensive MS study was conducted using samples collected dusty, clean, polluted days. To supplement data obtained from electrospray (ESI), strategy for analyzing OAs quartz fiber filter directly utilizing laser desorption (LDI) employed. Additionally, ESI method explore suitable approaches determining various Results In situ LDI has advantages significantly reducing sample volume, simplifying preparation, overcoming problem overestimating sulfur‐containing compounds usually encountered ESI. It is characterization highly unsaturated hydrophobic aerosols, such brown carbon‐type with low volatility high stability, which supplementary Conclusions Compared other methods, helps provide complementary description molecular OAs, especially day samples. This may contribute more analysis elusive atmosphere.

Язык: Английский

Multistage Linear Frequency Scanning Mass Analysis Processed by Fractional Fourier Transform DOI
Haoqiang Yan, Lei Hu,

Shi Zhang

и другие.

Journal of the American Society for Mass Spectrometry, Год журнала: 2025, Номер unknown

Опубликована: Апрель 1, 2025

The common method of mass analysis in a linear ion trap spectrometer is to eject ions with different mass-to-charge ratios (m/z) at times by resonance excitation. Ions are ejected onto an electron multiplier (EM), generating pulsed signals called the ejection signal. Typically, signal consisting multiple pulses smoothed into wider Gaussian-like pulse due limited bandwidth electronic system. For scan rates and samples, this bandwidth-limited system smoothing process will differentially increase peak width thus decrease resolution. In study, experiments were performed on "Brick" miniature spectrometer. We propose multistage frequency scanning mode that achieves improved resolution extended range, which fractional Fourier transform applied signals. proposed processing improves mitigates impact ghost peaks attributed scattered ejection. A 0.84 Da m/z value 242 rate 8000 Da/s was achieved experiments.

Язык: Английский

Процитировано

0

A pilot-scale study on performance and deactivation mechanism of MnOx supported on Y zeolite for ozone catalytic oxidation of VOCs at low temperature DOI
Qi Shao,

Haoran Xiao,

Lei Gao

и другие.

Process Safety and Environmental Protection, Год журнала: 2025, Номер unknown

Опубликована: Май 1, 2025

Язык: Английский

Процитировано

0

Theoretical Studies of Molecular Reactions at the Air–Water Interface: Recent Progress and Perspective DOI
Jing Kang,

Shixuan Wang,

Chenruyuan Li

и другие.

Wiley Interdisciplinary Reviews Computational Molecular Science, Год журнала: 2025, Номер 15(3)

Опубликована: Май 1, 2025

ABSTRACT Water microdroplets have been shown to possess unique properties. For instance, compared bulk water, can accelerate chemical reactions by several orders of magnitude and trigger that cannot occur in water. These phenomena generated significant interest various fields like atmospheric science, green synthesis, materials preparation. properties are associated with at the air–water interface; however, underlying mechanisms remain unclear. Studying microscopic details interface remains a substantial experimental challenge. Meanwhile, molecular dynamics (MD) simulations related computational methods provide powerful tools for studying interface. This review aims summarize processes from perspective theoretical simulations. First, we discuss physical Subsequently, systematically introduce simulation strategies four categories interfacial reactions: (a) near‐barrierless reactions, (b) some energy barriers, (c) employing high‐level quantum methods, (d) photochemical reactions. Finally, focus on simulating thermal interface, particular emphasis chemistry. The discussed involve Criegee intermediates, nitrogen‐containing compounds, chlorine‐containing while include H 2 O phenol. results here enable an improved understanding as well processes.

Язык: Английский

Процитировано

0

Insights into the formation of secondary organic aerosols from agricultural residue burning emissions: A review of chamber-based studies DOI
Swati Joshi, Neeraj Rastogi, Atinderpal Singh

и другие.

The Science of The Total Environment, Год журнала: 2024, Номер 952, С. 175932 - 175932

Опубликована: Авг. 31, 2024

Язык: Английский

Процитировано

2

A Review of Gastrodia Elata Bl. : Extraction, Analysis and Application of Functional Food DOI

C. Li,

Jieqing Li, Yuanzhong Wang

и другие.

Critical Reviews in Analytical Chemistry, Год журнала: 2024, Номер unknown, С. 1 - 30

Опубликована: Сен. 27, 2024

Bl. still widely known as a medicinal plant due to its anti-inflammatory, neuroprotection, cardiovascular protection etc. Additionally, these medical applications cannot be separated from antioxidant, anti-aging, regulating cell apoptosis ability, which make it have potential functional food well has been eaten for more than 2,000 years in China. At present, although

Язык: Английский

Процитировано

1

Atomic spectrometry update – a review of advances in environmental analysis DOI
Warren R. L. Cairns, Owen T. Butler, Olga Cavoura

и другие.

Journal of Analytical Atomic Spectrometry, Год журнала: 2024, Номер unknown

Опубликована: Дек. 11, 2024

This review covers advances in the analysis of air, water, plants, soils and geological materials by a range atomic spectrometric techniques, including emission, absorption, fluorescence mass spectrometry.

Язык: Английский

Процитировано

1

Selective molecular characterization of organic aerosols using in situ laser desorption ionization mass spectrometry DOI

Daohe Yuan,

Yulin Qi, Chao Ma

и другие.

Rapid Communications in Mass Spectrometry, Год журнала: 2024, Номер 38(16)

Опубликована: Июнь 18, 2024

Rationale The sources and chemical compositions of organic aerosol (OA) exert a significant influence on both regional global atmospheric conditions, thereby having far‐reaching implications environmental chemistry. However, existing mass spectrometry (MS) methods have limitations in characterizing the detailed composition OA due to selective ionization as well fractionation during cold‐water extraction solid‐phase (SPE). Methods A comprehensive MS study was conducted using samples collected dusty, clean, polluted days. To supplement data obtained from electrospray (ESI), strategy for analyzing OAs quartz fiber filter directly utilizing laser desorption (LDI) employed. Additionally, ESI method explore suitable approaches determining various Results In situ LDI has advantages significantly reducing sample volume, simplifying preparation, overcoming problem overestimating sulfur‐containing compounds usually encountered ESI. It is characterization highly unsaturated hydrophobic aerosols, such brown carbon‐type with low volatility high stability, which supplementary Conclusions Compared other methods, helps provide complementary description molecular OAs, especially day samples. This may contribute more analysis elusive atmosphere.

Язык: Английский

Процитировано

0