Cobalt-Catalyzed Borylative Reduction of Azobenzenes to Hydrazobenzenes via a Diborylated-Hydrazine Intermediate DOI

Wenli Wang,

Yuli Wang, Yiying Yang

и другие.

The Journal of Organic Chemistry, Год журнала: 2024, Номер 89(13), С. 9265 - 9274

Опубликована: Июнь 20, 2024

Cobalt-catalyzed borylative reduction of azobenzenes using pinacolborane is developed. The simple cobalt chloride catalyst and reaction conditions make this protocol attractive for hydrazobenzene synthesis. This shows good functional group compatibility can be readily scaled up to the gram scale. Preliminary mechanistic studies clarified proton source hydrazine products. cobalt-catalyzed azobenzene provides a practical prepare synthetically useful diborylated hydrazines.

Язык: Английский

Iron(I) and Iron(II) Boxmi Pincer Complexes: Coordination Chemistry and Catalytic Hydroboration of Nitriles DOI

David Bürgy,

Clemens K. Blasius,

Tim Bruckhoff

и другие.

Organometallics, Год журнала: 2025, Номер unknown

Опубликована: Июнь 4, 2025

Язык: Английский

Процитировано

0

Au Nanoparticle-Catalyzed Double Hydrosilylation of Nitriles by Diethylsilane DOI Creative Commons

Maria Ioanna Karapanou,

Dimitra Malliotaki,

Manolis Stratakis

и другие.

Organic & Biomolecular Chemistry, Год журнала: 2024, Номер 22(26), С. 5346 - 5352

Опубликована: Янв. 1, 2024

We present the first example of Au-catalyzed reduction nitriles into primary amines. In contrast to monohydrosilanes which are completely unreactive, diethylsilane (a dihydrosilane) is capable reducing aryl or alkyl amines under catalysis by Au nanoparticles supported on TiO

Язык: Английский

Процитировано

1

Cobalt-Catalyzed Borylative Reduction of Azobenzenes to Hydrazobenzenes via a Diborylated-Hydrazine Intermediate DOI

Wenli Wang,

Yuli Wang, Yiying Yang

и другие.

The Journal of Organic Chemistry, Год журнала: 2024, Номер 89(13), С. 9265 - 9274

Опубликована: Июнь 20, 2024

Cobalt-catalyzed borylative reduction of azobenzenes using pinacolborane is developed. The simple cobalt chloride catalyst and reaction conditions make this protocol attractive for hydrazobenzene synthesis. This shows good functional group compatibility can be readily scaled up to the gram scale. Preliminary mechanistic studies clarified proton source hydrazine products. cobalt-catalyzed azobenzene provides a practical prepare synthetically useful diborylated hydrazines.

Язык: Английский

Процитировано

1