Chemical Communications,
Год журнала:
2023,
Номер
59(23), С. 3439 - 3442
Опубликована: Янв. 1, 2023
The
solventless
synthesis
of
an
amide
was
performed
in
a
twin-screw
extruder
the
presence
coupling
agent,
providing
high
yielding
and
productive
method.
reaction
conditions
were
optimized
to
prepare
APIs,
teriflunomide
moclobemide.
Chemical Society Reviews,
Год журнала:
2021,
Номер
50(14), С. 8279 - 8318
Опубликована: Янв. 1, 2021
For
inorganic
metathesis
and
reduction
reactivity,
mechanochemistry
is
demonstrating
great
promise
towards
both
nanoparticles
organometallics
syntheses.
ACS Sustainable Chemistry & Engineering,
Год журнала:
2022,
Номер
10(16), С. 5110 - 5116
Опубликована: Март 10, 2022
As
the
demand
increases
for
more
sustainable
chemical
production,
mechanochemical
processes
have
been
proposed
as
greener
alternatives
to
traditional
manufacturing
methods.
To
support
transition
processes,
quantitative
assessment
methods
must
be
developed
measure
and
compare
greenness
of
processes.
MilliporeSigma's
DOZN
2.0
Green
Chemistry
Evaluator
was
utilized
quantify
adherence
12
Principles
synthesis
Active
Pharmaceutical
Ingredient
(API)
nitrofurantoin
in
batch
continuous
Through
this
analysis,
SPEX
mill
twin-screw
extrusion
(TSE)
were
shown
compared
a
commercial
solution-based
process.
This
conclusion
result
scores
which
demonstrated
TSE
having
increased
energy
efficiency,
improved
resources
use,
reduced
human
environmental
hazards
other
Green Chemistry,
Год журнала:
2023,
Номер
25(16), С. 6120 - 6148
Опубликована: Янв. 1, 2023
This
article
presents
a
review
of
the
reports
on
catalyst-free
mechanochemical
organic
transformations
and
ability
to
initiate
reactions
that
are
extremely
difficult/impossible
occur
is
notable
advancement
process.
Chemical Communications,
Год журнала:
2023,
Номер
59(23), С. 3439 - 3442
Опубликована: Янв. 1, 2023
The
solventless
synthesis
of
an
amide
was
performed
in
a
twin-screw
extruder
the
presence
coupling
agent,
providing
high
yielding
and
productive
method.
reaction
conditions
were
optimized
to
prepare
APIs,
teriflunomide
moclobemide.