Molybdenum‐Catalyzed Direct Synthesis of Pyrroles from Nitroarenes with Glycols as Reductants DOI Creative Commons
Sara Gómez‐Gil, Samuel Suárez‐Pantiga, M.R. Pedrosa

и другие.

Advanced Synthesis & Catalysis, Год журнала: 2024, Номер unknown

Опубликована: Окт. 21, 2024

Abstract A molybdenum‐catalyzed synthesis of N ‐(hetero)aryl pyrroles directly from inexpensive and commonly available (hetero)nitroarenes via reduction with pinacol annulation 1,4‐dicarbonyls or cyclobutane‐1,2‐diols has been described. The process does not require an inert atmosphere tolerates the presence air water. This non‐noble catalytic system shows high chemoselectivity, allowing a diverse range potentially reducible functional groups such as alkynes, alkenes, halogens, cyano, carbonyls. Moreover, this strategy enables reuse waste byproduct reactant, facilitating formation challenging accessible used reducing agents.

Язык: Английский

Radical p‐Doping Spiro‐OMeTAD for Efficient, Stable and Self‐Healing Flexible Perovskite Solar Cells DOI
Zhengchi Yang, Wei Jin, Yu Liu

и другие.

Advanced Materials, Год журнала: 2025, Номер unknown

Опубликована: Апрель 22, 2025

Abstract Spiro‐OMeTAD is the primary hole transport material (HTM) for high‐efficiency and stable flexible perovskite solar cells (FPSCs). However, slow oxidation rate susceptibility to film cracking under stress in lead reduced device stability efficiency. In this paper, a multi‐functional novel self‐healing nitroxide radical monomer, 4‐[[5‐(1,2‐dithiolane‐3‐yl)‐1‐oxopentyl]amino]‐2,2,6,6‐tetramethylpiperidin‐1‐oxyl (DT‐TEMPO), has been introduced address these challenges. DT‐TEMPO, on one side, enhances mobility conductivity by p‐doping Spiro‐OMeTAD, while boosting charge transfer process from with an optimized energy level alignment other side. Additionally, DT‐TEMPO endows capability through introduction of dynamic breaking reconstructing disulfide bond. The achieve impressive power conversion efficiencies, 25.69% rigid substrates (certified 25.30%), 21.23% mini‐modules, 24.19% substrates. Remarkably, FPSCs retain over 90% their initial efficiency even after 20 000 bending cycles ( r = 6 mm) recover ≈95% value process.

Язык: Английский

Процитировано

0

Oxygen-Vacancy-Engineered Cu/Cu2O/CuO@C nanocomposites from Copper–Furan 2, 5-Dicarboxylic acid Metal-Organic Framework: Unlocking catalytic Mastery in nitroarene hydrogenation DOI
Hao Wu, Yanyan Yu, Yinghe He

и другие.

Separation and Purification Technology, Год журнала: 2025, Номер unknown, С. 133233 - 133233

Опубликована: Апрель 1, 2025

Язык: Английский

Процитировано

0

A Green, Cheap and Robust Method for Selective Hydrogenation of Nitroarenes DOI

Piao Ding,

Eman Fayad,

Ola A. Abu Ali

и другие.

Tetrahedron, Год журнала: 2024, Номер unknown, С. 134269 - 134269

Опубликована: Сен. 1, 2024

Язык: Английский

Процитировано

3

Molybdenum‐Catalyzed Direct Synthesis of Pyrroles from Nitroarenes with Glycols as Reductants DOI Creative Commons
Sara Gómez‐Gil, Samuel Suárez‐Pantiga, M.R. Pedrosa

и другие.

Advanced Synthesis & Catalysis, Год журнала: 2024, Номер unknown

Опубликована: Окт. 21, 2024

Abstract A molybdenum‐catalyzed synthesis of N ‐(hetero)aryl pyrroles directly from inexpensive and commonly available (hetero)nitroarenes via reduction with pinacol annulation 1,4‐dicarbonyls or cyclobutane‐1,2‐diols has been described. The process does not require an inert atmosphere tolerates the presence air water. This non‐noble catalytic system shows high chemoselectivity, allowing a diverse range potentially reducible functional groups such as alkynes, alkenes, halogens, cyano, carbonyls. Moreover, this strategy enables reuse waste byproduct reactant, facilitating formation challenging accessible used reducing agents.

Язык: Английский

Процитировано

1