Disulfide-Directed Multicyclic Peptides with N-Terminally Extendable α-Helices for Recognition and Activation of G Protein-Coupled Receptors DOI
Shihui Fan, Jie Li, Jie Zhuang

и другие.

Journal of the American Chemical Society, Год журнала: 2024, Номер unknown

Опубликована: Дек. 17, 2024

Many peptide hormones adopt long α-helical structures upon interacting with their cognate receptors but often exhibit flexible conformations when unbound. Strategies that can stabilize α-helices without disrupting binding to are still lacking, which hinders progress in biological applications and drug development. Here, we present an approach combines rational design library screening create identify a unique disulfide-directed multicyclic (DDMP) scaffold, could effectively N-terminally extendable while displaying exceptional efficiency disulfide pairing oxidative folding. This DDMP scaffold was then utilized for stabilizing the structure of glucagon-like peptide-1 (GLP-1), resulting potent GLP-1 receptor (GLP-1R) agonist significantly improved α-helicity proteolytic stability. By incorporating external into preserve native N-terminal allowing extensive evolution C-terminal disulfide-rich domain enhancing target binding, as demonstrated by generation DDMP-stabilized (g1:Ox). The cryo-electron microscopy g1:Ox-GLP-1R complex heterotrimeric G

Язык: Английский

Development of Selective Nanomolar Cyclic Peptide Ligands as GBA1 Enzyme Stabilizers DOI Creative Commons
Rebecca E. Katzy, Renier H. P. van Neer, Maria J. Ferraz

и другие.

RSC Chemical Biology, Год журнала: 2025, Номер unknown

Опубликована: Янв. 1, 2025

The stabilisation of recombinant glycosidases by exogenous ligands, known as pharmacological chaperones or enzyme stabilisers, has recently garnered great clinical interest. This strategy can prevent degradation in the blood, reducing required dosages and extending IV injection intervals, thereby side effects, improving patient lifestyles treatment costs. While this therapeutic approach been successfully implemented for treating Pompe Fabry diseases, studies Gaucher disease using alone combination with replacement therapy (ERT) have limited, no small molecule yet approved condition. Developing such therapies requires selective effective reversible GBA1 ligands. Here, we describe development a new class macrocyclic peptide ligands random nonstandard peptides integrated discovery (RaPID) technology, demonstrate their ability to bind stabilise rhGBA1 plasma at nanomolar concentrations. These cyclic do not inhibit endogenous cells due poor cell permeability but extracellular plasma, presenting significant potential combinatorial ERT-pharmacological chaperone disease.

Язык: Английский

Процитировано

0

RaPID discovery of cell-permeable helical peptide inhibitors con-taining cyclic β-amino acids against SARS-CoV-2 main protease DOI Creative Commons

Marina Kawai,

Tika R. Malla, H. T. Henry Chan

и другие.

RSC Chemical Biology, Год журнала: 2025, Номер unknown

Опубликована: Янв. 1, 2025

The ribosomal synthesis of a helical peptide library containing structurally constrained cyclic β-amino acid at every third position and its application for the RaPID selection against SARS-CoV-2 main protease (M pro ) inhibitors.

Язык: Английский

Процитировано

0

Translation of Deoxyribonucleic Acid into Synthetic Alpha Helical Peptides for Darwinian Evolution DOI Creative Commons
Millicent Dockerill, Pramod M. Sabale, Francesco Russo

и другие.

JACS Au, Год журнала: 2024, Номер 4(10), С. 4013 - 4022

Опубликована: Окт. 2, 2024

DNA-encoded libraries connect the phenotypes of synthetic molecules to a DNA barcode; however, most do not tap into potential Darwinian evolution. Herein, we report DNA-templated synthesis (DTS) architecture make peptides that are stabilized α-helical conformations via head-to-tail supramolecular cyclization. Using pilot library targeting MDM2, show repeated screening can amplify binder from lowest abundance in ranking correlates binding affinity. The study also highlights need design such chemistry avoids biases heterogeneous yield DTS.

Язык: Английский

Процитировано

1

Disulfide-Directed Multicyclic Peptides with N-Terminally Extendable α-Helices for Recognition and Activation of G Protein-Coupled Receptors DOI
Shihui Fan, Jie Li, Jie Zhuang

и другие.

Journal of the American Chemical Society, Год журнала: 2024, Номер unknown

Опубликована: Дек. 17, 2024

Many peptide hormones adopt long α-helical structures upon interacting with their cognate receptors but often exhibit flexible conformations when unbound. Strategies that can stabilize α-helices without disrupting binding to are still lacking, which hinders progress in biological applications and drug development. Here, we present an approach combines rational design library screening create identify a unique disulfide-directed multicyclic (DDMP) scaffold, could effectively N-terminally extendable while displaying exceptional efficiency disulfide pairing oxidative folding. This DDMP scaffold was then utilized for stabilizing the structure of glucagon-like peptide-1 (GLP-1), resulting potent GLP-1 receptor (GLP-1R) agonist significantly improved α-helicity proteolytic stability. By incorporating external into preserve native N-terminal allowing extensive evolution C-terminal disulfide-rich domain enhancing target binding, as demonstrated by generation DDMP-stabilized (g1:Ox). The cryo-electron microscopy g1:Ox-GLP-1R complex heterotrimeric G

Язык: Английский

Процитировано

1