Exploring Excited‐State Intramolecular Proton‐Coupled Electron Transfer in Dinuclear Ir(III)‐Complex via Covalently Tagged Hydroquinone: Phototherapy Through Futile Redox Cycling DOI Creative Commons
Maniklal Shee,

Julia Schleisiek,

Nishith Maity

и другие.

Small, Год журнала: 2024, Номер unknown

Опубликована: Дек. 23, 2024

Anticipating intramolecular excited-state proton-coupled electron transfer (PCET) process within dinuclear Ir2-photocatalytic system via the covalent linkage is seminal, yet challenging. Indeed, development of various complexes also promising for studying integral photophysics and facilitating applications in catalysis or biology. Herein, this study reports [Ir2(bis{imidazo-phenanthrolin-2-yl}-hydroquinone)(ppy)4]2+ (12+) complex by leveraging both ligand-centered redox property H-bonding exploring dual proton-transfer assisted PCET process. The vital role covalently placed hydroquinone bridged ligand investigated as electron-proton (ET-PT) mediator validated from triplet spin density plot. Moreover, bimolecular photoinduced ET reaction studied acetonitrile/water medium, forging lowest energy charge separated (3CSPhen-Im) state 12+ with methyl viologen favorably concerted-PCET pathway. result indicates strong donor-acceptors coupling, which limits recombination enhances catalytic efficiency. To showcase potential application, bioinspired PCET-based photocatalytic platform phototherapeutics, indicating significant mitochondrial localization leading to programmed cell death (apoptosis) through futile cycling. consequences effective internalization (via energy-dependent endocytosis), better safety profile, higher antiproliferative activity compared Cisplatin, explored 3D tumor spheroids, anticipates it be a lead compound.

Язык: Английский

White light increases anticancer effectiveness of iridium(III) complexes toward lung cancer A549 cells DOI

Gechang Li,

Jing Chen, Yufeng Xie

и другие.

Journal of Inorganic Biochemistry, Год журнала: 2024, Номер 259, С. 112652 - 112652

Опубликована: Июнь 26, 2024

Язык: Английский

Процитировано

4

Advances in the Design of Photoactivatable Metallodrugs: Excited State Metallomics DOI Creative Commons
Huayun Shi, Rafael C. Marchi, Peter J. Sadler

и другие.

Angewandte Chemie International Edition, Год журнала: 2025, Номер unknown

Опубликована: Янв. 13, 2025

Abstract Photoactivatable metal complexes offer the prospect of novel drugs with low side effects and new mechanisms action to combat resistance current therapy. We highlight recent progress in design platinum, ruthenium, iridium, gold other transition complexes, especially for applications as anticancer anti‐infective agents. In particular, understanding excited state chemistry related identification bioactive species (excited metallomics/pharmacophores) is important. metallodrugs are classified here photocatalysts, photorelease agents ligand‐activated Their activation wavelengths, cellular action, experimental theoretical metallomics states photoproducts discussed explore strategies investigation photoactivatable metallodrugs. These have potential clinical Photodynamic Therapy (PDT), Photoactivated Chemotherapy (PACT) Photothermal (PTT).

Язык: Английский

Процитировано

0

Advances in the Design of Photoactivatable Metallodrugs: Excited State Metallomics DOI Creative Commons
Huayun Shi, Rafael C. Marchi, Peter J. Sadler

и другие.

Angewandte Chemie, Год журнала: 2025, Номер unknown

Опубликована: Янв. 13, 2025

Abstract Photoactivatable metal complexes offer the prospect of novel drugs with low side effects and new mechanisms action to combat resistance current therapy. We highlight recent progress in design platinum, ruthenium, iridium, gold other transition complexes, especially for applications as anticancer anti‐infective agents. In particular, understanding excited state chemistry related identification bioactive species (excited metallomics/pharmacophores) is important. metallodrugs are classified here photocatalysts, photorelease agents ligand‐activated Their activation wavelengths, cellular action, experimental theoretical metallomics states photoproducts discussed explore strategies investigation photoactivatable metallodrugs. These have potential clinical Photodynamic Therapy (PDT), Photoactivated Chemotherapy (PACT) Photothermal (PTT).

Язык: Английский

Процитировано

0

Exploring Excited‐State Intramolecular Proton‐Coupled Electron Transfer in Dinuclear Ir(III)‐Complex via Covalently Tagged Hydroquinone: Phototherapy Through Futile Redox Cycling DOI Creative Commons
Maniklal Shee,

Julia Schleisiek,

Nishith Maity

и другие.

Small, Год журнала: 2024, Номер unknown

Опубликована: Дек. 23, 2024

Anticipating intramolecular excited-state proton-coupled electron transfer (PCET) process within dinuclear Ir2-photocatalytic system via the covalent linkage is seminal, yet challenging. Indeed, development of various complexes also promising for studying integral photophysics and facilitating applications in catalysis or biology. Herein, this study reports [Ir2(bis{imidazo-phenanthrolin-2-yl}-hydroquinone)(ppy)4]2+ (12+) complex by leveraging both ligand-centered redox property H-bonding exploring dual proton-transfer assisted PCET process. The vital role covalently placed hydroquinone bridged ligand investigated as electron-proton (ET-PT) mediator validated from triplet spin density plot. Moreover, bimolecular photoinduced ET reaction studied acetonitrile/water medium, forging lowest energy charge separated (3CSPhen-Im) state 12+ with methyl viologen favorably concerted-PCET pathway. result indicates strong donor-acceptors coupling, which limits recombination enhances catalytic efficiency. To showcase potential application, bioinspired PCET-based photocatalytic platform phototherapeutics, indicating significant mitochondrial localization leading to programmed cell death (apoptosis) through futile cycling. consequences effective internalization (via energy-dependent endocytosis), better safety profile, higher antiproliferative activity compared Cisplatin, explored 3D tumor spheroids, anticipates it be a lead compound.

Язык: Английский

Процитировано

2