Unlocking the Potential of Redox‐Active Copper Complexes in Thin Films via Proton‐Coupled Electron Transfer for Enhanced Supercapacitor Performance DOI
Ritu Gupta, Ankur Malik, Pradeep Sachan

и другие.

Advanced Functional Materials, Год журнала: 2024, Номер unknown

Опубликована: Дек. 4, 2024

Abstract Nanoscale redox‐active molecular films are promising candidates for next‐generation energy storage applications due to their ability facilitate long‐range charge transport. However, establishing stable and efficient electrode‐molecule interfaces remains a critical challenge. In this study, the properties of copper‐polypyridyl thin covalently bonded graphite rods explored, investigating potential as supercapacitors. Using an electrochemical grafting method, robust covalent created, resulting in prepared on indium tin oxide (ITO) electrodes, exhibiting both Cu(II) Cu(I) redox states. These mettalo‐oligomeric demonstrate structural transition between octahedral tetrahedral geometries around Cu(II), Cu(I), respectively contributing capabilities. The combination electrical double‐layer capacitance pseudocapacitance through Faradaic transfer is evaluated different acidic electrolytes, showing significant enhancement. Notably, proton‐coupled electron (PCET) at free pyridine‐N sites polypyridyl complex identified key factor distinct behavior aqueous solutions, finding supported by computational studies. This study shows binder‐free supercapacitor applications, with maximum areal 6.8 mF cm⁻ 2 media, representing 1840% improvement over bare rods.

Язык: Английский

Chemical Functionalization Meets Enhanced Electrical Conductivity in Iron Oxide Nanoparticles DOI Open Access
Neha Singh, Anurag Pritam, Jonas Fransson

и другие.

Advanced Functional Materials, Год журнала: 2025, Номер unknown

Опубликована: Янв. 31, 2025

Abstract An excellent combination of either oxides or metallic nanoparticles (NPs) and functional π‐electron rich conjugated molecules can originate a variety intriguing phenomena convenient for technological applications. Functional π‐conjugated aromatic hold the potential to control size, shape, morphology, optoelectronic properties through formation covalent interfaces. Interfacial charge transfer at nanoparticles−molecules interfaces plays vital roles in modulating photophysical electrical conductivity properties, which found enormous applications catalysis, electrical, magnetism. This work illustrates iron oxide (Fe 3 O 4 NPs) capped with situ generated aryl radicals tuning properties. Organic different groups are covalently attached surface Fe NPs radical formation. insulating pristine turns into semiconductor behavior upon functionalization, is due synergistic efficient intermolecular between mixed valence metal ions 2+ , d 6 electronic system, 3+ 5 system) (donor–acceptor interactions). A theoretical framework strongly supports experimental findings. These findings on using small molecule provide promising avenue wide range

Язык: Английский

Процитировано

4

Lateral nanoarchitectonics from nano to life: Ongoing challenge in interfacial chemical science DOI Creative Commons
Jingwen Song, Anna Jančík Procházková, Kohsaku Kawakami

и другие.

Chemical Science, Год журнала: 2024, Номер 15(45), С. 18715 - 18750

Опубликована: Янв. 1, 2024

The construction of functional structures within a single plane still has lot challenges. This review article will help us find new groundbreaking directions in lateral nanoarchitectonics toward advanced material organization.

Язык: Английский

Процитировано

7

Electrosynthesis of Ru (II)‐Polypyridyl Oligomeric Films on ITO Electrode for Two Terminal Non‐Volatile Memory Devices and Neuromorphic Computing DOI Open Access
Pradeep Sachan,

Pritish Sharma,

Rajwinder Kaur

и другие.

Small Methods, Год журнала: 2025, Номер unknown

Опубликована: Янв. 23, 2025

Abstract Molecular electronics exhibiting resistive‐switching memory features hold great promise for the next generation of digital technology. In this work, electrosynthesis ruthenium polypyridyl nanoscale oligomeric films is demonstrated on an indium tin oxide (ITO) electrode followed by ITO top contact deposition yielding large‐scale (junction area = 0.7 × cm 2 ) two terminal molecular junctions. The junctions exhibit non‐volatile resistive switching at a relatively lower operational voltage, ±1 V, high ON/OFF electrical current ratio (≈10 3 ), low‐energy consumption (SET/RESET 27.94/14400 nJ), good cyclic stability (>300 cycles), and speed 25 ms/20 ms). A computational study suggests that accessible frontier orbitals metal‐complex to Fermi level electrodes facilitate charge transport bias filamentformation. An extensive analysis performed performance binary neural networks exploiting current‐voltage devices as synaptic weights exploring their potential neuromorphic logic‐in‐memory implementation IMPLICATION (IMPLY) operation which can realize universal gates. comprehensive indicates proposed redox‐active complex‐based device may be promising candidate high‐density data storage, energy‐efficient with software‐level accuracy, implementations.

Язык: Английский

Процитировано

1

Electrochemically grafted molecular layers as on-chip energy storage molecular junctions DOI Creative Commons
Rajwinder Kaur, Ankur Malik, Ritu Gupta

и другие.

Chemical Science, Год журнала: 2025, Номер unknown

Опубликована: Янв. 1, 2025

Electrochemically grown heteroatoms containing organic films utilized to fabricate crossbar molecular junctions as classical capacitors for energy storage applications.

Язык: Английский

Процитировано

0

Altered electrochemistry of poly(3,4-ethylenedioxythiophene) after activation of the inserted cobalt ions DOI Creative Commons
Esteban Guillén, Jerónimo Agrisuelas, José Juan García-Jareño

и другие.

Journal of Electroanalytical Chemistry, Год журнала: 2024, Номер 968, С. 118440 - 118440

Опубликована: Июнь 13, 2024

Cobalt ions were inserted into poly(3,4-ethylenedioxythiophene) by cyclic voltammetry in a 0.1 M CoNO32 aqueous solution (PEDOT(Co)). After activation of the cobalt, PEDOT(aCo) system was investigated voltammetry, digital video electrochemistry, spectroelectrogravimetry, and coupled impedance techniques (ac-electrogravimetry) to elucidate key role cobalt altered electrochemistry PEDOT. The incorporation Co2+ involves slow transfer cations for charge compensation during Co2+⇄Co3+ conversion inside This fact explains enhanced storage showed compared with pristine PEDOT at similar potentials. Finally, stability measuring same time current, mass motional resistance variation 100 cycles offering high all times.

Язык: Английский

Процитировано

0

EIS Behavior of Polyethylene + Graphite Composite Considered as an Approximation to an Ensemble of Microelectrodes DOI Open Access
J. Navarro‐Laboulais, José Juan García-Jareño, Jerónimo Agrisuelas

и другие.

Journal of Composites Science, Год журнала: 2024, Номер 8(9), С. 378 - 378

Опубликована: Сен. 22, 2024

The electrical percolation of alternating current through two-phase polyethylene/graphite composite electrodes with different contents graphite microparticles immersed in aqueous KCl solutions has been studied. Above the content first threshold, electrochemical impedance response this electrode is associated an equivalent circuit resistance Ru series a constant phase element (CPE). An insulator material + conducting filler model proposed which electroactive surface considered as intersection cluster solid and interfacial region. CPE analyzed assuming distribution microcapacitors particles contact dielectric solution inside polymeric phase.

Язык: Английский

Процитировано

0

Unlocking the Potential of Redox‐Active Copper Complexes in Thin Films via Proton‐Coupled Electron Transfer for Enhanced Supercapacitor Performance DOI
Ritu Gupta, Ankur Malik, Pradeep Sachan

и другие.

Advanced Functional Materials, Год журнала: 2024, Номер unknown

Опубликована: Дек. 4, 2024

Abstract Nanoscale redox‐active molecular films are promising candidates for next‐generation energy storage applications due to their ability facilitate long‐range charge transport. However, establishing stable and efficient electrode‐molecule interfaces remains a critical challenge. In this study, the properties of copper‐polypyridyl thin covalently bonded graphite rods explored, investigating potential as supercapacitors. Using an electrochemical grafting method, robust covalent created, resulting in prepared on indium tin oxide (ITO) electrodes, exhibiting both Cu(II) Cu(I) redox states. These mettalo‐oligomeric demonstrate structural transition between octahedral tetrahedral geometries around Cu(II), Cu(I), respectively contributing capabilities. The combination electrical double‐layer capacitance pseudocapacitance through Faradaic transfer is evaluated different acidic electrolytes, showing significant enhancement. Notably, proton‐coupled electron (PCET) at free pyridine‐N sites polypyridyl complex identified key factor distinct behavior aqueous solutions, finding supported by computational studies. This study shows binder‐free supercapacitor applications, with maximum areal 6.8 mF cm⁻ 2 media, representing 1840% improvement over bare rods.

Язык: Английский

Процитировано

0