Enhanced Urea Oxidation Reaction Through Layered Double Hydroxides: Insights From ZIF‐67‐Derived Nanostructures DOI Creative Commons
Yuri Jeon, Jury J. Medvedev,

Yeeun Seong

и другие.

EcoMat, Год журнала: 2024, Номер unknown

Опубликована: Дек. 10, 2024

ABSTRACT Layered double hydroxides (LDHs) are ionic layered compounds characterized by anion‐containing intermediate regions within positively charged brucite‐like layers. LDHs have shown high electrochemical activity in energy conversion systems such as batteries and fuel cells. In this study, we developed a hierarchically porous nanostructure derived from zeolitic imidazolate framework‐67, which was subsequently transformed into an LDH structure with varying Ni concentrations. We precisely controlled the Ni‐to‐Co ratio investigated how different mole fractions of Co influence catalytic selectivity for urea oxidation reaction (UOR). structures low content (up to 40%) demonstrated O 2 due their structural instability predominant oxygen evolution (OER) originating ZIF‐67. contrast, (over 60%) supressed OER exhibited enhanced UOR. The resulting hollow expanded electrochemically active surface could improve mass transport diffusion at electrode interface, leading better kinetics higher current densities. These findings provide foundational design guideline metal–organic framework‐derived image

Язык: Английский

Current Progress in Layered Double Hydroxide-Based Electrocatalyst for Urea Oxidation: Insights into Strategies and Mechanisms DOI

Asha K Satheesan,

Ragunath Madhu, Sreenivasan Nagappan

и другие.

Chemical Communications, Год журнала: 2025, Номер unknown

Опубликована: Янв. 1, 2025

The urea oxidation reaction (UOR) presents a more favorable alternative to the conventional oxygen evolution (OER) for hydrogen production due its lower thermodynamic potential. This method offers advantages over traditional approaches operating conditions and potentially costs. However, complex 6-electron transfer process in UOR limits performance. Researchers are tackling this challenge by designing advanced electrocatalysts with optimized properties, such as porosity, heterostructures, controlled defects, surface functionalization, fine-tuned electronic structures. significant progress catalyst design holds promise future of clean energy technologies. In view this, layered double hydroxides (LDHs) attracting interest their potential role electrolysis synergistic cooperation metals, flexible configuration, tunable composition unique structure. review examines recent advancements synthesis LDH-based catalysts. Beyond highlighting breakthroughs catalysts, critically stresses strategies challenges towards conversion. Moreover, comprehensive approach provides valuable forward-looking perspective on research directions.

Язык: Английский

Процитировано

2

Triphenylamine-Substituted Ni(II) Porphyrins for Urea Electro-oxidation DOI
Shun Lu, Xingqun Zheng, Yi Zeng

и другие.

Inorganic Chemistry, Год журнала: 2024, Номер unknown

Опубликована: Окт. 23, 2024

Porphyrin-based molecular catalysts possess a typical aromatic macrocyclic structure regarding their metal centers and coordination frameworks, allowing for the development of promising electrocatalysts through precise selection porphyrin ligand. However, reports on metalloporphyrins as electrocatalytic urea oxidation reaction (UOR) remain scarce. With these considerations in mind, triphenylamine-Ni(II) (NiPor-TPA) was synthesized solvothermal approach from 5,10,15,20-tetrakis [4-(diphenylamino)phenyl]porphyrin nickel(II) acetate this work. Experimental results reveal that introduction Ni species can serve active sites activate efficiently, thus prepared deliver better activity than metal-free TPA. The NiPor-TPA electrode delivers lowest potential 1.34 V versus reversible hydrogen (RHE) at 10 mA cm

Язык: Английский

Процитировано

5

Ball-milled Ni@Mo2C/C nanocomposites as efficient electrocatalysts for urea oxidation DOI
Dilip Kumar Tiwari, Tapan Kumar Ghosh, Ajay Gopinathan

и другие.

Environmental Science and Pollution Research, Год журнала: 2025, Номер unknown

Опубликована: Фев. 10, 2025

Язык: Английский

Процитировано

0

Sub-3 nm Pt3Ni nanoparticles for urea-assisted water splitting DOI Creative Commons
Shun Lu, Xingqun Zheng,

Kaixin Jiang

и другие.

Advanced Composites and Hybrid Materials, Год журнала: 2025, Номер 8(2)

Опубликована: Фев. 24, 2025

Язык: Английский

Процитировано

0

Carbon-constrained heterogeneous Ni-Mo telluride for efficient urea oxidation DOI

Chun Yin,

Shuli Wang, Fulin Yang

и другие.

Chinese Chemical Letters, Год журнала: 2025, Номер unknown, С. 110999 - 110999

Опубликована: Фев. 1, 2025

Язык: Английский

Процитировано

0

Insight into the High Activity of Nickel Phosphide Precatalysts for Urea Oxidation DOI
Fulin Yang, Xingyu Huang, Ruonan Li

и другие.

The Journal of Physical Chemistry C, Год журнала: 2024, Номер 128(45), С. 19436 - 19444

Опубликована: Ноя. 4, 2024

The quest for advanced Ni-based (pre)catalysts the urea oxidation reaction (UOR) has been significantly impeded by a lack of understanding regarding catalytic structures and mechanisms after surface reconstruction, particularly metalloid compounds like nickel phosphide. This study systematically investigates UOR performance Ni(OH)2, phosphate (Ni–Pi), Ni2P, shedding light on role electronic structure morphology in dictating activity. Through electrochemical experiments situ spectroscopic techniques, we demonstrate that superior activity Ni2P originates from its unique conductivity presence residual ions, which facilitate formation highly active, coordinatively unsaturated sites following reconstruction as well faster electron transport. A novel descriptor based reversibility Ni3+/Ni2+ redox couple is proposed to underscore importance NiOOH regeneration kinetics process. findings reveal rapid dynamics results minimal accumulation intermediates, indicative high efficiency. research not only elucidates metal-nonmetal but also offers strategic framework design efficient electrocatalysts sustainable energy applications.

Язык: Английский

Процитировано

3

An efficient NiCoSe4/NiCo-LDH/CF catalyst for the co-production of value-added formate and hydrogen via selective methanol electro-oxidation DOI Creative Commons
Jiaxin Li, Hongmei Yu, Jun Chi

и другие.

Journal of Materials Chemistry A, Год журнала: 2024, Номер 12(38), С. 25791 - 25800

Опубликована: Янв. 1, 2024

An enhanced catalytic performance for selective methanol electrooxidation to formate was achieved derived from the “shuttle-like” role of Se and bimetallic synergism in NCS/CF.

Язык: Английский

Процитировано

1

Coordination tuning of FeNi‐HMT Framework derived effective hybrid catalysts for water oxidation DOI Open Access

Yunmeng Wang,

Luhong Fu, Jiawei Wu

и другие.

ChemSusChem, Год журнала: 2024, Номер unknown

Опубликована: Окт. 27, 2024

FeNi-based hybrid materials are promising oxygen evolution reaction (OER) catalysts for water electrolysis in hydrogen generation. In this work, the coordination tuning of FeNi-HMT frameworks was achieved by simply changing Fe/Ni ratios using hexamethylenetetramine (HMT) as an organic ligand, and derived FeNi with varied compositions were probed OER. Incorporating varying amounts Fe

Язык: Английский

Процитировано

1

Deciphering Doping Effects in a V-Doped Ni Catalyst for Hydrogen Electrooxidation DOI

Siguang Lu,

Luhong Fu, Fulin Yang

и другие.

Inorganic Chemistry, Год журнала: 2024, Номер 63(44), С. 21293 - 21302

Опубликована: Окт. 23, 2024

The improved performance of soluble metal-doped Ni catalysts is perplexed by the evolvable surface structures in alkaline electrolytes for hydrogen oxidation reaction (HOR). Herein, V-doped nanoparticles, as a proof concept, were carefully evaluated to explore intrinsic function enthetic V-species assisting HOR kinetic improvement. As expected, it exhibits mass-normalized current density 50.34 mA mgNi–1, more than 12 times that counterpart without introduction V. Systematic investigations prove V-species, including V-oxides and doped V atoms at outmost layer, would be dissolved into during process. remaining V-dopants inside nanoparticles rationally weaken hydroxyl binding energy (OHBE) Ni-based surfaces, thereby accelerating formation water molecules. We also uncover located overstrong branch OHBE-described volcano plot through theoretical calculations alkali-metal cation probe experiments, weakening OHBE internal V-doping can leave activity volcanic apex.

Язык: Английский

Процитировано

0

Enhanced Urea Oxidation Reaction Through Layered Double Hydroxides: Insights From ZIF‐67‐Derived Nanostructures DOI Creative Commons
Yuri Jeon, Jury J. Medvedev,

Yeeun Seong

и другие.

EcoMat, Год журнала: 2024, Номер unknown

Опубликована: Дек. 10, 2024

ABSTRACT Layered double hydroxides (LDHs) are ionic layered compounds characterized by anion‐containing intermediate regions within positively charged brucite‐like layers. LDHs have shown high electrochemical activity in energy conversion systems such as batteries and fuel cells. In this study, we developed a hierarchically porous nanostructure derived from zeolitic imidazolate framework‐67, which was subsequently transformed into an LDH structure with varying Ni concentrations. We precisely controlled the Ni‐to‐Co ratio investigated how different mole fractions of Co influence catalytic selectivity for urea oxidation reaction (UOR). structures low content (up to 40%) demonstrated O 2 due their structural instability predominant oxygen evolution (OER) originating ZIF‐67. contrast, (over 60%) supressed OER exhibited enhanced UOR. The resulting hollow expanded electrochemically active surface could improve mass transport diffusion at electrode interface, leading better kinetics higher current densities. These findings provide foundational design guideline metal–organic framework‐derived image

Язык: Английский

Процитировано

0