Development and Validation of an HPLC-DAD Method to Determine Alkylphenols in Milk
Beverages,
Год журнала:
2025,
Номер
11(3), С. 59 - 59
Опубликована: Апрель 24, 2025
While
providing
considerable
societal
and
economic
benefits,
plastic
packaging
leads
to
global
pollution
poses
health
risks.
Plastic
additives
like
alkylphenols
(APs)
can
interfere
with
endocrine
functions
even
at
low
concentrations.
Therefore,
developing
validating
analytical
methods
for
their
routine
dosage
in
foods
is
paramount.
The
present
work
validated
a
chromatographic
method
quantify
(4-tert-octylphenol,
4-n-octylphenol
mono-ethoxylate,
4-n-octylphenol,
4-n-nonylphenol)
milk.
uses
Chem
Elut
S
rapid
supported
liquid
extraction
(SLE)
cartridges
eliminate
the
matrix
effect,
reverse
phase
chromatography
linked
Diode
Array
Detector
(DAD)
alkylphenols.
was
using
strategy
of
accuracy
profiling,
decision-making
instrument
that
calculates
method’s
total
error,
encompassing
bias
standard
deviation.
reliability
test
defined
by
lack
retention
times
APs
interfering
peaks,
close
linear
relationship
between
independent
dependent
variables
regression
model,
excellent
precision
each
concentration
level
intra-day
inter-day
measurements,
errors
procedure
(systematic
random)
estimated
within
pre-established
acceptability
limits
(±10%).
minimal
environmental
impact
ease
execution
suggest
its
use
analyses.
Язык: Английский
Recent Advances in Chromatographic Analysis of Emerging Pollutants in Dairy Milk: A Review (2018–2023)
Опубликована: Март 12, 2024
Emerging
pollutants
(EPs)
encompass
natural
or
synthetic
substances
in
the
environment
that
pose
potential
risks
but
have
only
recently
been
recognized
monitored.
EPs
consist
of
various
categories
including
pesticides,
pharmaceuticals,
hormones,
mycotoxins,
and
endocrine
disrupting
chemicals
(EDCs).
Through
several
pathways,
can
access
food,
potentially
leading
to
health
impacts
when
their
safe
concentrations
are
exceeded.
Milk,
being
a
highly
nutritious
heavily
consumed
food
product
by
many
consumers
different
ages,
is
crucial
matrix
where
should
be
regularly
In
literature,
large
number
studies
was
dedicated
for
determination
dairy
milk,
employing
analytical
techniques.
Chromatographic
based
techniques
were
most
prevalent
means
analysis
which
demonstrated
significant
efficiency,
sensitivity
accuracy
this
specific
purpose.
Prior
chromatographic
analysis,
extraction
from
complex
like
essential.
This
review
comprehensively
covers
relevant
research
papers
on
subsequent
detection
milk
methods
2018
until
2023.
Язык: Английский