Comprehensive Strategies for the Synthesis of 1,3-Enyne Derivatives DOI
Chinmoy Kumar Hazra, Chandi C. Malakar, Kamal Kant

и другие.

Synthesis, Год журнала: 2024, Номер unknown

Опубликована: Май 1, 2024

Abstract The synthesis of 1,3-enyne has widespread appeal in organic due to their proven adaptability as intermediates routes compounds significant biological and material interest. A variety methods have been designed formulate 1,3-enynes from diverse substrates, such alkynes, 1,3-diynes, alkynyl-substituted cyclopropanes, propargyl alcohols. This review covers the utilizing homo- cross-coupling nucleophilic metal/acid-induced cyclopropane ring opening, rearrangement/dehydration key concern procedures starting alkynes 1,3-diynes is management regio-, stereo-, and, where fitting, chemoselectivity. In contrast, cyclopropyl opening nucleophile orientation determines formed. Efficient for broad selective are highlighted specific examples given demonstrate efficacy these processes. 1 Introduction Scope 2 Synthesis 2.1 1,3-Enynes Alkynes 2.1.1 Metal-Catalyzed Cross-Coupling/Additions with Alkenes or Vinyl Aryl Halides 2.1.1.1 Palladium Catalysis 2.1.1.2 Rhodium 2.1.1.3 Copper 2.1.1.4 I ron 2.1.1.5 Nickel 2.1.1.6 Miscellaneous 2.2 Enynes Propargyl Alcohols 2.3 Metal/Acid-Catalyzed Ring Opening Cyclopropanes 3 Conclusion

Язык: Английский

Recent Advancements in Strategies for the Synthesis of Imidazoles, Thiazoles, Oxazoles, and Benzimidazoles DOI
Kamal Kant, Chandresh K. Patel, Sourav Banerjee

и другие.

ChemistrySelect, Год журнала: 2023, Номер 8(47)

Опубликована: Дек. 13, 2023

Abstract Nitrogen‐containing heterocycles such as imidazoles, thiazoles, and oxazoles play a significant role in the fields of biological pharmaceutical chemistry. These compounds were widely used for agrochemical, pesticide, medicinal, industrial applications. Due to wide spectrum structural diversity well activity N ‐heterocycles, plethora reports on their synthesis have appeared last few decades. However, developments various bond‐forming strategies C−C, C−N, C−O, C−S, N−N, C−H activation, been powerful synthetic tool derive copious ‐heterocycles. The most prominent fascinating imidazole, thiazole, oxazoles, benzimidazole moieties by C−C C−N coupling reactions, multi‐component cycloaddition etc. are discussed this study. studies demonstrated enormous potential methods accelerating modern chemical establishing molecular beauty through bonding. aspects methodologies, like optimized conditions, substrate scope, mechanistic investigations, detail.

Язык: Английский

Процитировано

19

Organocatalytic Approaches towards the Synthesis of Asymmetric Tetrahydroquinoline (THQ) Derivatives DOI
Chandi C. Malakar, Kamal Kant, Priyadarshini Naik

и другие.

Synthesis, Год журнала: 2024, Номер unknown

Опубликована: Июль 30, 2024

Abstract 1,2,3,4-Tetrahydroquinolines (THQs) are present in molecules with significant biological importance and pharmaceuticals diverse activities. Various synthetic routes have been developed to tetrahydroquinolines, such as the hydrogenation of quinolines, domino reactions, intramolecular cyclization, notably, Povarov reaction. Organocatalysts small, chiral organic that can successfully catalyze transformations. This review examines use organocatalysts asymmetric synthesis tetrahydroquinoline derivatives using aminocatalysis, NHC catalysis, H-bonding catalysis covering literature between 2000 early 2024. 1 Introduction 2 Aminocatalysis 3 Catalysis 4 H-Bonding 5 Miscellaneous 6 Conclusion

Язык: Английский

Процитировано

2

Comprehensive Strategies for the Synthesis of 1,3-Enyne Derivatives DOI
Chinmoy Kumar Hazra, Chandi C. Malakar, Kamal Kant

и другие.

Synthesis, Год журнала: 2024, Номер unknown

Опубликована: Май 1, 2024

Abstract The synthesis of 1,3-enyne has widespread appeal in organic due to their proven adaptability as intermediates routes compounds significant biological and material interest. A variety methods have been designed formulate 1,3-enynes from diverse substrates, such alkynes, 1,3-diynes, alkynyl-substituted cyclopropanes, propargyl alcohols. This review covers the utilizing homo- cross-coupling nucleophilic metal/acid-induced cyclopropane ring opening, rearrangement/dehydration key concern procedures starting alkynes 1,3-diynes is management regio-, stereo-, and, where fitting, chemoselectivity. In contrast, cyclopropyl opening nucleophile orientation determines formed. Efficient for broad selective are highlighted specific examples given demonstrate efficacy these processes. 1 Introduction Scope 2 Synthesis 2.1 1,3-Enynes Alkynes 2.1.1 Metal-Catalyzed Cross-Coupling/Additions with Alkenes or Vinyl Aryl Halides 2.1.1.1 Palladium Catalysis 2.1.1.2 Rhodium 2.1.1.3 Copper 2.1.1.4 I ron 2.1.1.5 Nickel 2.1.1.6 Miscellaneous 2.2 Enynes Propargyl Alcohols 2.3 Metal/Acid-Catalyzed Ring Opening Cyclopropanes 3 Conclusion

Язык: Английский

Процитировано

1