Integration of cocrystal and nanocrystal techniques to ameliorate solubility, topical antioxidant activity and cytotoxicity of curcumin DOI

A. D. Mohammed Saleem,

Hafsa Afzal,

Najam ul

и другие.

Research Square (Research Square), Год журнала: 2025, Номер unknown

Опубликована: Май 14, 2025

Abstract Curcumin (CUM), a promising nutraceutical, exhibits diverse pharmacological activities such as antioxidant, anti-inflammatory, antitumor and anti-hyperglycemic, but the clinical applications of CUM is restricted by virtue its scarce aqueous solubility, poor stability and, low oral topical absorption. In this work nano-cocrystal strategy, integrating benefits cocrystallization nanocrystal techniques, has been proposed to obtain superior characters CUM. A cocrystal was successfully synthesized with ascorbic acid solvent evaporation then transformed into (NCC) top down homogenization technique using poloxamer 188 stabilizer. NCC delineated SEM Zetasizer appeared be round-shaped particles mean particle size 200 ± 30nm. Further characterization undertaken PXRD, DSC FTIR spectroscopy. presented 16 10 fold enhanced solubility dissolution in distilled water comparison pure From In-vitro antioxidant cytotoxicity studies, it suggested that displayed highest percentage inhibition (99.154 0.58%) IC50 value 1.4 0.180µg/ml also led reduction viability MCF-7 breast cancer cells. On formulating gel, stable for six months at 4 2°C 30 /65 5% RH. release studies gel modified Franz diffusion cell demonstrated 2.4fold cumulative compared gel. Release data best fitted Hixon-Crowell kinetic model n showing non Fickian release. Hence, higher greater make formulation.

Язык: Английский

Integration of cocrystal and nanocrystal techniques to ameliorate solubility, topical antioxidant activity and cytotoxicity of curcumin DOI

A. D. Mohammed Saleem,

Hafsa Afzal,

Najam ul

и другие.

Research Square (Research Square), Год журнала: 2025, Номер unknown

Опубликована: Май 14, 2025

Abstract Curcumin (CUM), a promising nutraceutical, exhibits diverse pharmacological activities such as antioxidant, anti-inflammatory, antitumor and anti-hyperglycemic, but the clinical applications of CUM is restricted by virtue its scarce aqueous solubility, poor stability and, low oral topical absorption. In this work nano-cocrystal strategy, integrating benefits cocrystallization nanocrystal techniques, has been proposed to obtain superior characters CUM. A cocrystal was successfully synthesized with ascorbic acid solvent evaporation then transformed into (NCC) top down homogenization technique using poloxamer 188 stabilizer. NCC delineated SEM Zetasizer appeared be round-shaped particles mean particle size 200 ± 30nm. Further characterization undertaken PXRD, DSC FTIR spectroscopy. presented 16 10 fold enhanced solubility dissolution in distilled water comparison pure From In-vitro antioxidant cytotoxicity studies, it suggested that displayed highest percentage inhibition (99.154 0.58%) IC50 value 1.4 0.180µg/ml also led reduction viability MCF-7 breast cancer cells. On formulating gel, stable for six months at 4 2°C 30 /65 5% RH. release studies gel modified Franz diffusion cell demonstrated 2.4fold cumulative compared gel. Release data best fitted Hixon-Crowell kinetic model n showing non Fickian release. Hence, higher greater make formulation.

Язык: Английский

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