Visible-Light-Induced Radical Carbon Oximation of Styrenes Using N-Nitrosoamine and Organic Halides DOI

Jinping Lan,

Xiaolong Li, Mengyu Xu

и другие.

The Journal of Organic Chemistry, Год журнала: 2024, Номер unknown

Опубликована: Дек. 23, 2024

An efficient visible-light-induced radical carbon oximation of styrenes with 1-nitrosopyrrolidine and organic halides is developed. The reaction proceeds smoothly in the absence a transition metal photocatalyst under mild conditions, producing wide range functionalized oximes moderate to good yields. Mechanistic studies reveal that involves generation nucleophilic α-amino alkyl radicals subsequent halogen atom transfer (XAT) halides.

Язык: Английский

Inorganic Bismuth Catalysts for Photocatalytic Organic Reactions DOI Open Access
Hai He, Qi‐Yan Lv, Bing Yu

и другие.

Catalysts, Год журнала: 2025, Номер 15(2), С. 135 - 135

Опубликована: Фев. 1, 2025

Bismuth (Bi) is recognized as a low-toxicity and environmentally friendly metal. Owing to its diverse oxidation states, Bi-based compounds demonstrate exceptional catalytic activities across numerous organic reactions. In particular, inorganic materials have emerged promising class of photocatalysts in synthetic chemistry. this review, the recent applications Bi-materials, e.g., Bi2O3, BiVO4, BiCl3, Bi2WO6, Bi4O5Br2, various reactions, including C-H oxidation, radical addition olefins, coupling been summarized. The reaction mechanisms are discussed reveal crucial steps for enhancing performance. Moreover, current challenges prospects vibrant research area also outlined, aiming provide valuable insights guidance development more efficient their pathways.

Язык: Английский

Процитировано

0

Solar refinery: a disruptive strategy for upcycling plastic wastes DOI
Baowen Zhou, Ding Wang

Science China Chemistry, Год журнала: 2025, Номер unknown

Опубликована: Фев. 12, 2025

Язык: Английский

Процитировано

0

Crystalline Arylstibinidene Chalcogenides: Heavier Congeners of Aromatic Nitroso Compounds DOI
Xinyi Li, Yizhen Chen, Shicheng Dong

и другие.

Journal of the American Chemical Society, Год журнала: 2025, Номер unknown

Опубликована: Март 10, 2025

Nitroso compounds, R-N═O, containing N═O double bonds are ubiquitous and widely utilized in organic synthesis. In contrast, heavier congeners of nitroso namely pnictinidene chalcogenides R-Pn = E (Pn P, As, Sb, Bi; O, S, Se, Te), highly reactive scarce. They have been stabilized the coordination sphere Lewis acid/base or by pronounced contribution from resonance structures, whereas free species with unperturbed pnictogen-chalcogen remains elusive. this work, we report isolation characterization arylstibinidene chalcogenides, which first aromatic compounds. facilely synthesized through salt metathesis reactions aryldichlorostibane dilithium chalcogenides. bear Sb═E (E Se Te) due to poor orbital overlap between C 2p orbitals phenyl ring substituent Sb 5p orbitals. Moreover, they show versatile reactivity, including acting as chalcogen atom transfer reagents reacting small molecules via (cyclo)addition.

Язык: Английский

Процитировано

0

Synthesis of Primary and Secondary Amines via Electrochemical Reduction of Hydrazines DOI

Dong Wang,

Qiulu Wang,

Mingxia Liu

и другие.

Organic Letters, Год журнала: 2024, Номер 26(51), С. 11123 - 11128

Опубликована: Дек. 13, 2024

We herein introduce an electrochemical route for the N–N bond cleavage of hydrazines. This mild and green methodology utilized readily available mono- 1,1-disubstituted hydrazines or their HCl salts as starting materials to access a broad scope primary secondary amines in high yields. The mechanistic investigation suggests that amine product is formed by consecutive SET reduction, utilization hydrazine salt important providing sufficient conductivity acidity facilitate this reaction.

Язык: Английский

Процитировано

2

Recent Advances in the Synthetic Applications of Nitrosoarene Chemistry DOI
Feng Lin, Rongzhi Tang, Sheng Liu

и другие.

Organic & Biomolecular Chemistry, Год журнала: 2024, Номер unknown

Опубликована: Ноя. 20, 2024

This review covers reactions involving nitrosoarenes over the last decade, including cyclization, with attacks at oxygen or nitrogen terminus, dimerization, rearrangement, coordination, and other significant reactions.

Язык: Английский

Процитировано

1

Visible-Light-Induced Radical Carbon Oximation of Styrenes Using N-Nitrosoamine and Organic Halides DOI

Jinping Lan,

Xiaolong Li, Mengyu Xu

и другие.

The Journal of Organic Chemistry, Год журнала: 2024, Номер unknown

Опубликована: Дек. 23, 2024

An efficient visible-light-induced radical carbon oximation of styrenes with 1-nitrosopyrrolidine and organic halides is developed. The reaction proceeds smoothly in the absence a transition metal photocatalyst under mild conditions, producing wide range functionalized oximes moderate to good yields. Mechanistic studies reveal that involves generation nucleophilic α-amino alkyl radicals subsequent halogen atom transfer (XAT) halides.

Язык: Английский

Процитировано

0