Colorimetric and fluorescent dual mode detection of Fe (III) ion in blood samples in combination with cloud point extraction

Microchemical Journal, Год журнала: 2023, Номер 195, С. 109390 - 109390

Опубликована: Сен. 21, 2023

Язык: Английский

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Detection of antibiotics in yak and other non-traditional milks and health risks assessments from the Northwestern Himalayan region

Microchemical Journal, Год журнала: 2024, Номер unknown, С. 112530 - 112530

Опубликована: Дек. 1, 2024

Язык: Английский

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The potential of new solvents and materials in the context of green analytical chemistry

Advances in Sample Preparation, Год журнала: 2023, Номер 8, С. 100096 - 100096

Опубликована: Сен. 25, 2023

Язык: Английский

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In vitro dissolution equivalence of Jordanian sildenafil generics via validated, stability-indicating HPLC method

Bioanalysis, Год журнала: 2024, Номер 16(9), С. 369 - 384

Опубликована: Март 18, 2024

This study was conducted to compare dissolution profiles of four Jordanian registered sildenafil (SDF) products the originator. Dissolution samples were analyzed utilizing a validated and stability-indicating HPLC method in human plasma. Validation performed for specificity, linearity, limit detection, lower quantification, precision, trueness stability. SDF extracted from plasma using liquid–liquid extraction. The analysis isocratic elution on C18 column with 1.0 ml/min flow rate. regression value ∼0.999 over 3 days drug recovery between 86.6 89.8%with 10 ng/ml quantitation. displayed good selectivity improved stability under various conditions. used quantification medium. Similarity factors local varied according mediums, but all passed vitro test since them showed released >85% after 60 min at mediums.

Язык: Английский

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Advances in pharmacotoxicological investigation of Sudden Cardiac Death: Literature review and novel perspectives

Journal of Chromatography Open, Год журнала: 2024, Номер 6, С. 100153 - 100153

Опубликована: Июль 10, 2024

Pharmacotoxicology is one of the fields that in recent years growing exponentially, further reaffirming its proven usefulness field forensic sciences. An interesting goal this to identify and quantify cause death. This review paper aims represent a literature order evaluate state art regarding research pharmacotoxicology cases Sudden Cardiac Death (SCD), frequent problem on several occasions, which can be derived from use fatal substances or such concentrations causing sudden In overview, most frequently observed biomarkers for SCD were found ethanol, illicit drugs, antidepressants, some common compounds like caffeine Trenbolone. Concurrently, applied instrument configurations represented by hyphenated liquid (or gas) chromatographic tools coupled with mass spectrometry (LC-MS GC–MS) reach high accuracy confidence levels confirmatory analyses, preceded sample preparation technique as solid-liquid extraction liquid-liquid extraction. It was understand approaches researchers have approached topic, because hand there are those who been interested comparison between matrices (conventional not) other hand, has researched metabolites able trace intake not substance. particular, work want highlight evaluate, medical-legal point view, main physiological markers interest methods, instrumental procedures used their evaluation. The organized considering analytical methods divided types drugs/substances.

Язык: Английский

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Sample preparation using microfluidic technologies for non-invasive tests

Elsevier eBooks, Год журнала: 2024, Номер unknown

Опубликована: Янв. 1, 2024

Язык: Английский

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Green solvent microextraction

Elsevier eBooks, Год журнала: 2024, Номер unknown, С. 337 - 360

Опубликована: Ноя. 1, 2024

Язык: Английский

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