Colorimetric and fluorescent dual mode detection of Fe (III) ion in blood samples in combination with cloud point extraction

Microchemical Journal, Journal Year: 2023, Volume and Issue: 195, P. 109390 - 109390

Published: Sept. 21, 2023

Language: Английский

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Detection of antibiotics in yak and other non-traditional milks and health risks assessments from the Northwestern Himalayan region

Microchemical Journal, Journal Year: 2024, Volume and Issue: unknown, P. 112530 - 112530

Published: Dec. 1, 2024

Language: Английский

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In vitro dissolution equivalence of Jordanian sildenafil generics via validated, stability-indicating HPLC method

Bioanalysis, Journal Year: 2024, Volume and Issue: 16(9), P. 369 - 384

Published: March 18, 2024

This study was conducted to compare dissolution profiles of four Jordanian registered sildenafil (SDF) products the originator. Dissolution samples were analyzed utilizing a validated and stability-indicating HPLC method in human plasma. Validation performed for specificity, linearity, limit detection, lower quantification, precision, trueness stability. SDF extracted from plasma using liquid–liquid extraction. The analysis isocratic elution on C18 column with 1.0 ml/min flow rate. regression value ∼0.999 over 3 days drug recovery between 86.6 89.8%with 10 ng/ml quantitation. displayed good selectivity improved stability under various conditions. used quantification medium. Similarity factors local varied according mediums, but all passed vitro test since them showed released >85% after 60 min at mediums.

Language: Английский

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Advances in pharmacotoxicological investigation of Sudden Cardiac Death: Literature review and novel perspectives

Journal of Chromatography Open, Journal Year: 2024, Volume and Issue: 6, P. 100153 - 100153

Published: July 10, 2024

Pharmacotoxicology is one of the fields that in recent years growing exponentially, further reaffirming its proven usefulness field forensic sciences. An interesting goal this to identify and quantify cause death. This review paper aims represent a literature order evaluate state art regarding research pharmacotoxicology cases Sudden Cardiac Death (SCD), frequent problem on several occasions, which can be derived from use fatal substances or such concentrations causing sudden In overview, most frequently observed biomarkers for SCD were found ethanol, illicit drugs, antidepressants, some common compounds like caffeine Trenbolone. Concurrently, applied instrument configurations represented by hyphenated liquid (or gas) chromatographic tools coupled with mass spectrometry (LC-MS GC–MS) reach high accuracy confidence levels confirmatory analyses, preceded sample preparation technique as solid-liquid extraction liquid-liquid extraction. It was understand approaches researchers have approached topic, because hand there are those who been interested comparison between matrices (conventional not) other hand, has researched metabolites able trace intake not substance. particular, work want highlight evaluate, medical-legal point view, main physiological markers interest methods, instrumental procedures used their evaluation. The organized considering analytical methods divided types drugs/substances.

Language: Английский

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Sample preparation using microfluidic technologies for non-invasive tests

Elsevier eBooks, Journal Year: 2024, Volume and Issue: unknown

Published: Jan. 1, 2024

Language: Английский

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Green solvent microextraction

Elsevier eBooks, Journal Year: 2024, Volume and Issue: unknown, P. 337 - 360

Published: Nov. 1, 2024

Language: Английский

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The potential of new solvents and materials in the context of green analytical chemistry

Advances in Sample Preparation, Journal Year: 2023, Volume and Issue: 8, P. 100096 - 100096

Published: Sept. 25, 2023

Language: Английский

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