Simultaneous quantification of 39 pesticide and veterinary drug residues in aquaculture products using ultra performance liquid chromatography tandem mass spectrometry with modified QuEChERS DOI Creative Commons
Shuo Li, Yijun Liu, Dan Jiang

и другие.

Research Square (Research Square), Год журнала: 2023, Номер unknown

Опубликована: Дек. 22, 2023

Abstract A high throughput quantification multi-residues method for the simultaneous detection of 39 pesticides and veterinary drugs in aquaculture products were developed by using Ultra-high performance liquid chromatography coupled to tandem mass spectrometry (UPLC-MS/MS) with modified QuEChERS (quick、easy、cheap、effective、rugged、safe). In order balance recovery efficiency, several parameters optimized, including extracting, clarification, purification. Chromatographic conditions optimized given run time ＜ 13 min. Six representative matrices (muscle tissues yellow croaker, pomfret, shrimp, white shell, flower razor clam) show applicability all target analytes showed recoveries (60.3%~119.0%) acceptable precision (4.3%~20.8%). Furthermore, limits (LODs) (LOQs) range 1.0 ~ 5.0 µg/kg 3.0 10.0 µg/kg, respectively, that providing a practical safety internal risk controlling aquaculture.

Язык: Английский

Trophic transfer of sulfonamide antibiotics in aquatic food chains:a comprehensive review with a focus on environmental health risks DOI

Tianwei Peng,

Biao Song,

Yuchen Wang

и другие.

Environmental Pollution, Год журнала: 2025, Номер unknown, С. 125823 - 125823

Опубликована: Фев. 1, 2025

Язык: Английский

Процитировано

2
An innovative nanoparticle-modified carbon paste sensor for ultrasensitive detection of lignocaine and its extremely carcinogenic metabolite residues in bovine food samples: Application of NEMI, ESA, AGREE, ComplexGAPI, and RGB12 algorithms DOI
Sherif M. Eid, Khalid A.M. Attia, Ahmed El‐Olemy

и другие.

Food Chemistry, Год журнала: 2023, Номер 426, С. 136579 - 136579

Опубликована: Июнь 12, 2023

Язык: Английский

Процитировано

23
Green metrics for analytical methodologies: Uncovering sustainable chromatography approaches for detecting emerging contaminants in food and environmental water DOI
Nor Munira Hashim, Maisarah Nasution Waras, Noorfatimah Yahaya

и другие.

TrAC Trends in Analytical Chemistry, Год журнала: 2024, Номер 172, С. 117598 - 117598

Опубликована: Фев. 16, 2024

Язык: Английский

Процитировано

6
Advances in thin film micro-extraction (TFME) of selected organic pollutants, and the evaluation of the sample preparation procedures using the AGREEprep green metric tool DOI
Herbert Musarurwa

Microchemical Journal, Год журнала: 2024, Номер 203, С. 110938 - 110938

Опубликована: Июнь 12, 2024

Язык: Английский

Процитировано

5
Validated chromatographic approach for determination of two ternary mixtures in newly approved formulations for helicobacter pylori eradication: assessment of greenness profile and content uniformity DOI Creative Commons
Yomna A. Salem,

Samah A. Elsabour,

Amal A. El‐Masry

и другие.

BMC Chemistry, Год журнала: 2024, Номер 18(1)

Опубликована: Июнь 12, 2024

Abstract A new, sensitive, and rapid isocratic reversed phase chromatographic method (RP-HPLC–UV) was developed for simultaneous separation of two newly co-formulated antiulcer mixtures; Amoxicillin, Vonoprazan Clarithromycin [Mixture (I)], Lansoprazole (II)]. Analytical performed using a Promosil C 18 column ultraviolet detection at 210 nm. The achieved within only 8 min. For both mixtures, an aqueous solution, composed (Acetonitrile: Methanol: 0. 2 M phosphoric acid) ratio (30: 30: 40) adjusted to final pH 3.0, the mobile phase. This validated as per International Conference on Harmonization guidelines. linearity ranges these proposed (Mixture (I)) were 25.0–400.0 µg/mL 0.5–8.0 Vonoprazan, 12.5–200.0 Clarithromycin. And (II)) 10.0–300.0 0.3–9.0 5.0–150.0 firstly applied effective (I)]. It fulfilled good repeatability, sensitivity, accuracy (R.S.D. < 2.0%). mean recoveries analytes in their Tri-Pak formulations acceptable. greenness methods assessed Eco-scale it content uniformity testing United States Pharmacopoeia (USP) acceptance value Mixture (I) 2.88, values (II) 2.592, 2.424, respectively.

Язык: Английский

Процитировано

5
Recent developments in sample pretreatment techniques for the determination of fluoroquinolones in foods DOI
Irina Timofeeva,

Kirill Barbayanov,

Maria Kochetkova

и другие.

TrAC Trends in Analytical Chemistry, Год журнала: 2024, Номер 178, С. 117831 - 117831

Опубликована: Июнь 22, 2024

Язык: Английский

Процитировано

5
Microplastic and Associated Emerging Contaminants in Marine Fish from the South China Sea: Exposure and Human Risks DOI
Xiaoxuan Yu,

Qilin Gutang,

Yuxuan Wang

и другие.

Journal of Hazardous Materials, Год журнала: 2024, Номер 480, С. 136200 - 136200

Опубликована: Окт. 16, 2024

Язык: Английский

Процитировано

5
Breaking barrier of binding buffer in colorimetric aptasensing of tetracycline in food fish using peroxidase mimic gold NanoZyme DOI
Dhruba Jyoti Sarkar,

Ramij Raja,

Vikash Kumar

и другие.

Methods, Год журнала: 2025, Номер unknown

Опубликована: Апрель 1, 2025

Язык: Английский

Процитировано

0
Dispersive Solid-Phase Extraction and Ultra-Performance Liquid Chromatography–Tandem Mass Spectrometry—A Rapid and Accurate Method for Detecting 10 Macrolide Residues in Aquatic Products DOI Creative Commons
Jinyu Chen,

Guangming Mei,

Xiaojun Zhang

и другие.

Foods, Год журнала: 2024, Номер 13(6), С. 866 - 866

Опубликована: Март 13, 2024

The amount of macrolide (MAL) residues in aquatic products, including oleandomycin (OLD), erythromycin (ERM), clarithromycin (CLA), azithromycin (AZI), kitasamycin (KIT), josamycin (JOS), spiramycin (SPI), tilmicosin (TIL), tylosin (TYL), and roxithromycin (ROX), was determined using solid-phase extraction ultra-performance liquid chromatography–tandem mass spectrometry (UPLC-MS/MS). were extracted with 1% ammonia acetonitrile solution purified by neutral alumina adsorption. Chromatographic separation completed on an ACQUITY UPLC BEH C18 column acetonitrile–0.1% formic acid aqueous as the mobile phase, detection performed multiple reaction monitoring scanning positive mode electrospray ion source (ESI+). Five isotopically labeled compounds used internal standards for quality control purposes. findings indicated that across concentration span 1.0–100 μg/L, there a strong linear correlation (R2 > 0.99) between instrumental response 10 MALs. limit UPLC-MS/MS 0.25–0.50 μg/kg, quantitation 0.5–1.0 μg/kg. added recovery blank matrix samples at standard gradient levels (1.0, 5.0, 50.0 μg/kg) 83.1–116.6%, intra-day precision inter-day precisions 3.7 13.8%, respectively. method is simple fast, high accuracy good repeatability, line requirements accurate qualitative quantitative analysis MALs products.

Язык: Английский

Процитировано

3
Bioaccumulation of Organic and Inorganic Pollutants in Fish from Thermaikos Gulf: Preliminary Human Health Risk Assessment Assisted by a Computational Approach DOI Creative Commons
Konstantinos M. Kasiotis, Effrosyni Zafeiraki, Electra Manea-Karga

и другие.

Journal of Xenobiotics, Год журнала: 2024, Номер 14(2), С. 701 - 716

Опубликована: Июнь 1, 2024

The monitoring of contaminants in fish species is pivotal for fishes’ health and reproduction, as well human health. In the specific work, three major categories contaminants, pesticides, pharmaceuticals, macro trace elements, were investigated two species, Dicentrarchus labrax Solea solea, collected from Thermaikos Gulf, Greece. To achieve this goal, analytical methods using LC-MS/MS, GC-MS/MS, ICP-MS developed, validated, applied to samples. results indicated a very low prevalence caffeine acetaminophen, both not exceeding 3.8 μg/kg fish. Similarly, thiabendazole, cypermethrin, tricyclazole (pesticides) found concentration range 0.9 13.7 fish, while one D. sample, traces metabolite organochlorine pesticide DDT, o,p’-DDE detected. Al, Mn, Fe, Zn, Sr predominant elements 500–20,000 Macro levels varied 280 5405 mg/kg Health risk assessment did unveil an unacceptable adults, apart sample presenting Hg above regulatory levels. On contrary, children, calculated hazard quotient values all cases As detections higher than threshold value 1, indicating potential risk.

Язык: Английский

Процитировано

3