Simultaneous quantification of 39 pesticide and veterinary drug residues in aquaculture products using ultra performance liquid chromatography tandem mass spectrometry with modified QuEChERS DOI Creative Commons
Shuo Li, Yijun Liu, Dan Jiang

et al.

Research Square (Research Square), Journal Year: 2023, Volume and Issue: unknown

Published: Dec. 22, 2023

Abstract A high throughput quantification multi-residues method for the simultaneous detection of 39 pesticides and veterinary drugs in aquaculture products were developed by using Ultra-high performance liquid chromatography coupled to tandem mass spectrometry (UPLC-MS/MS) with modified QuEChERS (quick、easy、cheap、effective、rugged、safe). In order balance recovery efficiency, several parameters optimized, including extracting, clarification, purification. Chromatographic conditions optimized given run time ＜ 13 min. Six representative matrices (muscle tissues yellow croaker, pomfret, shrimp, white shell, flower razor clam) show applicability all target analytes showed recoveries (60.3%~119.0%) acceptable precision (4.3%~20.8%). Furthermore, limits (LODs) (LOQs) range 1.0 ~ 5.0 µg/kg 3.0 10.0 µg/kg, respectively, that providing a practical safety internal risk controlling aquaculture.

Language: Английский

Trophic transfer of sulfonamide antibiotics in aquatic food chains:a comprehensive review with a focus on environmental health risks DOI

Tianwei Peng,

Biao Song,

Yuchen Wang

et al.

Environmental Pollution, Journal Year: 2025, Volume and Issue: unknown, P. 125823 - 125823

Published: Feb. 1, 2025

Language: Английский

Citations

1
An innovative nanoparticle-modified carbon paste sensor for ultrasensitive detection of lignocaine and its extremely carcinogenic metabolite residues in bovine food samples: Application of NEMI, ESA, AGREE, ComplexGAPI, and RGB12 algorithms DOI
Sherif M. Eid, Khalid A.M. Attia, Ahmed El‐Olemy

et al.

Food Chemistry, Journal Year: 2023, Volume and Issue: 426, P. 136579 - 136579

Published: June 12, 2023

Language: Английский

Citations

23
Green metrics for analytical methodologies: Uncovering sustainable chromatography approaches for detecting emerging contaminants in food and environmental water DOI
Nor Munira Hashim, Maisarah Nasution Waras, Noorfatimah Yahaya

et al.

TrAC Trends in Analytical Chemistry, Journal Year: 2024, Volume and Issue: 172, P. 117598 - 117598

Published: Feb. 16, 2024

Language: Английский

Citations

6
Advances in thin film micro-extraction (TFME) of selected organic pollutants, and the evaluation of the sample preparation procedures using the AGREEprep green metric tool DOI
Herbert Musarurwa

Microchemical Journal, Journal Year: 2024, Volume and Issue: 203, P. 110938 - 110938

Published: June 12, 2024

Language: Английский

Citations

5
Validated chromatographic approach for determination of two ternary mixtures in newly approved formulations for helicobacter pylori eradication: assessment of greenness profile and content uniformity DOI Creative Commons
Yomna A. Salem,

Samah A. Elsabour,

Amal A. El‐Masry

et al.

BMC Chemistry, Journal Year: 2024, Volume and Issue: 18(1)

Published: June 12, 2024

Abstract A new, sensitive, and rapid isocratic reversed phase chromatographic method (RP-HPLC–UV) was developed for simultaneous separation of two newly co-formulated antiulcer mixtures; Amoxicillin, Vonoprazan Clarithromycin [Mixture (I)], Lansoprazole (II)]. Analytical performed using a Promosil C 18 column ultraviolet detection at 210 nm. The achieved within only 8 min. For both mixtures, an aqueous solution, composed (Acetonitrile: Methanol: 0. 2 M phosphoric acid) ratio (30: 30: 40) adjusted to final pH 3.0, the mobile phase. This validated as per International Conference on Harmonization guidelines. linearity ranges these proposed (Mixture (I)) were 25.0–400.0 µg/mL 0.5–8.0 Vonoprazan, 12.5–200.0 Clarithromycin. And (II)) 10.0–300.0 0.3–9.0 5.0–150.0 firstly applied effective (I)]. It fulfilled good repeatability, sensitivity, accuracy (R.S.D. < 2.0%). mean recoveries analytes in their Tri-Pak formulations acceptable. greenness methods assessed Eco-scale it content uniformity testing United States Pharmacopoeia (USP) acceptance value Mixture (I) 2.88, values (II) 2.592, 2.424, respectively.

Language: Английский

Citations

5
Recent developments in sample pretreatment techniques for the determination of fluoroquinolones in foods DOI
Irina Timofeeva,

Kirill Barbayanov,

Maria Kochetkova

et al.

TrAC Trends in Analytical Chemistry, Journal Year: 2024, Volume and Issue: 178, P. 117831 - 117831

Published: June 22, 2024

Language: Английский

Citations

5
Microplastic and Associated Emerging Contaminants in Marine Fish from the South China Sea: Exposure and Human Risks DOI
Xiaoxuan Yu,

Qilin Gutang,

Yuxuan Wang

et al.

Journal of Hazardous Materials, Journal Year: 2024, Volume and Issue: 480, P. 136200 - 136200

Published: Oct. 16, 2024

Language: Английский

Citations

4
Breaking barrier of binding buffer in colorimetric aptasensing of tetracycline in food fish using peroxidase mimic gold NanoZyme DOI
Dhruba Jyoti Sarkar,

Ramij Raja,

Vikash Kumar

et al.

Methods, Journal Year: 2025, Volume and Issue: unknown

Published: April 1, 2025

Language: Английский

Citations

0
Occurrence and distribution of selected pharmaceuticals in fresh fish along the Kenyan coast and assessment of potential human health risks DOI Creative Commons

Veronica Wayayi Ogolla Wanjeri,

Eric Ochieng Okuku, Jane Catherine Ngila

et al.

Environmental Science Advances, Journal Year: 2025, Volume and Issue: unknown

Published: Jan. 1, 2025

Fish consumption is known to have several health benefits.

Language: Английский

Citations

0
Dispersive Solid-Phase Extraction and Ultra-Performance Liquid Chromatography–Tandem Mass Spectrometry—A Rapid and Accurate Method for Detecting 10 Macrolide Residues in Aquatic Products DOI Creative Commons
Jinyu Chen,

Guangming Mei,

Xiaojun Zhang

et al.

Foods, Journal Year: 2024, Volume and Issue: 13(6), P. 866 - 866

Published: March 13, 2024

The amount of macrolide (MAL) residues in aquatic products, including oleandomycin (OLD), erythromycin (ERM), clarithromycin (CLA), azithromycin (AZI), kitasamycin (KIT), josamycin (JOS), spiramycin (SPI), tilmicosin (TIL), tylosin (TYL), and roxithromycin (ROX), was determined using solid-phase extraction ultra-performance liquid chromatography–tandem mass spectrometry (UPLC-MS/MS). were extracted with 1% ammonia acetonitrile solution purified by neutral alumina adsorption. Chromatographic separation completed on an ACQUITY UPLC BEH C18 column acetonitrile–0.1% formic acid aqueous as the mobile phase, detection performed multiple reaction monitoring scanning positive mode electrospray ion source (ESI+). Five isotopically labeled compounds used internal standards for quality control purposes. findings indicated that across concentration span 1.0–100 μg/L, there a strong linear correlation (R2 > 0.99) between instrumental response 10 MALs. limit UPLC-MS/MS 0.25–0.50 μg/kg, quantitation 0.5–1.0 μg/kg. added recovery blank matrix samples at standard gradient levels (1.0, 5.0, 50.0 μg/kg) 83.1–116.6%, intra-day precision inter-day precisions 3.7 13.8%, respectively. method is simple fast, high accuracy good repeatability, line requirements accurate qualitative quantitative analysis MALs products.

Language: Английский

Citations

3