Journal of Pharmaceutical Analysis,
Год журнала:
2024,
Номер
14(11), С. 101013 - 101013
Опубликована: Май 25, 2024
Green
analytical
chemistry
(GAC)
focuses
on
mitigating
the
adverse
effects
of
activities
human
safety,
health,
and
environment.
In
addition
to
12
principles
GAC,
proper
GAC
tools
should
be
developed
employed
assess
greenness
different
assays.
The
15
widely
used
metrics,
i.e.,
national
environmental
methods
index
(NEMI),
advanced
NEMI,
assessment
green
profile
(AGP),
chloroform-oriented
toxicity
estimation
scale
(ChlorTox
Scale),
Analytical
Eco-Scale,
Certificate
Modified
method
score
(AMGS),
procedure
(GAPI),
ComplexGAPI,
red-green-blue
(RGB)
additive
color
model,
RGB
algorithm,
calculator
(AGREE),
AGREE
preparation
(AGREEprep),
HEXAGON,
blue
applicability
grade
(BAGI),
are
selected
as
typical
tools.
This
article
comprehensively
presents
elucidates
principles,
characteristics,
merits,
demerits
review
is
helpful
for
researchers
use
current
metrics
sustainability
Green Analytical Chemistry,
Год журнала:
2024,
Номер
9, С. 100107 - 100107
Опубликована: Март 21, 2024
Intestinal
coccidiosis
is
a
serious
parasitic
disease
in
poultry.
Amprolium
hydrochloride(AMP)
widely
used
for
the
treatment
and
prevention
of
coccidiosis.
Three
simple
green
spectrophotometric
methods
have
been
developed
assay
AMP
bulk
powder
dosage
form.
The
first
method
relies
on
measuring
derivative
(D1)
spectrum
at
Δλ=
3
nm
AMP.
This
D1
possesses
characteristic
peak
234
nm.
second
difference
spectrophotometry
(ΔA)
its
(ΔD1)
spectra
drug
solutions
0.1
N
HCl
against
corresponding
NaOH.
value
amplitudes
ΔA
ΔD1
(∆λ
=
nm)
were
measured
248
240
nm,
respectively.
third
involves
colorimetric
reaction
with
KMnO4
alkaline
medium
colored
product
610
validated
accordance
ICH
guidelines
evaluated
greenness
using
three
metrics;
Analytical
Eco-Scale
(AES),
GREEness
calculator
(AGREE),
Green
Procedure
Index
(GAPI).
All
proposed
showed
excellent
simplicity
as
they
don't
require
sophisticated
instrumentation
or
tedious
analytical
procedure
steps.
Molecules,
Год журнала:
2024,
Номер
29(13), С. 3169 - 3169
Опубликована: Июль 3, 2024
Interest
in
measuring
major
and
trace
elements
plants
has
increased
recent
years
because
of
growing
concerns
about
the
elements'
contribution
to
daily
intakes
or
health
risks
posed
by
ingesting
vegetables
contaminated
potentially
toxic
elements.
The
advances
using
inductively
coupled
plasma
atomic
emission
spectrometry
(ICP-OES)
measure
plant
samples
are
reviewed
present
work.
sample
preparation
before
instrumental
determination
main
advantages
limitations
ICP-OES
described.
New
trends
element
extraction
liquid
solutions
fewer
solvents
microextractions
observed
recently
published
literature.
Even
though
is
a
well-established
routine
technique,
innovations
increase
its
performance
have
been
found.
Validated
methods
needed
ensure
obtaining
reliable
results.
Much
research
focused
on
assessing
principal
figures
merit,
such
as
limits
detection,
quantification,
selectivity,
working
ranges,
precision
terms
repeatability
reproducibility,
accuracy
through
spiked
certified
reference
materials
analysis.
According
literature,
50
after
release
first
commercially
available
equipment,
remains
powerful
highly
recommended
tool
for
wide
range
concentrations.
