Organic Letters, Год журнала: 2025, Номер unknown
Опубликована: Март 25, 2025
A new catalytic conversion type of nitro substrate with CO2 as a single-carbon source is presented, wherein great collection azaheterocycles generated by newly established iridium-catalyzed, copper-induced reductive system. This procedure handily employs poly(methylhydrosiloxane) (PMHS) the reductant to simultaneously realize dual reduction highest oxidation-state and units in one operation. Elaborate mechanistic studies illustrate essential role iridium catalyst reducing NO2 moiety well double functions copper additive subsequent formylation C-H cyclization steps.
Язык: Английский