Optimization of Ultrasonic-Assisted Extraction of Phenolics and Terpenoids from Sweet Basil Leaves Using Natural Deep Eutectic Solvents DOI Creative Commons
Tan Phat Vo, Thuy Han Phan,

Nguyen Thuc Doan Luu

и другие.

International Journal of Chemical Engineering, Год журнала: 2024, Номер 2024, С. 1 - 13

Опубликована: Фев. 28, 2024

This investigation focused on assessing and enhancing ultrasound-assisted extraction (UAE) using natural deep eutectic solvents (NADES) to extract phenolics terpenoids from sweet basil leaves. The initial stage involved evaluating the performance of twelve NADES ethanol. A comprising lactic acid glucose with a 2 : 1 molar ratio 20% water content (WC) obtained highest total phenolic (TPC) terpenoid (TTC). Single-factor experiments systematically examined impact liquid-to-solid (LSR), in (WC), ultrasound power, temperature, exposure time yield. Optimization Box–Behnken Design (BBD) models for glucose-based UAE revealed optimal conditions be 80 ml/g LSR, 30% water, 300 W, 50°C 15-minute time. Under these optimized parameters, achieved TPC TTC at 69.88 mg GAE/g 110.71 UA/g, respectively. study presents an environmentally friendly sustainable protocol compounds

Язык: Английский

Exploring Natural Deep Eutectic Solvents (NADES) for Enhanced Essential Oil Extraction: Current Insights and Applications DOI Creative Commons

Luis Acosta-Vega,

Alejandro Cifuentes, Elena Ibáñez

и другие.

Molecules, Год журнала: 2025, Номер 30(2), С. 284 - 284

Опубликована: Янв. 13, 2025

Essential oils (EOs) are highly valued in the cosmetic and food industries for their diverse properties. However, traditional extraction methods often result low yields, inconsistent compositions, lengthy times, use of potentially harmful solvents. Natural deep eutectic solvents (NADES) have emerged as promising alternatives, offering advantages such higher efficiency, cost-effectiveness, biodegradability, tunable This review explores application NADES enhancing EO extraction, focusing on current methodologies, key insights, practical applications. It examines factors that influence with NADES, including optimization physicochemical properties, techniques, operational conditions, role sample pretreatment improving efficiency. Additionally, this covers chemical characterization biological activities EOs extracted using NADES. By providing a comprehensive overview, it highlights potential to improve suggests directions future research field.

Язык: Английский

Процитировано

3

The Effects of Selected Extraction Methods and Natural Deep Eutectic Solvents on the Recovery of Active Principles from Aralia elata var. mandshurica (Rupr. & Maxim.) J. Wen: A Non-Targeted Metabolomics Approach DOI Creative Commons

Alyona Kaleta,

Nadezhda Frolova, Anastasia Orlova

и другие.

Pharmaceuticals, Год журнала: 2024, Номер 17(3), С. 355 - 355

Опубликована: Март 9, 2024

The methods and solvents employed in routine extraction protocols essentially impact the composition of resulting extracts, i.e., relative abundances individual biologically active metabolites quality stability isolates. Natural deep eutectic (NADESs) represent a new class environmentally friendly solvents, which are recognized as promising extractants alternative to conventional organic liquids. However, their efficiencies when applied different workflows still poorly characterized. Therefore, here, we compare potential three for natural products from Aralia elata var. mandshurica with selected using non-targeted metabolomics approach. metabolite profiling relied on reversed-phase ultra-high-performance liquid chromatography–high-resolution mass spectrometry (RP-UHPLC-HR-MS). roots A. were extracted by maceration, ultrasound-assisted (UAE), vibrocavitation-assisted (VAE). Principal component analysis (PCA) revealed clear separation extracts obtained NADES1 (choline chloride/malic acid) NADES2 (sorbitol/malic acid/water). Based results hierarchical clustering normalized further statistical evaluation t-test, it could be concluded that showed superior efficiency all addressed. this NADES was more detail. PCA followed t-test yielded only 3 efficiently whereas 46 compounds abundant VAE. When VAE UAE compared, 108 appeared VAE, 1 recovered UAE. These facts clearly indicate advantage method over maceration Seven twenty-seven tentatively identified tandem (MS/MS) found first time. Additional studies necessary understand applicability other plant materials.

Язык: Английский

Процитировано

12

Biofungicides Based on Plant Extracts: On the Road to Organic Farming DOI Open Access
Antonio de Jesús Cenobio-Galindo, Alma Delia Hernández-Fuentes, Uriel González-Lemus

и другие.

International Journal of Molecular Sciences, Год журнала: 2024, Номер 25(13), С. 6879 - 6879

Опубликована: Июнь 22, 2024

Phytopathogenic fungi are responsible for diseases in commercially important crops and cause major supply problems the global food chain. Plants were able to protect themselves from disease before humans played an active role protecting plants. They known synthesize a variety of secondary metabolites (SMs), such as terpenes, alkaloids, phenolic compounds, which can be extracted using conventional unconventional techniques formulate biofungicides; plant extracts have antifungal activity various mechanisms action against these organisms. In addition, they considered non-phytotoxic potentially effective control. sustainable economically viable alternative use agriculture, is why biofungicides increasingly recognized attractive option solve caused by synthetic fungicides. Currently, organic farming continues grow, highlighting importance developing environmentally friendly alternatives crop production. This review provides compilation literature on biosynthesis, phytopathogens, extraction formulation biofungicides, biological phytopathogenic fungi, regulation, advantages, disadvantages overview current agriculture.

Язык: Английский

Процитировано

11

Microwave-assisted butylene glycol extraction: An environmentally friendly method for isolating bioactive compounds from coffee silverskin with antioxidant, anti-tyrosinase, and anti-melanogenic effects DOI Creative Commons
Nuntawat Khat‐udomkiri,

Su Myat Win

Industrial Crops and Products, Год журнала: 2025, Номер 226, С. 120647 - 120647

Опубликована: Фев. 6, 2025

Язык: Английский

Процитировано

1

Current developments and trends in hybrid extraction techniques for green analytical applications in natural products DOI

N. K. Soni,

Mukul Yadav,

M. Malarvannan

и другие.

Journal of Chromatography B, Год журнала: 2025, Номер 1256, С. 124543 - 124543

Опубликована: Фев. 27, 2025

Язык: Английский

Процитировано

1

Impact of Microwave Processing on Phytochemicals, Antioxidant Status, Anti-Nutritional Factors and Metabolite Profile of Maize Flour DOI Creative Commons

Alla Yaswanth Naveen Kumar,

Alonkrita Chowdhury,

Rajesh Kumar

и другие.

Applied Food Research, Год журнала: 2025, Номер unknown, С. 100712 - 100712

Опубликована: Янв. 1, 2025

Язык: Английский

Процитировано

1

Extracting phenolics, flavonoids, and terpenoids from Codonopsis pilosula using green solvents DOI
Tan Phat Vo,

Minh Thu Ho,

Phan Uoc Nguyen Nguyen

и другие.

Sustainable Chemistry and Pharmacy, Год журнала: 2023, Номер 37, С. 101395 - 101395

Опубликована: Дек. 21, 2023

Язык: Английский

Процитировано

16

Extracting bioactive compounds and proteins from Bacopa monnieri using natural deep eutectic solvents DOI Creative Commons
Tan Phat Vo,

Tran Ha Phuong Nguyen,

Vy Khang Nguyen

и другие.

PLoS ONE, Год журнала: 2024, Номер 19(3), С. e0300969 - e0300969

Опубликована: Март 29, 2024

This study employed novel extraction methods with natural deep eutectic solvents (NADES) to extract bioactive compounds and proteins from Bacopa monnieri leaves. The conditional influence of ultrasonic-assisted (UAE), microwave-assisted (MAE), enzymatic-assisted (EAE) on the recovery efficiency phenolics, proteins, flavonoids, terpenoids was evaluated. conditions UAE were 50 mL/g LSR, 600W ultrasonic power, 30% water content 40°C for 1 min obtain highest protein contents. MAE 40 400W microwave power 3 reach contents biological compounds. EAE 30 20 U/g enzyme concentration L-Gly-Na molar ratio at 2:4:1, 40% 60 acquire compound Scanning electron microscopy (SEM) is analyze surface leaves before after extraction. Comparing seven conducted find most favorable ones. result showed that UMEAE method effective way exploit suggested effectively extracts terpenoids, DBMP.

Язык: Английский

Процитировано

6

Recovering bioactive compounds from yacon (Smallanthus sonchifolius) using the ultrasonic-microwave-assisted extraction technique DOI Creative Commons
Tan Phat Vo,

Thai Anh Thi Ho,

Nguyen Minh Huy Ha

и другие.

Applied Food Research, Год журнала: 2024, Номер 4(2), С. 100451 - 100451

Опубликована: Июль 24, 2024

The aim of this study was to recover bioactive compounds from Smallanthus sonchifolius roots, including flavonoids, terpenoids, phenolics, vitamin C, and reducing sugar contents, as well examine antioxidant activities using ultrasonic-assisted microwave-assisted extraction technique. Single-factor experiments were employed explore the impact various independent variables, concentration, method, power, duration, temperature, pH, on dependent variables yacon ultrasonic-microwave-assisted method. Plackett-Burman Design Model used screen parameters that significantly influenced efficiency. Box-Behnken utilized optimize extracting process acquire compounds. highest yield total flavonoid contents obtained with 4.00 743.33 W microwave 39.08°C ultrasonic temperature. According optimization, optimum conditions 3.98 36.17 seconds time 40°C To C optimized 1:40 g/mL sample-to-solvent ratio, 3.99 45.33 time, 451.09 power. Regarding terpenoids yield, for 2.48 30.49 49.48 °C Under conditions, recovery flavonoid, terpenoid, 7.95 mg rutin equivalents/g, 47.93 ursolic acid 107.78 ascorbic acid/g, 230.39 D-glucose respectively. Ultrasonic-microwave-assisted showed higher performance than singular methods is regarded a sustainable effective approach target roots.

Язык: Английский

Процитировано

4

Latest Advances in Green Extraction of Polyphenols from Plants, Foods and Food By-Products DOI Creative Commons
Andrea Palos-Hernández, Ana M. Gonzaléz‐Paramás, Celestino Santos‐Buelga

и другие.

Molecules, Год журнала: 2024, Номер 30(1), С. 55 - 55

Опубликована: Дек. 27, 2024

Phenolic compounds present in plants and foods are receiving increasing attention for their bioactive sensory properties, accompanied by consumers’ interest products with health benefits derived from natural rather than artificial sources. This, together the sustainable development goals 21st century, has driven of green extraction techniques that allow obtaining these safety quality required to be applied food, cosmetic pharmaceutical industries. Green involves practices aiming at reducing environmental impact preparation processes, based on using or less-polluting solvents, lower energetic requirements shorter times, while providing greater efficiency recovery target compounds. In this article, principles advances produced recent years regarding isolation polyphenols plants, food waste reviewed.

Язык: Английский

Процитировано

4