One‐pot green synthesis, study of fluorescence properties, and biological activity of pyrano[3,2‐c]chromenes derivatives via mesoporous materials MgO/SBA‐15
Ahmed Chelihi,
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Ridha Hassaine,
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Souad Nachat
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et al.
Journal of Heterocyclic Chemistry,
Journal Year:
2023,
Volume and Issue:
61(3), P. 439 - 457
Published: Dec. 27, 2023
Abstract
This
current
work
describes
the
preparation
of
MgO‐SBA‐15
catalysts
by
ultrasonic
method,
and
it
is
characterized
different
analysis
techniques
XRD,
BET,
SEM,
IRTF.
In
order
to
find
out
an
application
for
this
mesoporous
material,
MgO/SBA‐15
was
used
as
a
heterogeneous
catalyst
in
one‐pot
synthesis
pyrano[3,2‐c]chromenes
derivatives
isolated
at
room
temperature
reaction
according
green
chemistry
criteria.
To
enhance
these
derivatives,
spectroscopic
study
molecular
fluorescence
properties
carried
well
identification
nuclear
magnetic
resonance
FTIR
used.
Furthermore,
biological
activity
experiment
also
out,
from
where
obtained
test
results
were
satisfactory
AC09
,
AC05
AC10
compounds
they
are
checked
after
computation
modeling.
Language: Английский
One-Pot Reactions of Triethyl Orthoformate with Amines
Reactions,
Journal Year:
2023,
Volume and Issue:
4(4), P. 779 - 800
Published: Dec. 2, 2023
One-pot
reactions
offer
advantages
like
easy
automation,
higher
product
yields,
minimal
waste
generation,
operational
simplicity,
and
thus
reduced
cost,
time
energy.
This
review
presents
a
comprehensive
overview
of
one-pot
including
triethyl
orthoformate
amines
as
valuable
efficient
reagents
for
carrying
out
two-,
three-
or
four-component
organic
reactions.
Language: Английский