Microwave-assisted preparation of polysubstituted imidazoles using Zingiber extract synthesized green Cr2O3 nanoparticles DOI Creative Commons
Leila Kafi‐Ahmadi, Shahin Khademinia, Ahmad Poursattar Marjani

et al.

Scientific Reports, Journal Year: 2022, Volume and Issue: 12(1)

Published: Nov. 19, 2022

Abstract Cr 2 O 3 nanoparticles were prepared using Zingiber officinal extract which used as an efficient and reusable catalyst in the practical synthesis of polysubstituted imidazoles by means a convenient reaction aromatic aldehydes with ammonium acetate benzil under microwave irradiation H solvent. The structure compounds was studied IR 1 H-NMR spectrum. most important benefits this process are operational simplicity, reasonable times, excellent yield products. results show that optimal conditions for formation imidazole derivatives follow: power 400 W, time 4–9 min, solvent, 15 mmol amount.

Language: Английский

The electrochemical coupling reactions of organic halides compound in a valuable and practical manner for C C and C–heteroatom formation: An overview DOI Creative Commons
Sara Payamifar, Leila Behrouzi, Ahmad Poursattar Marjani

et al.

Arabian Journal of Chemistry, Journal Year: 2024, Volume and Issue: 17(8), P. 105822 - 105822

Published: May 24, 2024

Owing to the environmental and energy problems nowadays, one of enormous challenges is expanding clean, renewable reduce destructive ecological effects chemical industries. Compared with other traditional processes, electrochemical method has some benefits, such as being selective, causing minor waste, working under mild conditions no external oxidizing or reducing reagents, making this approach more economical eco-friendly. Electrochemistry represents a powerful tool within synthetic organic chemistry. The development part chemistry intends performance reactions employing electrons, including adding removing electrons. Using electric current reagent advantages, simplicity reactions, accessibility materials, replacing toxic applying an eco-friendly environment. During last decades, there been much effort decrease usage fossil fuels, electricity emerged common source. conversion into leads new paths, naturally safe environmentally friendly. Developing electrochemistry approaches for performing high-performance essential reaction green strategy because utilization instead stoichiometric oxidants reductants. Due its helpful friendly ability produce reactive intermediates, advanced considerably in oxidative hydrogen evolution coupling sacrificial anode electroreduction. New developments focus on developing electrolytic catalysts,photoelectrocatalysis, bioelectrosynthesis, optimizing electrode paired electrolysis, artificial intelligence-assisted electrosynthesis. Thus, daily significant number construction projects possibilities electrochemistry. Electrochemical methods constructing compounds have tolerated renewal past decades. Organic wealthy background synthesis. We hope review helps attract attention from researchers by using processes laboratory industrial centers, which pollution create In review, organohalides synthesizing various products summarized discussed since 2000.

Language: Английский

Citations

13

Microwave-assisted preparation of polysubstituted imidazoles using Zingiber extract synthesized green Cr2O3 nanoparticles DOI Creative Commons
Leila Kafi‐Ahmadi, Shahin Khademinia, Ahmad Poursattar Marjani

et al.

Scientific Reports, Journal Year: 2022, Volume and Issue: 12(1)

Published: Nov. 19, 2022

Abstract Cr 2 O 3 nanoparticles were prepared using Zingiber officinal extract which used as an efficient and reusable catalyst in the practical synthesis of polysubstituted imidazoles by means a convenient reaction aromatic aldehydes with ammonium acetate benzil under microwave irradiation H solvent. The structure compounds was studied IR 1 H-NMR spectrum. most important benefits this process are operational simplicity, reasonable times, excellent yield products. results show that optimal conditions for formation imidazole derivatives follow: power 400 W, time 4–9 min, solvent, 15 mmol amount.

Language: Английский

Citations

30