RECENT REVIEW OF THE QUECHERS SAMPLE PREPARATION METHOD FOR FOOD AND ENVIRONMENTAL SAMPLE ANALYSIS DOI Creative Commons

Isah Yusuf Shinkafi,

Abubakar Lawal, Nura Suleiman Gwaram

et al.

FUDMA Journal of Sciences, Journal Year: 2024, Volume and Issue: 8(6), P. 155 - 169

Published: Dec. 5, 2024

Creating reliable, environmentally responsible, and effective processes that ensure the traceability, safety, caliber of their results is one main challenges facing researchers doing multi-residue analysis. The QuEChERS which stands for Quick, Easy, Cheap, Effective, Rugged, Safe method has shown itself to be highly adaptable, yielding positive outcomes with a range analytes. This allows versatility in choice solvents, salts, buffers salting-out partitioning, as well use various sorbents throughout cleanup process. more friendly sample preparation technique fits perfectly analytical chemistry's rising emphasis on sustainability. review paper's goal illustrate primary applications method, focus food environmental investigations. It also covers important improvements history methods offers insights into classes substances have been effectively evaluated this methodology.

Language: Английский

Environmental Applications of Mass Spectrometry for Emerging Contaminants DOI Creative Commons
Anil Kumar Meher,

Akli Zarouri

Molecules, Journal Year: 2025, Volume and Issue: 30(2), P. 364 - 364

Published: Jan. 17, 2025

Emerging contaminants (ECs), encompassing pharmaceuticals, personal care products, pesticides, and industrial chemicals, represent a growing threat to ecosystems human health due their persistence, bioaccumulation potential, often-unknown toxicological profiles. Addressing these challenges necessitates advanced analytical tools capable of detecting quantifying trace levels ECs in complex environmental matrices. This review highlights the pivotal role mass spectrometry (MS) monitoring ECs, emphasizing its high sensitivity, specificity, versatility across various techniques such as Gas Chromatography-Mass Spectrometry (GC-MS), Liquid (LC-MS), High-Resolution Mass (HR-MS). The application MS has facilitated real-time detection volatile organic compounds, comprehensive non-targeted screening unknown contaminants, accurate quantification diverse matrices including water, soil, air. Despite effectiveness, matrix interferences, lack standardized methodologies, limited spectral libraries persist. However, recent advancements, hybrid systems integration artificial intelligence (AI), are paving way for more efficient predictive modeling contaminant behavior. Continued innovation technologies collaborative efforts essential overcome existing ensure sustainable solutions mitigating risks associated with emerging contaminants.

Language: Английский

Citations

1
Unveiling the pharmaceutical footprint in freshwater and seawater: HRMS method optimization, validation, and uncertainty estimation DOI
Christina Nannou, Christina Efthymiou, Vasiliki Boti

et al.

Microchemical Journal, Journal Year: 2025, Volume and Issue: 210, P. 112933 - 112933

Published: Feb. 1, 2025

Language: Английский

Citations

0
Synthesis and Characterization of Molecularly Imprinted Polymers for the Rapid and Selective Determination of Oxytetracycline in Chicken Boiler Meat DOI Open Access
Shendi Suryana,

Aji Najihudin,

Salma Elivania

et al.

Polymers for Advanced Technologies, Journal Year: 2025, Volume and Issue: 36(4)

Published: March 28, 2025

ABSTRACT Oxytetracycline (OTC) residues in poultry meat products can develop antibiotic resistance humans who consume them. Therefore, sensitive analytical techniques are required to measure the quantities of OTC establish whether these commodities safe for consumption. The study used molecular imprinting technology create a sorbent measuring chicken broiler products. computational methods utilized early phases research choose functional monomers were validated using association constant (Ka) and Job plot. We synthesized molecularly polymers (MIPs) two different manufacturing processes, which we then examined. bond energy‐based investigation indicated that hydroxyethyl methacrylic acid (HEMA) was ideal monomer at an OTC‐to‐HEMA molar ratio 1:4. examined Ka HEMA various solvents. highest obtained by combining methanol chloroform. plot showed 1:4 best synthesizing imprinted polymer mixture created MIPs alternative techniques, bulk (MIP1) precipitation (MIP2), with set Physical testing FT‐IR, SEM, PSA, BET demonstrated successful synthesis spherical uniform agglomeration particles particle diameters MIP1 MIP2, respectively, 0.21 μm 0.19 μm. surface areas MIP2 186,416 264,486 m2/g, respectively. findings adsorption capacity show fits Langmuir model well, whereas Freundlich better. recovery rates spike‐chicken 81,42% ± 3,6% when applied 95,30% 2.2% used. results selectivity test also is more effective than it remove from has been spiked while taking another antibiotic. influences measurement spike meat.

Language: Английский

Citations

0
Aquatic photochemistry and transformations of multiclass emerging organic contaminants in environmental water matrices DOI Creative Commons
Aleksander Kravos, Oliver Bajt, Helena Prosen

et al.

Journal of Photochemistry and Photobiology A Chemistry, Journal Year: 2025, Volume and Issue: unknown, P. 116491 - 116491

Published: May 1, 2025

Language: Английский

Citations

0
Determination of Nine Organophosphorus Pesticide Residues in Corn by Capillary Electrophoresis with Solid Phase Extraction DOI Creative Commons

Chunxiu Gu,

Baining Liu,

Kaowen Zhou

et al.

International Journal of Electrochemical Science, Journal Year: 2024, Volume and Issue: unknown, P. 100845 - 100845

Published: Oct. 1, 2024

Language: Английский

Citations

2
RECENT REVIEW OF THE QUECHERS SAMPLE PREPARATION METHOD FOR FOOD AND ENVIRONMENTAL SAMPLE ANALYSIS DOI Creative Commons

Isah Yusuf Shinkafi,

Abubakar Lawal, Nura Suleiman Gwaram

et al.

FUDMA Journal of Sciences, Journal Year: 2024, Volume and Issue: 8(6), P. 155 - 169

Published: Dec. 5, 2024

Creating reliable, environmentally responsible, and effective processes that ensure the traceability, safety, caliber of their results is one main challenges facing researchers doing multi-residue analysis. The QuEChERS which stands for Quick, Easy, Cheap, Effective, Rugged, Safe method has shown itself to be highly adaptable, yielding positive outcomes with a range analytes. This allows versatility in choice solvents, salts, buffers salting-out partitioning, as well use various sorbents throughout cleanup process. more friendly sample preparation technique fits perfectly analytical chemistry's rising emphasis on sustainability. review paper's goal illustrate primary applications method, focus food environmental investigations. It also covers important improvements history methods offers insights into classes substances have been effectively evaluated this methodology.

Language: Английский

Citations

0