Chemical Reviews,
Journal Year:
2025,
Volume and Issue:
unknown
Published: May 1, 2025
The
advancement
of
battery
technology
necessitates
a
profound
understanding
the
physical,
chemical,
and
electrochemical
processes
at
various
scales.
Focused
Ion
Beam-Scanning
Electron
Microscopy
(FIB-SEM)
has
emerged
as
an
indispensable
tool
for
research,
enabling
high-resolution
imaging
multiscale
analysis
from
macroscopic
structures
to
nanoscale
features
multiple
dimensions.
This
review
starts
with
introducing
fundamentals
focused
beam
matter
interaction
under
framework
FIB-SEM
instrumentation
then
explores
application
characterization
on
rechargeable
batteries
(lithium-ion
beyond),
focus
cathode
anode
materials,
well
solid-state
batteries.
Analytical
techniques
such
Energy
Dispersive
X-ray
Spectroscopy,
Backscatter
Diffraction,
Secondary
Mass
Spectrometry
are
discussed
in
context
their
ability
provide
detailed
morphological,
crystallographic,
chemical
insights.
also
highlights
several
emerging
applications
including
workflow
maintain
sample
integrity,
in-operando
characterization,
correlative
microscopy.
integration
Artificial
Intelligence
enhanced
data
predictive
modeling,
which
significantly
improves
accuracy
efficiency
material
is
discussed.
Through
comprehensive
multimodal
analysis,
poised
advance
development
high-performance
paving
way
future
innovations
technology.
International Journal of Low-Carbon Technologies,
Journal Year:
2025,
Volume and Issue:
20, P. 466 - 479
Published: Jan. 1, 2025
Abstract
Lithium-manganese
oxide
batteries
are
known
for
their
long-term
storage
capabilities,
characterized
by
low
impedance
and
high
discharge
capacity.
This
study
aims
to
enhance
these
properties
optimizing
key
battery
components.
XRD
analysis
of
MnO2
(MD)
powder,
heat-treated
at
400
°C
5
hours,
revealed
improved
In
addition,
hot-pressed
polypropylene
nonwoven
separators
with
electrolyte
absorption
exceeding
67
mg
successfully
reduced
after-discharge
minimal
capacity
loss
(0.96%–1.26%).
Last,
the
use
additives
led
a
significant
reduction
in
commercial
electrolytes
X
Y,
contributing
overall
performance
improvement.
RSC Advances,
Journal Year:
2025,
Volume and Issue:
15(16), P. 12372 - 12381
Published: Jan. 1, 2025
Oxidized
carbon
cloth
(OCC)
modified
with
oxygen-containing
functional
groups
(–COOH,
–C–OH)
as
a
host
framework
can
guide
homogeneous
deposition
of
Li
and
restrain
dendrite
growth.
Chemical Reviews,
Journal Year:
2025,
Volume and Issue:
unknown
Published: May 1, 2025
The
advancement
of
battery
technology
necessitates
a
profound
understanding
the
physical,
chemical,
and
electrochemical
processes
at
various
scales.
Focused
Ion
Beam-Scanning
Electron
Microscopy
(FIB-SEM)
has
emerged
as
an
indispensable
tool
for
research,
enabling
high-resolution
imaging
multiscale
analysis
from
macroscopic
structures
to
nanoscale
features
multiple
dimensions.
This
review
starts
with
introducing
fundamentals
focused
beam
matter
interaction
under
framework
FIB-SEM
instrumentation
then
explores
application
characterization
on
rechargeable
batteries
(lithium-ion
beyond),
focus
cathode
anode
materials,
well
solid-state
batteries.
Analytical
techniques
such
Energy
Dispersive
X-ray
Spectroscopy,
Backscatter
Diffraction,
Secondary
Mass
Spectrometry
are
discussed
in
context
their
ability
provide
detailed
morphological,
crystallographic,
chemical
insights.
also
highlights
several
emerging
applications
including
workflow
maintain
sample
integrity,
in-operando
characterization,
correlative
microscopy.
integration
Artificial
Intelligence
enhanced
data
predictive
modeling,
which
significantly
improves
accuracy
efficiency
material
is
discussed.
Through
comprehensive
multimodal
analysis,
poised
advance
development
high-performance
paving
way
future
innovations
technology.
