Halogenation of arenes using alkali metal halides/Fe(NO3)3·9H2O at room temperature DOI Creative Commons

Caicui Li,

Cheng Yao,

Fangfang Pang

et al.

RSC Advances, Journal Year: 2025, Volume and Issue: 15(11), P. 8523 - 8528

Published: Jan. 1, 2025

A simple, efficient and environmentally friendly methodology for the halodecarboxylation of anisole analogues using Fe(NO3)3·9H2O/KBr or NaI at room temperature was developed. In this method, most substrates with an electron-donating group afforded corresponding products in good to excellent yields, whereas those electron-withdrawing low moderate yields. More importantly, protocol also applicable gram-scale synthesis. It is hoped that will be highly useful organic

Language: Английский

Halogenation of arenes using alkali metal halides/Fe(NO3)3·9H2O at room temperature DOI Creative Commons

Caicui Li,

Cheng Yao,

Fangfang Pang

et al.

RSC Advances, Journal Year: 2025, Volume and Issue: 15(11), P. 8523 - 8528

Published: Jan. 1, 2025

A simple, efficient and environmentally friendly methodology for the halodecarboxylation of anisole analogues using Fe(NO3)3·9H2O/KBr or NaI at room temperature was developed. In this method, most substrates with an electron-donating group afforded corresponding products in good to excellent yields, whereas those electron-withdrawing low moderate yields. More importantly, protocol also applicable gram-scale synthesis. It is hoped that will be highly useful organic

Language: Английский

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