Extraction of curcuminoids from Curcuma longa L. by fatty acid-based ionic liquid aqueous solution: Experimental and mechanism study DOI
Yun Tian,

Na Wang,

Huanyu Liu

et al.

Food Chemistry, Journal Year: 2024, Volume and Issue: 464, P. 141605 - 141605

Published: Oct. 9, 2024

Language: Английский

Thin film microextraction of apixaban from plasma based on the covalent organic framework coated on a mesh prior to liquid chromatography-tandem mass spectrometry DOI

Aysan Changizi Kecheklou,

Mohammad Reza Afshar Mogaddam, Saeed Mohammad Sorouraddin

et al.

Journal of Chromatography B, Journal Year: 2024, Volume and Issue: 1247, P. 124302 - 124302

Published: Sept. 20, 2024

Language: Английский

Citations

4
Analytical Methods for the Determination of Apixaban in Pharmaceuticals and Biological Matrices: A Systematic Review DOI
Wanbing Rao,

Chenxia Zhang,

Shuming Wu

et al.

Critical Reviews in Analytical Chemistry, Journal Year: 2025, Volume and Issue: unknown, P. 1 - 16

Published: April 2, 2025

Apixaban (APX) is a direct oral anticoagulant (DOAC) developed by Bristol Myers Squibb and Pfizer for the prevention of stroke systemic embolism in patients with non valvular atrial fibrillation (NVAF), as well prophylaxis deep vein thrombosis (DVT) reduction recurrent DVT pulmonary risk following initial therapy. This paper provides comprehensive review physicochemical properties APX analytical methodologies its quantification bulk drug, pharmaceutical formulations, biological fluids. The methods reported to date have been summarized, an emphasis on major techniques such spectrophotometry, reverse-phase high performance liquid chromatography (RP-HPLC) coupled ultraviolet (UV) detection or mass spectrometry (MS). Sample pretreatment analysis matrices also systematically discussed. Additionally, "whiteness" determination matrix are assessed according RGB 12 algorithm.

Language: Английский

Citations

0
Eco-friendly solvents in liquid–liquid microextraction techniques for biological and environmental analysis: a critical review DOI

Aldana A. Lemos,

Agostina L. Chapana,

Cecilia E. Luján

et al.

Analytical and Bioanalytical Chemistry, Journal Year: 2024, Volume and Issue: unknown

Published: Oct. 11, 2024

Language: Английский

Citations

3
An immobilization of aminopropyl trimethoxysilane-phenanthrene carbaldehyde on graphene oxide for toluene extraction and separation in water samples DOI

Shahnaz Teimoori,

Hamid Shirkhanloo, Amir Hessam Hassani

et al.

Chemosphere, Journal Year: 2023, Volume and Issue: 316, P. 137800 - 137800

Published: Jan. 9, 2023

Language: Английский

Citations

9
Application of bio-metal-organic framework-based magnetic dispersive solid phase extraction for the extraction of polycyclic aromatic hydrocarbons from pasteurized milk DOI
Ali Mohebbi, Ali Fathi, Mohammad Reza Afshar Mogaddam

et al.

Microchemical Journal, Journal Year: 2023, Volume and Issue: 193, P. 109156 - 109156

Published: July 31, 2023

Language: Английский

Citations

7
Evaluating the Simultaneous Electrochemical Determination of Antineoplastic Drugs Using LaNiO3/g-C3N4@RGH nanocomposite material DOI
Wiem Bouali,

Nevin Erk,

Buse Sert

et al.

Talanta, Journal Year: 2024, Volume and Issue: 278, P. 126486 - 126486

Published: June 28, 2024

Language: Английский

Citations

2
Determination of metronidazole and clarithromycin in plasma samples using surfactant-modified amorphous carbon-based DSPE combined with DLLME followed by HPLC DOI Open Access

Faezeh Javanbakht,

Mohammad Reza Afshar Mogaddam, Mahboob Nemati

et al.

Analytical Sciences, Journal Year: 2023, Volume and Issue: 39(8), P. 1287 - 1295

Published: May 14, 2023

This work offers preparation of surfactant-modified amorphous carbon and its application in dispersive solid phase extraction metronidazole clarithromycin from plasma samples. The procedure was combined with liquid-liquid microextraction for further preconcentration the analytes sensitive determination followed by high performance liquid chromatography-diode array detector. In this work, first, sorbent added to sample mixture vortexed adsorb analytes. Then, obtained supernatant after centrifuging is discarded loaded onto surface were eluted a water-miscible organic solvent. following, enrichment step done. For purpose, eluate taken, mixed water-immiscible solvent, injected into deionized water. After centrifuging, an aliquat sedimented taken analytical instrument quantitative analysis. Under optimum conditions, recoveries (79 89% clarithromycin, respectively), low limits detection (2.1 1.9 ng mL-1 respectively) quantification (7.0 6.3 good repeatability (relative standard deviations less than 4.3% intra- 6.3% inter-day precisions), wide linear ranges (7.3-1000 6.3-1000 obtained. At end, introduced method applied on samples patients treated successfully.

Language: Английский

Citations

6
Current advances in carbonaceous materials for analytical applications in liquid phase DOI
Susy Piovesana, Aldo Laganà, Anna Laura Capriotti

et al.

TrAC Trends in Analytical Chemistry, Journal Year: 2023, Volume and Issue: 168, P. 117297 - 117297

Published: Sept. 17, 2023

Language: Английский

Citations

6
Development of microextraction methods for the determination of sulfamethoxazole in water and biological samples: modelling, optimization and verification by central composite design DOI Creative Commons

Issa Sheibani Amin,

Ali Naser Neysari,

Raed H. Althomali

et al.

Frontiers in Environmental Science, Journal Year: 2023, Volume and Issue: 11

Published: Aug. 21, 2023

This study aimed to preconcentration of sulfamethoxazole (SMX) in water and biological samples. Ultrasound-assisted dispersive liquid-liquid microextraction (UA-DLLME) ultrasound-assisted solid-phase (UA-DSPME) methods paired with spectrophotometry were applied extraction SMX. ZnFe 2 O 4 nanoparticles prepared as adsorbent UA-DSPME method by hydrothermal method. The scanning electron microscopy (SEM) technique showed that the had symmetrical, bullet-shaped particles uniform size. results X-ray diffraction (XRD) successful synthesis nanoparticles. Effective parameters extraction, including ultrasonication time, disperser solvent volume, amount, eluent pH investigated optimized. practical optimal conditions process determined central composite design (CCD). 0.024 g adsorbent, 535 µL 7.5 min 235 5, 185 volume. Linear ranges detection limits 20–1,200 μg L −1 6 for 10–800 3 UA-DLLME. Relative standard deviation (RSD) less than 4% obtained UA-DLLME methods. reusability could extract SMX up five cycles adsorption/desorption without significant reduction its efficiency. Also, interference studies presence different cations anions did not significantly interfere outcomes real-time samples analysis both was range 92.44%–99.12%. developed are simple, sensitive, suitable environmental

Language: Английский

Citations

5
A reverse micelle-mediated dispersive liquid-liquid microextraction coupled to high-performance liquid chromatography for the simultaneous determination of agomelatine and venlafaxine in pharmaceuticals and human plasma DOI
Asmaa Kamal El‐Deen, Galal Magdy, Kuniyoshi Shimizu

et al.

Journal of Chromatography A, Journal Year: 2023, Volume and Issue: 1710, P. 464441 - 464441

Published: Oct. 10, 2023

Language: Английский

Citations

5