Green Synthesis, Characterization and Physico-Chemical Properties of Superionic Na Β-Type Hexagonal Ferrite Nanoparticles for Electrochemical Sensor of Cefixime DOI
Sajjad Hussain, Imran Sadiq, Jameel Ahmed Baig

et al.

Published: Jan. 1, 2023

The quantitative study of antibiotics is significant due to their extensive application in treating many diseases worldwide. Cefixime (Cfx) a third-generation cephalosporin medicine used as an antibacterial. In the current project, using ginger root extract, sol-gel green methodology was for sodium β-type hexagonal ferrite nanoparticles (NaFe11O17-NPs). NaFe11O17-NPs were subjected analytical characterization X-ray diffraction (XRD), atomic force microscopy (AFM), field emission scanning electron (FE-SEM), photoelectron spectroscopy (XPS), Brunauer, Emmett and Teller (BET) analysis, UV-visible spectroscopy, vibrating sample magnetometer (VSM) analysis. confirmed prepared material's crystalline behaviour, surface morphology, particle size, area, magnetic nature. drop-casting method efficient electrochemical sensor by modifying gold electrode (AuE) with NaFe11O17-NPs/AuE assist sensitive selective quantification Cfx. fabricated achieved notably low detection limit 14 nM. developed applied successfully quantitatively determine Cfx clinical samples pharmaceutical preparations excellent recoveries from 95.20 102.48%.

Language: Английский

Effect of Mn dopant on physiochemical properties of V2O5 and their photocatalytic application toward mineralization of malachite green (MG) dye DOI

F.F. Alharbi,

Maria Zulfiqar,

Syeda Rabia Ejaz

et al.

Materials Chemistry and Physics, Journal Year: 2024, Volume and Issue: 322, P. 129556 - 129556

Published: June 3, 2024

Language: Английский

Citations

16
Influence of Pr-cations on structural, spectral, elemental, and electrical features of Zr2–R type ferrites DOI

Muhammad Zeeshan Qamar,

Muhammad Irfan, Majid Niaz Akhtar

et al.

Ceramics International, Journal Year: 2024, Volume and Issue: 50(13), P. 23808 - 23824

Published: April 9, 2024

Language: Английский

Citations

9
Green Synthesis, Microstructural Characterization, and Synergizing Effect of Na‐β‐Type Hexagonal Ferrite Nanomaterials as a Probe for Cefixime Electrochemical Sensors DOI Open Access
Sajjad Hussain, Imran Sadiq, Jameel Ahmed Baig

et al.

Microscopy Research and Technique, Journal Year: 2025, Volume and Issue: unknown

Published: March 27, 2025

ABSTRACT The quantitative study of antibiotics is important in various biomedical applications. Cefixime a third‐generation cephalosporin medication used to treat range bacterial infections. In this study, the green synthesis sodium β‐type hexagonal ferrite nanomaterial (NaFe 11 O 17 ‐NMs) was carried out from ginger root extract via sol–gel method. as‐synthesized NMs were characterized atomic force microscopy (AFM), field‐emission scanning electron (FE‐SEM), X‐ray diffraction (XRD), photoelectron spectroscopy (XPS), vibrating sample magnetometer (VSM) analysis, and UV–visible spectroscopy. Furthermore, drop‐casting process synthesize an efficient electrochemical sensor by coating gold electrode (AuE) with NaFe ‐NMs/AuE), which helps sensitive selective quantification cefixime. as‐prepared had remarkably low detection limit 14 nM. as‐fabricated effectively quantify cefixime levels clinical samples pharmaceutical formulations, recoveries ranging 95.20% 102.48%.

Language: Английский

Citations

0
Effect of Mn Doped on Structural, Optical, and Dielectric Properties of BiFe1–xMnxO3 for Efficient Antioxidant Activity DOI Creative Commons
Muhammad Uzair, Shamsa Kanwal,

M.I. Khan

et al.

ACS Omega, Journal Year: 2023, Volume and Issue: 8(45), P. 42390 - 42397

Published: Oct. 31, 2023

Manganese-doped bismuth ferrites were synthesized using the coprecipitation method with green extract Azadirachta indica. Our incorporation of transition element, manganese, into tackles challenge increased leakage current often observed in intrinsic ferrites. We gained key insights through a comprehensive examination structural, dielectric, and optical properties these materials, utilizing Fourier transform infrared spectroscopy (FTIR), impedance spectroscopy, UV-visible respectively. The formation an octahedral geometry was confirmed FTIR technique. indicated that 2% Mn doping is optimal, while we obtained low band gap energy (2.21 eV) high refractive index (3.010) at this amount doping. manufactured materials exhibited typical ferrite-like dielectric response, is, parameter gradually decreased as frequency then stayed constant high-frequency range. Using diphenylpicrylhydrazyl (DPPH) free radical assay, also examined antioxidant activity concluded among different Mn-doped BiFeMnO3-based nanomaterials, 2 wt % BiFeMnO3 shows highest activity. This finding substantiates efficacy optimized material regard to its potent activity, positioning it promising candidate for potential biomedical applications.

Language: Английский

Citations

7
Adopting the sol–gel auto-combustion approach to synthesize the La3+ substituted hexagonal ferrites suitable for permanent magnets and high-frequency applications DOI
Abrar Hussain, Imran Sadiq, Ghulam Mustafa

et al.

Journal of Sol-Gel Science and Technology, Journal Year: 2024, Volume and Issue: 109(3), P. 626 - 638

Published: Jan. 28, 2024

Language: Английский

Citations

2
Modifications in the structural, optical, magnetic, electrical polarization and hyperthermia properties of SrSnFe8O15 V-type hexaferrites with Sm3+ ions substitution DOI

Laraib Ameen,

Asif Ameen,

Farhan Sadiq

et al.

Ceramics International, Journal Year: 2024, Volume and Issue: 50(21), P. 41407 - 41416

Published: Aug. 3, 2024

Language: Английский

Citations

1
Recent Advances in U-type hexagonal ferrites: Synthesis, Characterizations, Magnetic and Absorption Properties DOI Creative Commons
A. Muhammad, Muhammad Irfan, Majid Niaz Akhtar

et al.

Hybrid Advances, Journal Year: 2024, Volume and Issue: 7, P. 100324 - 100324

Published: Nov. 9, 2024

Language: Английский

Citations

1
Synergetic effect of Hexaferrite and reduced Graphene oxide (rGO) in Photothermal therapy and Hyperthermia applications DOI
Muhammad Jamshaid Shabbir,

Ruqyya Aqeel,

M. Hassan

et al.

Synthetic Metals, Journal Year: 2024, Volume and Issue: 309, P. 117775 - 117775

Published: Nov. 4, 2024

Language: Английский

Citations

0
Green Synthesis, Characterization and Physico-Chemical Properties of Superionic Na Β-Type Hexagonal Ferrite Nanoparticles for Electrochemical Sensor of Cefixime DOI
Sajjad Hussain, Imran Sadiq, Jameel Ahmed Baig

et al.

Published: Jan. 1, 2023

The quantitative study of antibiotics is significant due to their extensive application in treating many diseases worldwide. Cefixime (Cfx) a third-generation cephalosporin medicine used as an antibacterial. In the current project, using ginger root extract, sol-gel green methodology was for sodium β-type hexagonal ferrite nanoparticles (NaFe11O17-NPs). NaFe11O17-NPs were subjected analytical characterization X-ray diffraction (XRD), atomic force microscopy (AFM), field emission scanning electron (FE-SEM), photoelectron spectroscopy (XPS), Brunauer, Emmett and Teller (BET) analysis, UV-visible spectroscopy, vibrating sample magnetometer (VSM) analysis. confirmed prepared material's crystalline behaviour, surface morphology, particle size, area, magnetic nature. drop-casting method efficient electrochemical sensor by modifying gold electrode (AuE) with NaFe11O17-NPs/AuE assist sensitive selective quantification Cfx. fabricated achieved notably low detection limit 14 nM. developed applied successfully quantitatively determine Cfx clinical samples pharmaceutical preparations excellent recoveries from 95.20 102.48%.

Language: Английский

Citations

0