Novel Solvent-Free Mechanochemical Synthesis of Znin2s4 Photocatalyst DOI

Lyazzat Mussapirova,

Shuoping Ding, Nina Daneu

et al.

Published: Jan. 1, 2024

Language: Английский

Red mud-based Fe2O3/Cu-Al LDH prepared through mechanochemical synthesis as effective peroxymonosulfate activator for lomefloxacin hydrochloride degradation via radical-nonradical cooperation mechanisms DOI

Junchi Gu,

Guangtao Wei,

Yuliang He

et al.

Journal of Water Process Engineering, Journal Year: 2024, Volume and Issue: 68, P. 106517 - 106517

Published: Nov. 16, 2024

Language: Английский

Citations

3
Solvent-free mechanochemical synthesis of photocatalytically active nanocomposite based on binary and ternary sulfides of zinc and indium DOI Creative Commons
Lyazzat Mussapyrova, Shuoping Ding, Nina Daneu

et al.

Journal of Physics and Chemistry of Solids, Journal Year: 2025, Volume and Issue: 201, P. 112647 - 112647

Published: Feb. 24, 2025

Language: Английский

Citations

0
Novel Solvent-Free Mechanochemical Synthesis of Znin2s4 Photocatalyst DOI

Lyazzat Mussapirova,

Shuoping Ding, Nina Daneu

et al.

Published: Jan. 1, 2024

A novel rapid solvent-free approach for the preparation of zinc indium sulfide (ZIS) photocatalyst is reported herein. In just 15 minutes processing, elemental mixture zinc, and sulfur in a planetary ball mill, considerable amount nanocrystalline ZIS was obtained via mechanochemical synthesis (ZIS-15). The progress followed by X-ray diffraction Raman spectroscopy, showing reaction mechanism proceeds binary intermediate sulfides. detailed investigation lattice parameters Rietveld refinement has shown continuous shrinkage unit cell upon incorporation into sulfide. When milling prolonged further (ZIS-30), color changed from brown to orange increased, albeit it not possible completely transform intermediates (zinc sulfide) ZIS. ZIS-15 ZIS-30 were characterized SEM, TEM, XPS, UV-Vis, PL, SBET zeta potential (ZP) measurements. majority mentioned analyses, provided very similar results, apart ZP values, which documented be -21.6 -11.5 mV ZIS-30, respectively, documenting different surface charge. difference most probably caused higher content case ZIS-15. obvious evidenced also photocatalytic activity decompose Rhodamine B dye, 2.5 times ZIS-15, thus presence seems beneficial. proposed study highlights great suitability sustainable production semiconductor photocatalysts, as calculated E-factor 22.9 much lower than when using traditional hydrothermal synthesis. This accounts atom economy, we are only reactants forming product, whereas chemistry uses salts.

Language: Английский

Citations

0
Novel Solvent-Free Mechanochemical Synthesis of Znin2s4 Photocatalyst DOI

Lyazzat Mussapirova,

Shuoping Ding, Nina Daneu

et al.

Published: Jan. 1, 2024

Language: Английский

Citations

0