Environmental Technology, Journal Year: 2023, Volume and Issue: 45(25), P. 5233 - 5243
Published: Nov. 21, 2023
The study proposed a method for determining total nitrogen (TN) content in activated sludge by ultrasound pre-treatment assisted wet method. Based on the single-factor experiment, with TN as response value, surface methodology was employed to examine individual and interactive effects of three factors: dilution multiple mixture, ultrasonic time, power. At same physico-chemical parameters digestion-oxidation were optimised. results indicated that optimal follows; 225 times, stirring rate 400 r/min, time 22 minutes, power 720 W, added volume potassium persulfate at 8 mL digestion 40 minutes. relative standard deviation (RSD) parallel determination samples using ≤2.77%, spike recovery 98.49-101.43%. method, determine concentration sludge, simpler operate, more accurate.
Language: Английский