
Foods, Journal Year: 2024, Volume and Issue: 13(21), P. 3431 - 3431
Published: Oct. 28, 2024
Phenolic antioxidants such as tert-butylhydroquinone (TBHQ) can prolong the shelf life of edible oils by delaying oxidation process. The excessive use TBHQ damage food quality and public health, so it is necessary to develop an efficient detection technique. In this work, nickel-aluminum double hydroxide (NiAl-LDH) was grown on glucose carbon spheres (GC), which formed porous nanomaterials (named NiAl-LDH@GC-800) after pyrolysis at 800 °C. successful synthesis material verified scanning electron microscopy, X-ray diffraction, photoelectron spectroscopy. obtained NiAl-LDH@GC-800 dopped onto a glass electrode prepare electrochemical sensor for TBHQ. synergistic effect Ni metal reduced from NiAl-LDH high-temperature calcination accelerated transfer rate improved sensitivity sensor. prepared showed low limit (LOD) 8.2 nM, high (4.2 A·M−1), good linear range (20~300 µM) in detecting also successfully used oils, including chili oil, peanut rapeseed oil.
Language: Английский