Electrochemical Characterization of Pyrogenic Carbons: Implications for Degradation of Groundwater Contaminants with Carbon-Based Amendments DOI
Jeffrey M. Hudson, Paul G. Tratnyek

Environmental Science & Technology, Journal Year: 2025, Volume and Issue: unknown

Published: April 15, 2025

Pyrogenic carbons (PCs) are important mediators of biogeochemical redox reactions and contribute to contaminant degradation in some remediation methods. Contaminant by electron transfer from PC is influenced its conductivity storage capacity, atom involving atomic hydrogen, but resolving their contributions difficult. In this study, we developed a method modify working electrodes with agarose-stabilized thin films PCs used them characterize reactivity using 2,4,6-trinitrotoluene (TNT) as model several electrochemical Chronoamperometry showed that TNT reduction rates increase increasing temperature, impedance spectroscopy because the heterogeneous rate constants (k0) inversely correlated resistivity (Rp) films. As result, like biochars, which have higher charge resistance (Rct), give lower rates, whereas Rct activated faster reduction. Current H2O/H+ H2 (HER) was significant only for low Rp PC-films on Pt electrodes. The reactive intermediates involved HER react preferentially quinonoid moieties PC, thereby competing limiting at overpotentials (

Language: Английский

Electrochemical Characterization of Pyrogenic Carbons: Implications for Degradation of Groundwater Contaminants with Carbon-Based Amendments DOI
Jeffrey M. Hudson, Paul G. Tratnyek

Environmental Science & Technology, Journal Year: 2025, Volume and Issue: unknown

Published: April 15, 2025

Pyrogenic carbons (PCs) are important mediators of biogeochemical redox reactions and contribute to contaminant degradation in some remediation methods. Contaminant by electron transfer from PC is influenced its conductivity storage capacity, atom involving atomic hydrogen, but resolving their contributions difficult. In this study, we developed a method modify working electrodes with agarose-stabilized thin films PCs used them characterize reactivity using 2,4,6-trinitrotoluene (TNT) as model several electrochemical Chronoamperometry showed that TNT reduction rates increase increasing temperature, impedance spectroscopy because the heterogeneous rate constants (k0) inversely correlated resistivity (Rp) films. As result, like biochars, which have higher charge resistance (Rct), give lower rates, whereas Rct activated faster reduction. Current H2O/H+ H2 (HER) was significant only for low Rp PC-films on Pt electrodes. The reactive intermediates involved HER react preferentially quinonoid moieties PC, thereby competing limiting at overpotentials (

Language: Английский

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