1,3-Dipolar Cycloadduct of Organometallic Allene with Dipolarophile─An Apparent Hückel–Möbius Aromatic Five-Membered Organometallic Carbene with Ambiphilic Reactivity DOI
Jishnu Sai Gopinath, Pattiyil Parameswaran

Organometallics, Journal Year: 2024, Volume and Issue: 43(13), P. 1411 - 1424

Published: June 25, 2024

1,3-Dipolar cycloaddition reaction is a powerful synthetic for the generation of heterocycles in organic chemistry. However, similar reactions organometallic chemistry are limited. Here, we report structure and bonding A-frame μ-carbido compounds [M2(μ-C)Cl2(μ-dppm)2] (1M, M = Co, Rh, Ir), their with dipolarophile, dimethylacetylenediacetate (DMAD), resulting cycloadduct five-membered bimetallic carbene complexes [M2(μ-C)(μ-DMAD)Cl2(μ-dppm)2] (2M). The geometrical analysis revealed that carbido complex 1M exhibits linear M–C–M spine planar environment around metal atom. indicated has bisallylic anionic type scenario. Accordingly, carbon atom highly electrophilic as by very high values hydride affinities. allylic delocalization enforces compound to act 1,3-dipole. Hence, these undergo stepwise DMAD 2M. center shows ambiphilic reactivity compared nucleophilic Arduengo N-heterocyclic carbene. bimetalla cyclic ring Hückel–Möbius aromatic having 10π electrons, which contrast 6π Hückel-type delocalization.

Language: Английский

Magnetic Antiaromaticity─Paratropicity─Does Not Necessarily Imply Instability DOI Creative Commons
Cina Foroutan‐Nejad

The Journal of Organic Chemistry, Journal Year: 2023, Volume and Issue: 88(20), P. 14831 - 14835

Published: Sept. 29, 2023

Magnetically induced ring currents are a conventional tool for the characterization of aromaticity. Dia- and paratropic thought to be associated with stabilization (aromaticity) destabilization (antiaromaticity), respectively. In present work, I have questioned validity as measure antiaromaticity among monocyclic hydrocarbons. shown that while reduced/oxidized radical ions hydrocarbons sustain strong currents, they often gain extra via cyclic conjugation compared their acyclic counterparts.

Language: Английский

Citations

18

Mechanical performance and durability attributes of biodegradable natural fibre-reinforced composites—a review DOI Creative Commons
Raviduth Ramful

Deleted Journal, Journal Year: 2024, Volume and Issue: 19(1)

Published: Dec. 26, 2024

Abstract With the rising awareness about impact of excessive urbanization on environment, alternative and more eco-friendly materials such as natural fibre-reinforced composites (NFRCs), which have lower embodied energy, can be considered in modern application ranging from construction housing to urban infrastructures order promote concept sustainable development. One current challenges faced by material engineers is develop NFRCs with optimized durability performance correspond high mechanical attributes during their service lifetime while possessing satisfactory degradability trait disposal phase. This proposed review study principally covered state-of-the-art progress made development composite advanced biodegradable NFRC. In first section, key aspects NFRC fabrication including fibres matrix selection, property-enhancing treatment for influence nanostructures composites. second phase this review, fibre-matrix interaction corresponding physical were discussed. The typical failure modes observed outlined means improve facture toughness proposed. Finally, third section comprised degradation assessment components NFRCs, namely fibre reinforcement, interface sections. Additionally, disposing similar environment was assessed, present-day recycling techniques Further research performance, traits enumerated will unquestionably use integration into a wider range engineering applications our society.

Language: Английский

Citations

2

1,3-Dipolar Cycloadduct of Organometallic Allene with Dipolarophile─An Apparent Hückel–Möbius Aromatic Five-Membered Organometallic Carbene with Ambiphilic Reactivity DOI
Jishnu Sai Gopinath, Pattiyil Parameswaran

Organometallics, Journal Year: 2024, Volume and Issue: 43(13), P. 1411 - 1424

Published: June 25, 2024

1,3-Dipolar cycloaddition reaction is a powerful synthetic for the generation of heterocycles in organic chemistry. However, similar reactions organometallic chemistry are limited. Here, we report structure and bonding A-frame μ-carbido compounds [M2(μ-C)Cl2(μ-dppm)2] (1M, M = Co, Rh, Ir), their with dipolarophile, dimethylacetylenediacetate (DMAD), resulting cycloadduct five-membered bimetallic carbene complexes [M2(μ-C)(μ-DMAD)Cl2(μ-dppm)2] (2M). The geometrical analysis revealed that carbido complex 1M exhibits linear M–C–M spine planar environment around metal atom. indicated has bisallylic anionic type scenario. Accordingly, carbon atom highly electrophilic as by very high values hydride affinities. allylic delocalization enforces compound to act 1,3-dipole. Hence, these undergo stepwise DMAD 2M. center shows ambiphilic reactivity compared nucleophilic Arduengo N-heterocyclic carbene. bimetalla cyclic ring Hückel–Möbius aromatic having 10π electrons, which contrast 6π Hückel-type delocalization.

Language: Английский

Citations

0