Zeitschrift für Kristallographie - New Crystal Structures,
Journal Year:
2022,
Volume and Issue:
238(1), P. 149 - 151
Published: Dec. 14, 2022
Abstract
C
28
H
O
7
,
triclinic,
P1‾
$P\overline{1}$
(no.
2),
a
=
11.0746(18)
Å,
b
11.4312(17)
c
11.552(2)
α
77.148(8)°,
β
62.164(8)°,
γ
67.858(8)°,
V
1195.9(4)
Å
3
Z
2,
R
gt
(
F
)
0.0522,
wR
ref
2
0.1862,
T
223(2)
K
.
RSC Advances,
Journal Year:
2024,
Volume and Issue:
14(27), P. 19581 - 19585
Published: Jan. 1, 2024
We
have
developed
a
facile
and
efficient
strategy
for
modular
access
to
furo[3,2-
c
]chromen-4-ones
by
formation
of
furan
ring
from
readily
available
starting
materials
with
broad
functional
group
compatibility
in
single
step.
IUCrData,
Journal Year:
2022,
Volume and Issue:
7(2)
Published: Feb. 25, 2022
In
the
title
compound,
C
23
H
19
NO
5
,
cyano
group
adopts
an
axial
orientation
and
ester
equatorial
orientation.
The
dihedral
angle
between
pendant
phenyl
benzene
ring
of
fused-ring
system
is
25.97
(8)°.
Intramolecular
O—H...O
C—H...O
hydrogen
bonds
are
observed
packing
consolidated
by
C—H...π
interactions.
Zeitschrift für Kristallographie - New Crystal Structures,
Journal Year:
2022,
Volume and Issue:
238(1), P. 149 - 151
Published: Dec. 14, 2022
Abstract
C
28
H
O
7
,
triclinic,
P1‾
$P\overline{1}$
(no.
2),
a
=
11.0746(18)
Å,
b
11.4312(17)
c
11.552(2)
α
77.148(8)°,
β
62.164(8)°,
γ
67.858(8)°,
V
1195.9(4)
Å
3
Z
2,
R
gt
(
F
)
0.0522,
wR
ref
2
0.1862,
T
223(2)
K
.