Advanced Energy and Sustainability Research, Journal Year: 2025, Volume and Issue: unknown

Published: April 24, 2025

Electrochemical processes involving electrified solid–liquid interfaces are pivotal in the area of catalysis reaction. Nevertheless, microscopic characteristics these catalytic interfaces, particularly structural transformations they undergo during reactions, have yet to be fully understood—posing considerable implications for practical applications. Exploring interface between catalysts and electrolytes can provide valuable insights into development a concise electrocatalytic mechanism. Advanced synchrotron X‐ray methodologies demonstrated their efficacy analyzing electronic electrocatalysts. Combined with situ/operando techniques, approaches successfully illuminate dynamic unveil genuine active sites. In this review, comprehensive overview latest advancements key such as scattering spectroscopy, highlighting current limitations challenges, is provided. Building on core principles robust characterization capabilities explored revealing understanding mechanisms. Finally, address complexity processes, “in mechanism probing map” specifically designed liquid–solid offering clear guide systematically uncover fundamental nature mechanisms, proposed

Language: Английский