In-situ monitoring of polymer mechanochemistry: what can be learned from small molecule systems DOI Creative Commons
Niamh Willis‐Fox

Frontiers in Chemistry, Journal Year: 2024, Volume and Issue: 12

Published: Oct. 16, 2024

Using mechanical energy to drive chemical transformations is an exciting prospect improve the sustainability of reactions and produce products not achievable by more traditional methods. In-situ monitoring reaction pathways vital deliver reproducible results required for scale up realize potential mechanochemistry beyond chemistry lab. This mini review will discuss recent advances in in-situ ball milling polymer mechanochemistry, highlighting shared knowledge up.

Language: Английский

Surface-Activated Mechano-Catalysis for Ambient Conversion of Plastic Waste DOI Creative Commons
Adrian H. Hergesell, Renate J. Baarslag, Claire L. Seitzinger

et al.

Journal of the American Chemical Society, Journal Year: 2024, Volume and Issue: 146(38), P. 26139 - 26147

Published: Sept. 9, 2024

Improved recycling technologies can offer sustainable end-of-life options for plastic waste. While polyolefins be converted into small hydrocarbons over acid catalysts at high temperatures, we demonstrate an alternative mechano-catalytic strategy ambient conditions. The mechanism is fundamentally different from classical acidity-driven high-temperature approaches, exploiting mechanochemically generated radical intermediates. Surface activation of zirconia grinding spheres creates redox active surface sites directly the point mechanical energy input. This allows control mechano-radical reactivity, while powder are not active. Optimized milling parameters enable formation 45% C

Language: Английский

Citations

6

Progress Toward Sustainable Polymer Technologies with Ball-Mill Grinding DOI
Antonio Rizzo, Gregory I. Peterson

Progress in Polymer Science, Journal Year: 2024, Volume and Issue: unknown, P. 101900 - 101900

Published: Oct. 1, 2024

Language: Английский

Citations

5

Influence of ball milling parameters on the mechano-chemical conversion of polyolefins DOI Creative Commons
Adrian H. Hergesell, Claire L. Seitzinger,

Justin Burg

et al.

RSC Mechanochemistry, Journal Year: 2024, Volume and Issue: unknown

Published: Dec. 18, 2024

Mechano-chemical plastic recycling suffers from low overall yields. We identified the role of key parameters to maximize mechanical impact increase productivity small hydrocarbons, such as propene, polypropylene.

Language: Английский

Citations

1

Impact of Ball Milling on the Microstructure of Polyethylene Terephthalate DOI Creative Commons

Ali Zaker,

Karine Auclair

ChemSusChem, Journal Year: 2024, Volume and Issue: unknown

Published: Oct. 7, 2024

Polyethylene terephthalate (PET) is a semi-crystalline polymer that finds broad use. Consequently, it contributes to the accumulation of plastics in environment, warranting PET recycling technologies. Ball milling commonly used technique for micronization before transformation. It has also recently been reported as an efficient mixing strategy enzymatic hydrolysis moist-solid mixtures. However, effect on microstructure not systematically investigated. Thus, primary objective this study characterize changes caused by various ball conditions. different forms was examined, including pre- and post-consumer PET, well textiles. The material treated range frequencies duration, analysis particle size, crystallinity differential scanning calorimetry powder X-ray diffraction, morphology electron microscopy. Interestingly, our results suggest convergence ~30 % within 15 minutes at 30 Hz. These are consistent with equilibrium between amorphous crystalline regions being established during milling. combined data constitutes reference guide research.

Language: Английский

Citations

0

In-situ monitoring of polymer mechanochemistry: what can be learned from small molecule systems DOI Creative Commons
Niamh Willis‐Fox

Frontiers in Chemistry, Journal Year: 2024, Volume and Issue: 12

Published: Oct. 16, 2024

Using mechanical energy to drive chemical transformations is an exciting prospect improve the sustainability of reactions and produce products not achievable by more traditional methods. In-situ monitoring reaction pathways vital deliver reproducible results required for scale up realize potential mechanochemistry beyond chemistry lab. This mini review will discuss recent advances in in-situ ball milling polymer mechanochemistry, highlighting shared knowledge up.

Language: Английский

Citations

0