Quantification of polystyrene microplastics in water, milk, and coffee using thermogravimetry coupled with Fourier transform infrared spectroscopy (TGA-FTIR) DOI Creative Commons
Tem Thi Dang, Ece Söğüt, Ilke Uysal‐Unalan

et al.

Chemosphere, Journal Year: 2024, Volume and Issue: 368, P. 143777 - 143777

Published: Nov. 1, 2024

Rapid quantification of plastic contaminants, particularly microplastics (MPs), in foods is a challenge. This study introduces novel method using Fourier transform infrared spectroscopy coupled with thermogravimetric (TGA-FTIR) and chemometric analysis for the MPs foods. A model was performed polystyrene (PS) (1 μm) added to various foods, namely, water, milk, coffee without any pretreatment. Foods were spiked PS microbeads at different concentrations, heated TGA, FTIR spectra gases evolved from TGA collected over time. The spectral data used construct Gram-Schmidt profile identify characteristic peak. spectrum corresponding peak maxima extracted represent specific concentration. dataset selected their associated concentrations preprocessed prior calibration cross-validation PLS regression models, each food matrix studied. results showed that models reliably predicted content R

Language: Английский

Microplastics, microfibers and associated microbiota biofilm analysis in seawater, a case study from the Vesuvian Coast, southern Italy DOI Creative Commons
Manuela Rossi, Alessandro Vergara, Romualdo Troisi

et al.

Journal of Hazardous Materials, Journal Year: 2025, Volume and Issue: 488, P. 137468 - 137468

Published: Feb. 4, 2025

The growing concerns regarding pollution from microplastics (MPs) and microfibers (MFs) have driven the scientific community to develop new solutions for monitoring ecosystems. However, many of proposed technologies still include protocols treating environmental samples that may alter plastic materials, leading inaccurate results both in observation counting. For this reason, we are refining a protocol, based on optical microscopy without use pretreatments, applicable different matrices, which allows not only counting but also complete morphological characterization MPs MFs. Previously, protocol has successfully been tested marine sediments Vesuvian area Gulf Naples (Italy) with good results. In present study, MFs seawater collected same geographical provide comprehensive overview their distribution environments. enabled collection information colonies microorganisms microparticles. Next Generation Sequencing (NGS) metagenomic us characterize microbiota composition sampled MPs, so-called Plastisphere. analytical approach allowed several potentially pathogenic bacteria, represent potential threat environment human health. fact, they exploit ability form biofilms plastics proliferate

Language: Английский

Citations

1

Quantification of polystyrene microplastics in water, milk, and coffee using thermogravimetry coupled with Fourier transform infrared spectroscopy (TGA-FTIR) DOI Creative Commons
Tem Thi Dang, Ece Söğüt, Ilke Uysal‐Unalan

et al.

Chemosphere, Journal Year: 2024, Volume and Issue: 368, P. 143777 - 143777

Published: Nov. 1, 2024

Rapid quantification of plastic contaminants, particularly microplastics (MPs), in foods is a challenge. This study introduces novel method using Fourier transform infrared spectroscopy coupled with thermogravimetric (TGA-FTIR) and chemometric analysis for the MPs foods. A model was performed polystyrene (PS) (1 μm) added to various foods, namely, water, milk, coffee without any pretreatment. Foods were spiked PS microbeads at different concentrations, heated TGA, FTIR spectra gases evolved from TGA collected over time. The spectral data used construct Gram-Schmidt profile identify characteristic peak. spectrum corresponding peak maxima extracted represent specific concentration. dataset selected their associated concentrations preprocessed prior calibration cross-validation PLS regression models, each food matrix studied. results showed that models reliably predicted content R

Language: Английский

Citations

2