Unraveling the Dynamic Properties of New-Age Energy Materials Chemistry Using Advanced In Situ Transmission Electron Microscopy DOI Creative Commons
Subramaniyan Ramasundaram, Sampathkumar Jeevanandham, Natarajan Vijay

et al.

Molecules, Journal Year: 2024, Volume and Issue: 29(18), P. 4411 - 4411

Published: Sept. 17, 2024

The field of energy storage and conversion materials has witnessed transformative advancements owing to the integration advanced in situ characterization techniques. Among them, numerous real-time techniques, especially transmission electron microscopy (TEM)/scanning TEM (STEM) have tremendously increased atomic-level understanding minute transition states during electrochemical processes. Advanced forms situ/operando STEM microscopic techniques also provide incredible insights into material phenomena at finest scale aid monitor phase transformations degradation mechanisms lithium-ion batteries. Notably, solid-electrolyte interface (SEI) is one most significant factors that associated with performance rechargeable SEI critically controls reactions occur electrode-electrolyte interface. Intricate chemical interfaces can be effectively monitored using temperature-sensitive deciphering reaction prevailing pathways nano- micrometer-scale spatial resolution. Further, advent cryogenic (Cryo)-TEM enhanced these studies by preserving native state sensitive materials. Cryo-TEM allows observation metastable phases intermediates are otherwise challenging capture. Along sophisticated Focused ion beam (FIB) induction been instrumental preparing site-specific cross-sectional samples, facilitating high-resolution analysis layers within devices. holistic provides a comprehensive dynamic changes This review highlights recent progress employing state-of-the-art such as TEM, STEM, Cryo-TEM, FIB for detailed investigation structural dynamics

Language: Английский

Unraveling the Dynamic Properties of New-Age Energy Materials Chemistry Using Advanced In Situ Transmission Electron Microscopy DOI Creative Commons
Subramaniyan Ramasundaram, Sampathkumar Jeevanandham, Natarajan Vijay

et al.

Molecules, Journal Year: 2024, Volume and Issue: 29(18), P. 4411 - 4411

Published: Sept. 17, 2024

The field of energy storage and conversion materials has witnessed transformative advancements owing to the integration advanced in situ characterization techniques. Among them, numerous real-time techniques, especially transmission electron microscopy (TEM)/scanning TEM (STEM) have tremendously increased atomic-level understanding minute transition states during electrochemical processes. Advanced forms situ/operando STEM microscopic techniques also provide incredible insights into material phenomena at finest scale aid monitor phase transformations degradation mechanisms lithium-ion batteries. Notably, solid-electrolyte interface (SEI) is one most significant factors that associated with performance rechargeable SEI critically controls reactions occur electrode-electrolyte interface. Intricate chemical interfaces can be effectively monitored using temperature-sensitive deciphering reaction prevailing pathways nano- micrometer-scale spatial resolution. Further, advent cryogenic (Cryo)-TEM enhanced these studies by preserving native state sensitive materials. Cryo-TEM allows observation metastable phases intermediates are otherwise challenging capture. Along sophisticated Focused ion beam (FIB) induction been instrumental preparing site-specific cross-sectional samples, facilitating high-resolution analysis layers within devices. holistic provides a comprehensive dynamic changes This review highlights recent progress employing state-of-the-art such as TEM, STEM, Cryo-TEM, FIB for detailed investigation structural dynamics

Language: Английский

Citations

0