Unraveling nano-scale effects of topotactic reduction in LaNiO2 crystals DOI Creative Commons
Yu‐Mi Wu, Pascal Puphal, Masahiko Isobe

et al.

APL Materials, Journal Year: 2024, Volume and Issue: 12(9)

Published: Sept. 1, 2024

Infinite-layer nickelates stand as a promising frontier in the exploration of unconventional superconductivity. Their synthesis through topotactic oxygen reduction from parent perovskite phase remains complex and elusive process. This study delves into nano-scale effects lattice transformation within LaNiO2 crystals. Leveraging high-resolution scanning transmission electron microscopy spectroscopy, our investigations uncover panorama structural alterations, including grain boundaries coherent twin boundaries, triggered by reduction-induced transformations. In addition, analyses unveil formation an oxygen-rich disordered transition encircling impurities pervading crystalline domains internal strain is accommodated boundary formation. By unraveling these effects, findings provide insights microscopic intricacies process elucidating to infinite-layer nickelate bulk

Language: Английский

Unconventional Crystal Structure of the High-Pressure Superconductor La3Ni2O7 DOI Creative Commons
Pascal Puphal, Pascal Reiss, Niklas Enderlein

et al.

Physical Review Letters, Journal Year: 2024, Volume and Issue: 133(14)

Published: Oct. 4, 2024

The discovery of high-temperature superconductivity in La3Ni2O7 at pressures above 14 GPa has spurred extensive research efforts. Yet, fundamental aspects the superconducting phase, including possibility a filamentary character, are currently subjects controversial debates. Conversely, crystal structure with NiO6 octahedral bilayers stacked along c-axis direction was consistently posited initial studies on La3Ni2O7. Here, we reassess this optical floating zone-grown La3Ni2O7 single crystals that show signs superconductivity. Employing scanning transmission electron microscopy and single-crystal x-ray diffraction under high pressures, observe multiple crystallographic phases these crystals, majority phase exhibiting alternating monolayers trilayers NiO6 octahedra, signifying profound deviation from previously suggested bilayer structure. Using density functional theory, disentangle individual contributions monolayer trilayer structural units to electronic band La3Ni2O7, providing firm basis for advanced theoretical modeling future evaluations potential monolayer-trilayer hosting Published by American Physical Society 2024

Language: Английский

Citations

23

Self-powered ultraviolet position-sensitive detectors based on PrNiO3/Nb-doped SrTiO3 p–n junctions DOI
Xianjie Wang, Chang Hu, Lingli Zhang

et al.

Applied Physics Letters, Journal Year: 2025, Volume and Issue: 126(2)

Published: Jan. 13, 2025

Position-sensitive detectors based on the lateral photovoltaic effect have been widely used in optical engineering for measurement of position, distance, and angles. However, self-powered ultraviolet position-sensitive with high sensitivity fast response are still lacking due to difficulty associated fabrication p-type wide bandgap semiconductors, which hinders their further design enhancement. Here, influence band structures interfacial transport properties performance PrNiO3/Nb:SrTiO3p–n junctions is systematically investigated. Large position relaxation time were observed up 400 K perovskite-based detectors. Hall measurements revealed that photoexcited carriers occurs mainly through interface PrNiO3/Nb:SrTiO3 junctions, resulting a stable effect. This study presents insights avenues designing perovskite oxide enhanced photoelectric performance.

Language: Английский

Citations

0

Three generations of infinite-layer nickelate crystals DOI Creative Commons
Y. Eren Suyolcu, Pascal Puphal, Matthias Hepting

et al.

MRS Communications, Journal Year: 2025, Volume and Issue: unknown

Published: Feb. 3, 2025

Language: Английский

Citations

0

Investigation of spin excitations and charge order in bulk crystals of the infinite-layer nickelate LaNiO2 DOI Creative Commons
Shohei Hayashida, V. Sundaramurthy, Pascal Puphal

et al.

Physical review. B./Physical review. B, Journal Year: 2024, Volume and Issue: 109(23)

Published: June 3, 2024

Recent x-ray spectroscopic studies have revealed spin excitations and charge density waves in thin films of infinite-layer (IL) nickelates. However, clarifying whether the origin these phenomena is intrinsic to material class or attributable impurity phases has presented a major challenge. Here we utilize topotactic methods synthesize bulk crystals IL nickelate LaNiO2 with crystallographically oriented surfaces. We examine using resonant inelastic scattering (RIXS) at Ni L3-edge elucidate correlations material. While detect presence prominent crystals, fingerprints order are absent ordering vectors identified previous thin-film studies. These results contribute understanding properties LaNiO2 establish topotactically synthesized as viable complementary specimens for investigations. Published by American Physical Society 2024

Language: Английский

Citations

1

Realization of a classical Ruddlesden Popper type bilayer nickelate in Sr3Ni2−xAlxO7−δ with unusual Ni4+ DOI Creative Commons
Hasan Yilmaz, Kathrin Küster, Ulrich Starke

et al.

npj Quantum Materials, Journal Year: 2024, Volume and Issue: 9(1)

Published: Nov. 22, 2024

Abstract The discovery of 80 K superconductivity in bilayer La 3 Ni 2 O 7 at pressures greater than 14 GPa presents a unique opportunity to study novel class high-temperature superconductors. Therefore, other nickelates following the classical ( T 4+ ) Ruddlesden-Popper (RP) series Sr would present an interesting new candidate. In this work, we stabilization RP n = phase 2− x Al 7− δ , via floating zone growth crystals. With powder and single-crystal XRD, stability range RP-type phase. Our Thermogravimetric Analysis (TGA), X-ray photoelectron spectroscopy (XPS) gas extraction studies reveal remarkably high oxidation state stabilized by chemical strain from Al. obtained black crystals are insulating transport show magnetic transition around 12 K.

Language: Английский

Citations

1

Unraveling nano-scale effects of topotactic reduction in LaNiO2 crystals DOI Creative Commons
Yu‐Mi Wu, Pascal Puphal, Masahiko Isobe

et al.

APL Materials, Journal Year: 2024, Volume and Issue: 12(9)

Published: Sept. 1, 2024

Infinite-layer nickelates stand as a promising frontier in the exploration of unconventional superconductivity. Their synthesis through topotactic oxygen reduction from parent perovskite phase remains complex and elusive process. This study delves into nano-scale effects lattice transformation within LaNiO2 crystals. Leveraging high-resolution scanning transmission electron microscopy spectroscopy, our investigations uncover panorama structural alterations, including grain boundaries coherent twin boundaries, triggered by reduction-induced transformations. In addition, analyses unveil formation an oxygen-rich disordered transition encircling impurities pervading crystalline domains internal strain is accommodated boundary formation. By unraveling these effects, findings provide insights microscopic intricacies process elucidating to infinite-layer nickelate bulk

Language: Английский

Citations

0